Current through Register Vol. 48, No. 9, September 27, 2024
(a) Industrial
sludge -Class A
(1) The requirement in
section504.32(a)(2)(a)(2) and the requirements in either
section504.32(a)(3)(a)(3), section504.32(a)(4)(a)(4),
section504.32(a)(5)(a)(5), section504.32(a)(6)(a)(6),
section504.32(a)(7)(a)(7), or section504.32(a)(8)(a)(8) shall be met for an
industrial sludge to be classified Class A with respect to pathogens if
pathogens are expected to be present.
(2) When pathogens are expected to be present
and the industrial sludge is expected to attract vectors, the Class A pathogen
requirements in section504.32(a)(3)(a)(3) through section504.32(a)(8)(a)(8)
shall be met either prior to meeting or at the same time the vector attraction
reduction requirements in section504.33, except the vector attraction reduction
requirements in section504.33(b)(6)(b)(6) through section504.33(b)(8)(b)(8),
are met.
(3) Class A -Alternative 1
(Not available for composting).
(i) Either
the density of fecal coliform in the industrial sludge shall be less than 1000
Most Probable Number per gram of total solids (dry weight basis), or the
density of Salmonella sp. bacteria in the industrial sludge shall be less than
three Most Probable Number per four grams of total solids (dry weight basis) at
the time the industrial sludge is used or disposed; at the time the industrial
sludge is prepared for sale or give away in a bag or other container for
application to the land; or at the time the industrial sludge or material
derived from industrial sludge is prepared to meet the requirements in
section504.10(b)(b), section504.10(e)(e), or section504.10(f)(f).
(ii) The temperature of the industrial sludge
that is used or disposed shall be maintained at a specific value for a period
of time.
(A) When the percent solids of the
industrial sludge is seven percent or higher, the temperature of the industrial
sludge shall be 50 degrees Celsius or higher; the time period shall be 20
minutes or longer; and the temperature and time period shall be determined
using equation (2), except when small particles of industrial sludge are heated
by either warmed gases or an immiscible liquid.
D = 131,700,000 (Equation 2)
-----------
100.1400t
Where,
D = time in days.
t = temperature in degrees Celsius.
TABLE 1 OF Section 504.32--If the industrial
sludge is 7% solids or higher.
|
Temperature (Celsius)
|
Time
|
50.0 (minimum)
|
13.17 days
|
60.0
|
12 hours 43 minutes
|
65.0
|
2 hours 39 minutes
|
70.0
|
30 minutes
|
71.3
|
20 minutes (minimum)
|
(B) When the percent solids of the industrial
sludge is seven percent or higher and small particles of industrial sludge are
heated by either warmed gases or an immiscible liquid, the temperature of the
industrial sludge shall be 50 degrees Celsius or higher; the time period shall
be 15 seconds or longer; and the temperature and time period shall be
determined using equation (2).
TABLE 2 OF Section 504.32 If the industrial
sludge is 7% solids or higher and small particles of industrial sludge are
heated by warm gases or an immiscible liquid. |
Temperature (Celsius)
|
Time
|
50.0 (minimum)
|
13.17 days
|
65.0
|
2 hours 39 minutes
|
71.3
|
20 minutes
|
80.0
|
1 minute 12 seconds
|
84.9
|
15 seconds (minimum)
|
(C) When the percent solids of the industrial
sludge is less than seven percent and the time period is at least 15 seconds,
but less than 30 minutes, the temperature and time period shall be determined
using equation (2).
TABLE 3 OF Section 504.32--If the industrial
sludge is less than 7% solids and the time period is at least 15 seconds, but
less than 30 minutes.
|
Temperature (Celsius)
|
Time
|
70.0
|
30 minutes (Maximum time. See (D) for greater
than 30 minutes)
|
71.3
|
20 minutes
|
75.0
|
6 minutes
|
80.0
|
1 minute 12 seconds
|
84.9
|
15 seconds (minimum)
|
(D) When the percent solids of the industrial
sludge is less than seven percent; the temperature of the industrial sludge is
50 degrees Celsius or higher; and the time period is 30 minutes or longer, the
temperature and time period shall be determined using equation (3).
D = 50,070,000 (Equation 3)
-----------
100.1400t
Where,
D = time in days.
t = temperature in degrees Celsius.
TABLE 4 OF Section 504.32--If the industrial
sludge is less than 7% solids an the temperature of the industrial sludge is 50
degrees Celsius or higher; and the time period is 30 minutes or longer.
|
Temperature (Celsius)
|
Time
|
50.0 (minimum)
|
5.0 days
|
55.0
|
1.0 day
|
60.0
|
4 hours 48 minutes
|
65.0
|
58 minutes
|
67.0
|
30 minutes (minimum)
|
(iii) The temperature used in equation (2)
and equation (3) will be the lowest, continuously measured temperature within
the reaction vessel during a 24-hour period or the lowest measured temperature
during any 24-hour period, if a continuous treatment process is used. If a
batch treatment process is used, the temperature used in the equation (2) and
equation (3) will be the lowest temperature measured during the batch
treatment.
(iv) For design
temperatures measuring greater than 70 degrees Celsius, continuous temperature
monitoring shall be required.
(4) Class A -Alternative 2
(i) Either the density of fecal coliform in
the industrial sludge shall be less than 1000 Most Probable Number per gram of
total solids (dry weight basis), or the density of Salmonella sp. bacteria in
the industrial sludge shall be less than three Most Probable Number per four
grams of total solids (dry weight basis) at the time the industrial sludge is
used or disposed; at the time the industrial sludge is prepared for sale or
give away in a bag or other container for application to the land; or at the
time the industrial sludge or material derived from industrial sludge is
prepared to meet the requirements in section504.10(b)(b), section504.10(e)(e),
or section504.10(f)(f).
(ii)
(A) The pH of the industrial sludge that is
used or disposed shall be raised to above 12 and shall remain above 12 for 72
hours.
(B) The temperature of the
industrial sludge shall be above 52 degrees Celsius for 12 hours or longer
during the period that the pH of the industrial sludge is above 12.
(C) At the end of the 72 hour period during
which the pH of the industrial sludge is above 12, the industrial sludge shall
be air dried to achieve a percent solids in the industrial sludge greater than
50 percent.
(5) Class A -Alternative 3
(i) Either the density of fecal coliform in
the industrial sludge shall be less than 1000 Most Probable Number per gram of
total solids (dry weight basis), or the density of Salmonella sp. bacteria in
industrial sludge shall be less than three Most Probable Number per four grams
of total solids (dry weight basis) at the time the industrial sludge is used or
disposed; at the time the industrial sludge is prepared for sale or give away
in a bag or other container for application to the land; or at the time the
industrial sludge or material derived from industrial sludge is prepared to
meet the requirements in section504.10(b)(b), section504.10(e)(e), or
section504.10(f)(f).
(ii)
(A) The industrial sludge shall be analyzed
prior to pathogen treatment to determine whether the industrial sludge contains
enteric viruses.
(B) When the
density of enteric viruses in the industrial sludge prior to pathogen treatment
is less than one Plaque-forming Unit per four grams of total solids (dry weight
basis), the industrial sludge is Class A with respect to enteric viruses until
the next monitoring episode for the industrial sludge.
(C) When the density of enteric viruses in
the industrial sludge prior to pathogen treatment is equal to or greater than
one Plaque-forming Unit per four grams of total solids (dry weight basis), the
industrial sludge is Class A with respect to enteric viruses when the density
of enteric viruses in the industrial sludge after pathogen treatment is less
than one Plaque-forming Unit per four grams of total solids (dry weight basis)
and when the values or ranges of values for the operating parameters for the
pathogen treatment process that produces the industrial sludge that meets the
enteric virus density requirement are documented.
(D) After the enteric virus reduction in
paragraph (a)(5)(ii)(C) of this subsection is demonstrated for the pathogen
treatment process, the industrial sludge continues to be Class A with respect
to enteric viruses when the values for the pathogen treatment process operating
parameters are consistent with the values or ranges of values documented in
paragraph (a)(5)(ii)(C) of this subsection.
(iii)
(A)
The industrial sludge shall be analyzed prior to pathogen treatment to
determine whether the industrial sludge contains viable helminth ova.
(B) When the density of viable helminth ova
in the industrial sludge prior to pathogen treatment is less than one per four
grams of total solids (dry weight basis), the industrial sludge is Class A with
respect to viable helminth ova until the next monitoring episode for the
industrial sludge.
(C) When the
density of viable helminth ova in the industrial sludge prior to pathogen
treatment is equal to or greater than one per four grams of total solids (dry
weight basis), the industrial sludge is Class A with respect to viable helminth
ova when the density of viable helminth ova in the industrial sludge after
pathogen treatment is less than one per four grams of total solids (dry weight
basis) and when the values or ranges of values for the operating parameters for
the pathogen treatment process that produces the industrial sludge that meets
the viable helminth ova density requirement are documented.
(D) After the viable helminth ova reduction
in paragraph (a)(5)(iii)(C) of this subsection is demonstrated for the pathogen
treatment process, the industrial sludge continues to be Class A with respect
to viable helminth ova when the values for the pathogen treatment process
operating parameters are consistent with the values or ranges of values
documented in paragraph (a)(5)(iii)(C) of this subsection.
(6) Class A -Alternative 4
(i) Either the density of fecal coliform in
the industrial sludge shall be less than 1000 Most Probable Number per gram of
total solids (dry weight basis), or the density of Salmonella sp. bacteria in
the industrial sludge shall be less than three Most Probable Number per four
grams of total solids (dry weight basis) at the time the industrial sludge is
used or disposed; at the time the industrial sludge is prepared for sale or
give away in a bag or other container for application to the land; or at the
time the industrial sludge or material derived from industrial sludge is
prepared to meet the requirements in section504.10(b)(b), section504.10(e)(e),
or section504.10(f)(f).
(ii) The
density of enteric viruses in the industrial sludge shall be less than one
Plaque-forming Unit per four grams of total solids (dry weight basis) at the
time the industrial sludge is used or disposed; at the time the industrial
sludge is prepared for sale or give away in a bag or other container for
application to the land; or at the time the industrial sludge or material
derived from industrial sludge is prepared to meet the requirements in
section504.10(b)(b), section504.10(e)(e), or section504.10(f)(f), unless
otherwise specified by the Department.
(iii) The density of viable helminth ova in
the industrial sludge shall be less than one per four grams of total solids
(dry weight basis) at the time the industrial sludge is used or disposed; at
the time the industrial sludge is prepared for sale or give away in a bag or
other container for application to the land; or at the time the industrial
sludge or material derived from industrial sludge is prepared to meet the
requirements in section504.10(b)(b), section504.10(e)(e), or
section504.10(f)(f), unless otherwise specified by the Department.
(7) Class A -Alternative 5
(i) Either the density of fecal coliform in
the industrial sludge shall be less than 1000 Most Probable Number per gram of
total solids (dry weight basis), or the density of Salmonella, sp. bacteria in
the industrial sludge shall be less than three Most Probable Number per four
grams of total solids (dry weight basis) at the time the industrial sludge is
used or disposed; at the time the industrial sludge is prepared for sale or
give away in a bag or other container for application to the land; or at the
time the industrial sludge or material derived from industrial sludge is
prepared to meet the requirements in section504.10(b)(b), section504.10(e)(e),
or section504.10(f)(f).
(ii)
Industrial sludge that is used or disposed shall be treated in one of the
Processes to Further Reduce Pathogens described in appendix B of this part if
pathogens are expected to be present.
(8) Class A -Alternative 6
(i) Either the density of fecal coliform in
the industrial sludge shall be less than 1000 Most Probable Number per gram of
total solids (dry weight basis), or the density of Salmonella, sp. bacteria in
the industrial sludge shall be less than three Most Probable Number per four
grams of total solids (dry weight basis) at the time the industrial sludge is
used or disposed; at the time the industrial sludge is prepared for sale or
give away in a bag or other container for application to the land; or at the
time the industrial sludge or material derived from industrial sludge is
prepared to meet the requirements in section504.10(b)(b), section504.10(e)(e),
or section504.10(f)(f).
(ii)
Industrial sludge that is used or disposed shall be treated in a process that
is equivalent to a Process to Further Reduce Pathogens, as determined by the
Department.
(b) Industrial sludge -Class B
(1)
(i) The
requirements in either section504.32(b)(2)(b)(2), section504.32(b)(3)(b)(3), or
section504.32(b)(4)(b)(4) shall be met for an industrial sludge to be
classified Class B with respect to pathogens if pathogens are expected to be
present.
(ii) The site restrictions
in section504.32(b)(5)(b)(5) shall be met when industrial sludge that meets the
Class B pathogen requirements in section504.32(b)(2)(b)(2),
section504.32(b)(3)(b)(3), or section504.32(b)(4)(b)(4) is applied to the
land.
(2) Class B
-Alternative 1
(i) Seven representative
samples of the industrial sludge shall be collected at the time the industrial
sludge is used or disposed.
(ii)
The geometric mean of the density of fecal coliform in the samples collected in
(b)(2)(i) of this subsection shall be less than either 2,000,000 Most Probable
Number per gram of total solids (dry weight basis) or 2,000,000 Colony Forming
Units per gram of total solids (dry weight basis).
(3) Class B -Alternative 2. Industrial sludge
that is used or disposed shall be treated in one of the Processes to
Significantly Reduce Pathogens described in appendix B of this part.
(4) Class B -Alternative 3. Industrial sludge
that is used or disposed shall be treated in a process that is equivalent to a
Process to Significantly Reduce Pathogens, as determined by the
Department.
(5) Site Restrictions
(i) Food crops with harvested parts that
touch the industrial sludge/soil mixture and are totally above the land surface
shall not be harvested for 14 months after application of industrial
sludge.
(ii) Food crops with
harvested parts below the surface of the land shall not be harvested for 20
months after application of industrial sludge when the industrial sludge
remains on the land surface for four months or longer prior to incorporation
into the soil.
(iii) Food crops
with harvested parts below the surface of the land shall not be harvested for
38 months after application of industrial sludge when the industrial sludge
remains on the land surface for less than four months prior to incorporation
into the soil.
(iv) Food crops,
feed crops, and fiber crops shall not be harvested for 30 days after
application of industrial sludge.
(v) Animals shall not be grazed on the land
for 30 days after application of industrial sludge.
(vi) Turf grown on land where industrial
sludge is applied shall not be harvested for one year after application of the
industrial sludge when the harvested turf is placed on either land with a high
potential for public exposure or a lawn, unless otherwise specified by the
Department.
(vii) Public access to
land with a high potential for public exposure shall be restricted for one year
after application of industrial sludge.
(viii) Public access to land with a low
potential for public exposure shall be restricted for 30 days after application
of industrial sludge.
(ix) The
Department may establish in permits the required application buffer setbacks
for property boundaries, roadways, residential developments, dwellings, water
wells, drainageways, and surface water as deemed necessary to protect public
health.
(x) The Department may
establish minimum requirements in permits for soil and/or groundwater
monitoring, for bulk application sites, to verify compliance with the
Regulation.