Current through August 26, 2024
The owner or operator of a source required to conduct
emission testing under s.
NR 439.075 shall comply with all applicable methods and
procedures listed in this section.
(1)
GENERAL. All emission tests conducted for the purpose of determining compliance
with an emission limitation under chs.
NR
400 to
499 shall be performed according
to the test methods established in 40 CFR part 60, Appendix A, 40 CFR part 61, Appendix B, and 40 CFR part 63, Appendix A, incorporated by reference in s.
NR 484.04(13), (23), and (25), or
according to other test methods approved in writing by the department. The
owner, operator or contractor responsible for emission testing shall follow the
procedures in this section. Unless the department requires or approves the
performance of a test at less than capacity, all compliance emission tests
shall be performed with the equipment operating at capacity or as close to
capacity as practicable.
(2)
EMISSION TEST NOTIFICATION AND TEST PLAN SUBMITTAL. The department shall be
notified in writing at least 20 business days in advance of a compliance
emission test, including initial certification tests and relative accuracy
tests performed under s.
NR 439.09, to provide the department an opportunity to
have a representative present to witness the testing procedures. The notice
shall provide a test plan which includes, but need not be limited to, the
following:
(a) A description of the sampling
equipment and the test methods and procedures to be used.
(b) A description of the process to be
tested.
(c) A description of the
process or operation variables which affect the air contaminant source's
emissions.
(d) The date and
starting time of the test.
(e) A
description of the number and location of the sampling ports and sampling
points including a sketch showing the distance of the sampling ports from the
nearest upstream and downstream flow disturbances and the stack
dimensions.
(f) A statement
indicating the production rate and the operating conditions at which the test
will be conducted.
(3)
TEST PLAN EVALUATION. In evaluating the test plan, the department shall respond
to the source owner or operator within 10 business days of receipt of the plan
and may require the following:
(a) A pre-test
conference which includes the owner or operator of the source, the tester and
the department to discuss any deficiencies in the plan or settle any test
procedure questions the department, the tester or the source owner or operator
might have.
(b) Any reasonable
stack or duct modification or any change to the sampling method that is deemed
necessary by the department to obtain a representative sample.
(c) Additional tests for the same pollutants
to be performed at the same or different operating conditions.
(d) A rescheduling of the test to accommodate
witnessing or source production schedules.
(4) NOTIFICATION OF TEST PLAN REVISION. The
source owner or operator shall notify the department of any modifications to
the test plan at least 5 business days prior to the test. In the event the
owner or operator is unable to conduct the compliance emission test on the date
specified in the test plan, due to unforeseeable circumstances beyond the owner
or operator's control, the owner or operator shall notify the department at
least 5 business days prior to the scheduled compliance emission test date and
specify the date when the test is rescheduled.
(5) TESTING FACILITIES. The department may
require the owner or operator of a source to provide the following emission
testing facilities:
(a) The installation of
sampling ports and safe sampling platforms.
(b) A safe work area for the test crew or any
witnessing personnel.
(c) Safe
access to the work area or sampling platform.
(d) Utilities for the sampling
equipment.
(e) Instrumentation to
monitor and record emissions data.
(6) WITNESSING REQUIREMENTS. The department
may require that a department representative be present at any compliance
emission test. The department representative has the following authority:
(a) The department representative shall,
during the test, supply the tester with the appropriate audit samples required
in the reference method for quality assurance purposes.
(b) The department representative may require
the tester to provide the department a copy of all test data and equipment
calibration data prepared or collected for the test.
(c) The department representative may take
any or all of the test samples collected during the test for analysis by the
department.
(d) The department
witness may require the source owner or operator and tester to correct any
deficiency in the performance of the test provided that the department witness
notifies the source owner or operator and tester of the deficiency as soon as
it is discovered. The failure of a source owner or operator and tester to
correct any deficiency may result in the department refusing to accept the
testing results.
(7)
EMISSION TESTING EQUIPMENT CALIBRATION REQUIREMENTS. The following components
of any emission sampling train or associated sampling equipment shall be
calibrated not more than 60 days before the test:
(a) Any equipment used to measure gas
velocity.
(b) Any equipment used to
meter sample gas volume.
(c) Any
equipment used to regulate sample gas flow.
(d) Any equipment used to measure
temperature.
(e) Any gas sampling
nozzle used during the emission test.
(f) Any equipment used to determine gas
molecular weight.
(g) Any other
sampling equipment that requires periodic calibration.
(8) PROCEDURES FOR CONDUCTING COMPLIANCE
EMISSION TESTS. In conducting any compliance emission test the following
procedures apply:
(a)
General
provisions. Except as provided for in par. (c), (d), (f) or (g), an
emission test shall consist of a minimum of 3 representative repetitions, as
determined by the department, of the applicable test method with a minimum
sampling time of one hour per repetition. Shorter sampling times as referenced
in par. (g) may be used with the written approval of the department. The
arithmetic mean of the results of all repetitions shall be used to determine
compliance with an emission limitation. In addition, the following requirements
apply:
1. The gas flow rate, in dry standard
cubic feet per minute, shall be determined during each repetition of an
emission test using Method 1, 1A, 2, 2A, 2B, 2C, 2D, 2E, 2F, 2G, 2H, 3, 3A, 3B,
and 4 in 40 CFR part 60, Appendix A, incorporated by reference in s.
NR 484.04(13), as applicable.
2. A record shall be maintained of all
persons who have handled the test samples.
(b)
Particulate matter. When
compliance with a particulate emission limitation is determined using Method 5,
5A, 5B, 5D, 5E, 5F, 5G, 5H, 5I, or 17 in 40 CFR part 60, Appendix A,
incorporated by reference in s.
NR 484.04(13), the test shall consist of
3 representative repetitions. In addition, the following provisions apply:
1. Sootblowing shall be performed during one
repetition of each test for particulate emissions on any boiler that routinely
employs sootblowing, unless the boiler uses a continuous sootblowing system. If
a continuous sootblowing system is operating during the test, compliance with
the emission limitation shall be determined by the arithmetic mean of the
results of all repetitions. If a continuous sootblowing system is not operating
during the test, the representative average pounds of particulate emissions per
million Btu heat input shall be determined by the following equation:
E = Es ((A + B) S/AR) +
Ens((R - S)/R - (BS/AR))
where:
E is the weighted average pounds of particulate matter per
million Btu heat input
Es is the pounds of particulate
matter per million Btu heat input for test runs during sootblowing
Ens is the arithmetic average pounds
of particulate matter per million Btu heat input for test runs with no
sootblowing
A is the hours of sootblowing during test runs containing
sootblowing
B is the hours with no sootblowing during test runs
containing sootblowing
R is the average hours of boiler operation per 24 hours
S is the average hours of sootblowing per 24 hours
2. Each repetition for a
particulate emission test shall have a sample volume of at least 30 dry
standard cubic feet.
3. Method 17,
for particulates, in 40 CFR part 60, Appendix A, incorporated by reference in
s.
NR 484.04(13), may not be used where
stack or duct temperatures exceed 320°F.
4. Heat input shall be equal to the fuel use
rate multiplied by the heat content of the fuel on an as-fired basis. Fuels
shall be analyzed for heat content using the procedures in Method 19 in 40 CFR
part 60, Appendix A, incorporated by reference in s.
NR 484.04(13).
5. Any boiler emission rate in pounds per
million Btu heat input shall be determined using the heat input based on fuel
use rate. The emission rate may be determined using the F-Factor calculation
shown in Method 19 in 40 CFR part 60, Appendix A, incorporated by reference in
s.
NR 484.04(13), with written approval
from the department. If the F-Factor method is used, an ultimate fuel analysis
shall be performed. An integrated gas sample, using Method 3, 3A or 3B in 40
CFR part 60, Appendix A, incorporated by reference in s.
NR 484.04(13), shall be collected and
analyzed for oxygen and carbon dioxide content. Other methods for determining
the boiler heat input may be used only if approved, in writing, by the
department.
6. If cyclonic flow is
a possibility at a particulate emission test location, a test for the presence
of cyclonic flow shall be performed before the particulate test using the
procedures in Method 1 in 40 CFR part 60, Appendix A, incorporated by reference
in s.
NR 484.04(13). If cyclonic flow is
present, the flow must be straightened before testing can begin unless the
source owner or operator demonstrates, to the department's satisfaction, the
acceptability of the location using the alternate procedure to Method 1. If
cyclonic flow is not present, testing can proceed.
7. Except for sources subject to emission
testing requirements in ch. NR 440, the department may require the owner or
operator of a source capable of emitting condensible particulate matter, to
include an analysis of the back half of the stack sampling train catch in the
total particulate catch for any emission test using Method 5, 5A, 5B, 5D, 5E,
5F, 5G, 5H, 5I, or 17, in 40 CFR part 60, Appendix A, incorporated by reference
in s.
NR 484.04(13). This procedure and
analysis shall be performed using Method 202 in 40 CFR part 51, Appendix M,
incorporated by reference in s.
NR 484.04(9).
(c)
Sulfur dioxide
emissions.
1. When compliance with a
sulfur dioxide emission limitation is determined using Method 6 or 6A in 40 CFR
part 60, Appendix A, incorporated by reference in s.
NR 484.04(13), the test shall consist of
3 repetitions. A repetition shall consist of 2 20-minute sampling periods with
each sampling period followed by a 15-minute fresh air purge. The 2 samples
shall be analyzed independently. The arithmetic mean of the results of the 2
samples shall be the result of that repetition.
2. When compliance with a sulfur dioxide
emission limitation is determined using Method 6B in 40 CFR part 60, Appendix
A, incorporated by reference in s.
NR 484.04(13), the test shall consist of
3 24-hour repetitions with the sampling train operating continuously during
each 24-hour repetition.
3. When
compliance with a sulfur dioxide emission limitation is determined using Method
6C in 40 CFR part 60, Appendix A, incorporated by reference in s.
NR 484.04(13), the test shall consist of
3 representative repetitions.
(d)
Nitrogen oxide
emissions.
1. When compliance with a
nitrogen oxide emission limitation is determined using Method 7, 7A or 7B in 40
CFR part 60, Appendix A, incorporated by reference in s.
NR 484.04(13), the test shall consist of
3 repetitions. A repetition shall consist of 4 2-liter evacuated sample bottles
that are filled, one at a time, with stack gas at 15 minute intervals. The 4
samples shall be analyzed independently. The arithmetic mean of the results of
the 4 samples shall be the result of that repetition.
2. When compliance with a nitrogen oxide
emission limitation is determined using Method 7C, 7D, or 7E in 40 CFR part 60,
Appendix A, incorporated by reference in s.
NR 484.04(13), the test shall consist of
3 representative repetitions.
(e)
Organic compound
emissions. When compliance with an organic compound emission
limitation is determined using Methods 18, 25, 25A, or 25B in 40 CFR part 60,
Appendix A, incorporated by reference in s.
NR 484.04(13), the test shall consist of
a minimum of 3 representative repetitions.
(f)
Visible emissions. When
compliance with a visible emission limitation is determined using Method 9 in
40 CFR part 60, Appendix A-4, incorporated by reference in s.
NR 484.04(13), the test shall be
performed based on the either of the following time criteria, unless otherwise
specified in any applicable regulation, permit or compliance order:
1. For a new construction permit, operation
permit or a renewal of an operation permit, the minimum total time of
observations shall be 60 minutes, consisting of 10 6-minute averages.
2. For any other circumstances, the minimum
total time of observations shall be 18 minutes, consisting of 3 6-minute
averages.
(g)
Exceptions. With department approval, compliance with pars.
(a) to (e) may be determined as the arithmetic mean of 2 representative
repetitions if 3 repetitions cannot be used to determine compliance because of
any of the following circumstances:
1. A
shutdown of the process being tested due to circumstances beyond the control of
the source owner or operator.
2. A
production cycle that does not allow for 3 repetitions of the test
method.
3. The interruption of the
test by unfavorable weather.
4. The
accidental loss of a sample.
5. Any
other circumstances beyond the control of the tester or the owner or operator
of the source.
(9) EMISSION TEST REPORTING REQUIREMENTS. The
owner or operator of the source tested, including initial certification tests
and relative accuracy tests performed under s.
NR 439.09, shall submit 2 copies of the emission test
report to the department within 60 days after completion of a compliance
emission test if no samples were collected by the department witness. If
samples were collected by the department, the test report shall be submitted
within 30 days after the results from the test samples have been reported to
the source owner or operator by the department. If requested, the department
may grant an extension of up to 30 days for test report submittal. The failure
to include the following information in an emission test report may result in
rejection of the test. The emission test report shall include, but need not be
limited to, the following information:
(a) A
detailed description of the process tested and the sampling procedure
employed.
(b) A log of the
operating conditions of the process tested and any associated air pollution
control device.
(c) A summary of
results expressed in units consistent with the emission limitation applicable
to the source.
(d) Sample
calculations employing all the formulas used to calculate the
results.
(e) The field and
laboratory data for each repetition of the test.
(f) Calibration data for the components of
the sampling train used.
(g) The
results of quality assurance audit sample analyses required in the reference
method.
(h) The report of any
visible emission evaluations performed by the tester or source owner or
operator.
(i) A copy of any steam,
opacity or airflow charts made during the test.
(j) The report of any fuel analysis performed
on the fuel burned during the test.
(k) Documentation of any process upset
occurring during the test.
(l) An
explanation of any excessive variation in the results when comparing the
repetitions of the compliance emission test.
(m) If the compliance emission test being
conducted is a retest, the changes made to the process or control device since
the last test.
(10)
REPORTING OF TEST RESULTS FOR TESTS CONDUCTED BY THE DEPARTMENT. The department
shall furnish a report of emission tests it conducts to the source owner or
operator within 60 days after the testing is completed. This emission test
report shall include, but need not be limited to, the following information:
(a) A summary of results expressed in units
consistent with the emission limitation applicable to the source.
(b) Sample calculations employing all
formulas used to calculate the results.
(c) The field and laboratory data for each
repetition of the test.
(d)
Calibration data for the components of the sampling train used.
(e) The results of quality assurance audit
sample analyses required in the reference method.
(f) The report of any visible emission
evaluations performed by the department.
(g) The report of any fuel analysis performed
on the fuel burned during the test.