Current through Register Vol. 48, No. 9, September 27, 2024
2.7.1 Licensing the Manufacture and the
Distribution of Devices to Persons Generally Licensed under RHA 2.4.2.
2.7.1.1 An application for a specific license to
manufacture or distribute devices containing radioactive material, excluding special
nuclear material, to persons generally licensed under RHA 2.4.2 or equivalent
regulations of the U.S. Nuclear Regulatory Commission, an Agreement State, or a
Licensing State will be approved if:
2.7.1.1.1 the
applicant satisfies the general requirements of
RHA 2.6;
2.7.1.1.2 the applicant submits sufficient
information relating to the design, manufacture, prototype testing, quality control,
labels, proposed uses, installation, servicing, leak testing, operating and safety
instructions, and potential hazards of the device to provide reasonable assurance
that:
2.7.1.1.2.1 the device can be safely
operated by persons not having training in radiological protection;
2.7.1.1.2.2 Under ordinary conditions of handling,
storage, and use of the device, the radioactive material contained in the device
will not be released or inadvertently removed from the device, and it is unlikely
that any person will receive in one year a dose in excess of 10% of the annual
limits specified in RHA 3.5.1; and
2.7.1.1.2.3 under accident conditions (such as
fire and explosion) associated with handling, storage, and the use of the device, it
is unlikely that any person would receive an external radiation dose or dose
commitment in excess of the following organ doses: Whole body: 15 rems head and
trunk; active bloodforming organs; gonads; or lens of eye: Hands and forearms; 200
rems feet and ankles; localized areas of skin averaged over areas no larger than 1
square centimeter. Other organs 50 rems.
2.7.1.1.3 Each device bears a durable, legible,
clearly visible label or labels approved by the Department, which contain in a
clearly identified and separate statement:
2.7.1.1.3.1 instructions and precautions necessary
to assure safe installation, operation, and servicing of the device (documents such
as operating and service manuals may be identified in the label and used to provide
this information);
2.7.1.1.3.2 the
requirement, or lack of requirement, for leak testing, or for testing any on-off
mechanism and indicator, including the maximum time interval for such testing, and
the identification of radioactive material by isotope, quantity of radioactivity,
and date of determination of the quantity; and
2.7.1.1.3.3 The information called for in the
following statement in the same or substantially similar form:
Receipt, possession, use, and transfer of this device
Model3*, Serial No
3*, containing (Identity and quantity of
radioactive material) are subject to a general license or the equivalent and the
regulations of the U.S. Nuclear Regulatory Commission, an Agreement State, or a
Licensing State. This label shall be maintained on the device in a legible
condition. Removal of this label is prohibited.
CAUTION-RADIOACTIVE MATERIAL
_______________________________________________
(Name of manufacturer or initial
transferor)3*
2.7.1.1.4 Each device having a separable source
housing that provides the primary shielding for the source also bears, on the source
housing, a durable label containing the device model number and serial number, the
isotope and quantity, the words, "Caution-Radioactive Material," the radiation
symbol described in RHA 3.21, and the name of the manufacturer or initial
distributor.
2.7.1.1.5 Each device
meeting the criteria of RHA 2.4.2.3.11.1 bears a permanent (e.g., embossed, etched,
stamped, or engraved) label affixed to the source housing if separable, or the
device if the source housing is not separable, that includes the words,
"Caution-Radioactive Material," and, if practicable the radiation symbol described
in RHA 3.21.
2.7.1.1.6 The device has
been registered in the Sealed Source and Device Registry.
2.7.1.2 In the event the applicant desires that
the device be required to be tested at intervals longer than six months, either for
proper operation of the on-off mechanism and indicator, if any, or for leakage of
radioactive material or for both, he shall include in his application sufficient
information to demonstrate that such longer interval is justified by performance
characteristics of the device or similar devices and by design features which have a
significant bearing on the probability or consequences of leakage of radioactive
material from the device or failure of the on-off mechanism and indicator. In
determining the acceptable interval for the test for leakage of radioactive
material, the Department will consider information which includes, but is not
limited to:
2.7.1.2.1 primary containment (source
capsule);
2.7.1.2.2 protection of
primary containment;
2.7.1.2.3 method of
sealing containment;
2.7.1.2.4
containment construction materials;
2.7.1.2.5 form of contained radioactive
material;
2.7.1.2.6 maximum temperature
withstood during prototype test;
2.7.1.2.7 maximum pressure withstood during
prototype tests;
2.7.1.2.8 maximum
quantity of contained radioactive material;
2.7.1.2.9 radiotoxicity of contained radioactive
material; and
2.7.1.2.10 operating
experience with identical devices or similarly designed and constructed
devices.
2.7.1.3 In the event
the applicant desires that the general licensee under RHA 2.4.2, or under the
equivalent regulations of the U.S. Nuclear Regulatory Commission, an Agreement
State, or a Licensing State be authorized to install the device, collect the sample
to be analyzed by a specific licensee for leakage of radioactive material, service
the device, test the on-off mechanism and indicator, or remove the device from
installation, he shall include in his application written instructions to be
followed by the general licensee, estimated calendar quarter doses associated with
such activity or activities, and bases for such estimates. The submitted information
shall demonstrate that performance of such activity or activities by an individual
untrained in radiological protection, in addition to other handling, storage, and
use of devices under the general license, is unlikely to cause that individual to
receive a calendar quarter dose in excess of 10% of the limits specified in the
table in RHA 3.2.1.
2.7.1.4 If a device
containing radioactive material is to be transferred for use under the general
license contained in RHA 2.4.2 of this part, each person that is licensed under RHA
2.7.1 shall provide the information specified in this paragraph to each person to
whom a device is to be transferred. This information must be provided before the
device may be transferred. In the case of a transfer through an intermediate person,
the information must also be provided to the intended user prior to initial transfer
to the intermediate person. The required information includes--
2.7.1.4.1 A copy of the general license contained
in RHA 2.4.2; if RHA 2.4.2.3.2 through 2.4.2.3.4 or RHA 2.4.2.3.11 do not apply to
the particular device, those paragraphs may be omitted.
2.7.1.4.2 A copy of RHA 2.4.1, 2.18, 3.44, and
3.45 of this part;
2.7.1.4.3 A list of
the services that can only be performed by a specific licensee;
2.7.1.4.4 Information on acceptable disposal
options including estimated costs of disposal; and
2.7.1.4.5 An indication that the Department's
policy is to issue high civil penalties for improper disposal.
2.7.1.5 If radioactive material is to be
transferred in a device for use under an equivalent general license of the NRC or an
Agreement State, each person that is licensed under RHA 2.7.1 shall provide the
information specified in this paragraph to each person to whom a device is to be
transferred. This information must be provided before the device may be transferred.
In the case of a transfer through an intermediate person, the information must also
be provided to the intended user prior to initial transfer to the intermediate
person. The required information includes--
2.7.1.5.1 A copy of the NRC or Agreement State or
regulations equivalent to RHA 2.4.1, 2.4.2, 2.18, 3.44 and 3.45 of this part or a
copy of these Agreement State regulations. If a copy of the Department's regulations
is provided to a prospective general licensee in lieu of the NRC regulations, it
shall be accompanied by a note explaining that use of the device is regulated by the
NRC or other Agreement State; if certain paragraphs of the regulations do not apply
to the particular device, those paragraphs may be omitted.
2.7.1.5.2 A list of the services that can only be
performed by a specific licensee;
2.7.1.5.3 Information on acceptable disposal
options including estimated costs of disposal; and
2.7.1.5.4 The name or title, address, and phone
number of the contact at the appropriate regulatory agency, NRC or Agreement State,
having jurisdiction at the devices new location, from which additional information
may be obtained.
2.7.1.6 An
alternative approach to informing customers may be proposed by the licensee for
approval by the Department.
2.7.1.7
Each device that is transferred after February 2004 must meet the labeling
requirements in RHA 2.7.1.4.3 through 2.7.1.4.5.
2.7.1.8 If a notification of bankruptcy has been
made under RHA 2.10.6 or the license is to be terminated, each person licensed under
RHA 2.7.1 shall provide, upon request, to the Department and to the appropriate
regulatory agency, NRC or Agreement State, having jurisdiction at the devices new
location, records of final disposition required under RHA 2.7.1.9.2.
2.7.1.9 Each person licensed under RHA 2.7.1 to
initially transfer devices to generally licensed persons shall comply with the
requirements of this section.
2.7.1.9.1 The person
shall report all transfers of devices to persons for use under the general license
in RHA 2.4.2 of these regulations and for use under equivalent NRC regulations (
10
CFR 31.5) or other Agreement State's regulations
and all receipts of devices from persons licensed under RHA 2.4.2 to the Department
or to the appropriate NRC office or other Agreement State office. The report must be
submitted on a quarterly basis on NRC Form 653--"Transfers of Industrial Devices
Report" or in a clear and legible report containing all of the data required by the
form. (NRC Form 653 may be obtained from the Department or found in NUREG-1556, Vol.
16.)
2.7.1.9.1.1 The required information for
transfers to general licensees includes--
(i) The
identity of each general licensee by name and mailing address for the location of
use; if there is no mailing address for the location of use, an alternate address
for the general licensee shall be submitted along with information on the actual
location of use.
(ii) The name, title,
and phone number of the person identified by the general licensee as having
knowledge of and authority to take required actions to ensure compliance with the
appropriate regulations and requirements;
(iii) The date of transfer;
(iv) The type, model number, and serial number of
the device transferred; and
(v) The
quantity and type of radioactive material contained in the
device.
2.7.1.9.1.2 If one or
more intermediate persons will temporarily possess the device at the intended place
of use before its possession by the user, the report must include the same
information for both the intended user and each intermediate person, and clearly
designate the intermediate person(s).
2.7.1.9.1.3 For devices received from a general
licensee, the report must include the identity of the general licensee by name and
address, the type, model number, and serial number of the device received, the date
of receipt, and, in the case of devices not initially transferred by the reporting
licensee, the name of the manufacturer or initial transferor.
2.7.1.9.1.4 If the licensee makes changes to a
device possessed by a general licensee, such that the label must be changed to
update required information, the report must identify the general licensee, the
device, and the changes to information on the device label.
2.7.1.9.1.5 The report must cover each calendar
quarter, must be filed within 30 days of the end of the calendar quarter, and must
clearly indicate the period covered by the report.
2.7.1.9.1.6 The report must clearly identify the
specific licensee submitting the report and include the license number of the
specific licensee.
2.7.1.9.1.7 If no
transfers have been made to or from persons generally licensed under RHA 2.4.2
during the reporting period, the report must so indicate. If no transfers have been
made to or from an NRC or other Agreement State during the reporting period, this
information should be made available to the responsible agency upon their
request.
2.7.1.9.2 The person
shall maintain all information concerning transfers and receipts of devices that
supports the reports required by this section. Records required by this paragraph
must be maintained for a period of 3 years following the date of the recorded event.
2.7.2 Licensing the
Introduction of Radioactive Material Into Products in Exempt Concentration
In addition to the requirements set forth in
RHA 2.6, a specific license
authorizing the introduction of radioactive material into a product or material
owned by or in the possession of a licensee or another to be transferred to persons
exempt under 2.20.2.1.1 will be issued only if:
2.7.2.1 The applicant submits a description of the
product or material into which the radioactive material will be introduced, intended
use of the radioactive material and the product or material into which it is
introduced, method of introduction, initial concentration of the radioactive
material in the product or material, control methods to assure that no more than the
specified concentration is introduced into the product or material, estimated time
interval between introduction and transfer of the radioactive material in the
product or material at the time of transfer; and
2.7.2.2 The applicant provides reasonable
assurance that the concentrations of radioactive material at the time of transfer
will not exceed the concentrations in
RHA
2.25 Schedule C, that reconcentration of the radioactive
material in concentrations exceeding those in
RHA
2.25 Schedule C is not likely, that use of lower
concentrations is not feasible, and that the product or material is not likely to be
incorporated in any food, beverage, cosmetic, drug, or other commodity or product
designed for ingestion or inhalation by, or application to, a human being. Each
person licensed under this section 2.7.2 shall file an annual report with the
Department which shall identify the type and quantity of each product or material
into which radioactive material has been introduced during the reporting period;
name and address of the person who owned or possessed the product or material, into
which radioactive material has been introduced, at the time of introduction; the
type and quantity of radionuclide introduced into each such product or material; and
the initial concentrations of the radionuclide in the product or material at time of
transfer of the radioactive material by the licensee. If no transfers of radioactive
material have been made pursuant to this section 2.7.2 during the reporting period,
the report shall so indicate. The report shall cover the year ending June 30, and
shall be filed within 30 days thereafter.
2.7.3 Manufacture and Distribution of Radioactive
Materials for Medical Use Under General License.
In addition to the requirements set forth in
RHA 2.6 above, a specific license
authorizing the distribution of radioactive material for use by physicians under the
general license of 2.4.6 will be issued only if:
2.7.3.1 The applicant submits evidence that the
radioactive material is to be manufactured, labeled and packaged in accordance with
a new drug application Administration has approved, or in accordance with a license
for a biologic product issued by the Secretary, Department of Health, Education, and
Welfare; and,
2.7.3.2 The following
statement, or a substantially similar statement which contains information called
for in the following statement, appears on the label affixed to the container or
appears in the leaflet or brochure which accompanies the package: "This radioactive
drug may be received, possessed, and used only by physicians licensed to dispense
drugs in the practice of medicine. Its receipt, possession, use and transfer are
subject to the regulations and a general license (or the equivalent) of the U.S.
Nuclear Regulatory Commission, an Agreement State, or a Licensing State."
__________
(Name of Manufacturer)
2.7.4 Manufacture and Distribution of Radioactive
Materials for Certain In Vitro Clinical, or Laboratory Testing Under General License
An application for a specific license to manufacture or distribute
radioactive material for use under the general license of 2.4.3 of this part will be
applied if:
2.7.4.1 The applicant satisfies
the general requirements specified in
RHA 2.6.
2.7.4.1.1 Has specialized training in the
diagnostic or therapeutic use of the sealed source considered or has experience
equivalent to such training, and
2.7.4.1.2 Is a physician.
2.7.4.2 The radioactive material is to be prepared
for distribution in prepackaged units of:
2.7.4.2.1 Iodine-125 in units not exceeding 10
microcuries each.
2.7.4.2.2 Iodine-131
in units not exceeding 10 microcuries each.
2.7.4.2.3 Carbon-14 in units not exceeding 10
microcuries each.
2.7.4.2.4 Hydrogen-3
(tritium) in units not exceeding 50 microcuries each.
2.7.4.2.5 Iron-59 in units not exceeding 20
microcuries each.
2.7.4.2.6 Cobalt-57 in
units not exceeding 10 microcuries (0.37 MBq) each.
2.7.4.2.7 Selenium-75 in units not exceeding 10
microcuries each.
2.7.4.2.8 Mock
Iodine-125 in units not exceeding 0.05 microcuries of Iodine 129 and 0.005
microcuries of Americium 241 each.
2.7.4.3 Each prepackage unit bears a durable,
clearly visible label:
2.7.4.3.1 Identifying the
radioactive contents as to chemical form and radionuclide, and indicating that the
amount of radioactivity does not exceed 10 microcuries (0.37 MBq) of Iodine-125,
Iodine-131, Selenium-75, or Carbon-14; 50 microcuries (1.85 MBq) of Hydrogen-3
(tritium); or 20 microcuries (0.74 MBq) of Iron-59; or Mock Iodine-125 in units not
exceeding 0.05 microcurie (1.85 kBq) of Iodine-129 and 0.005 microcurie (0.185 kBq)
of Americium-241 each; or Cobalt-57 in units not exceeding 10 microcuries (0.37
MBq); and
2.7.4.3.2 Displaying the
radiation caution symbol described in RHA 3.8 (3.8.1) of Part III and the words,
"CAUTION, RADIOACTIVE MATERIAL," and "Not for Internal or External Use in Humans or
Animals."
2.7.4.4 The following
statement, or substantially similar statement which contains the information called
for in the following statement, appears on a label affixed to each prepackaged unit
or appears in a leaflet or brochure which accompanies the package.
"This radioactive material may be received, acquired, possessed,
and used only by physicians, veterinarians in the practice of veterinary medicine,
clinical laboratories, or hospitals and only for In Vitro clinical or laboratory
tests not involving internal or external administration of the material, or the
radiation therefrom, to human beings or animals. Its receipt, acquisition,
possession, use and transfer are subject to the regulations and a general license of
the United States Nuclear Regulatory Commission, an Agreement State, or a licensing
State."
__________
Name of Manufacturer
2.7.4.5 The label affixed to the unit, or the
leaflet or brochure which accompanies the package, contains adequate information as
to the precautions to be observed in handling and storing such radioactive material.
In the case of the Mock Iodine-125 reference or calibration source, the information
accompanying the source must also contain directions to the licensee regarding the
waste disposal requirements set out in RHA 3.12.
2.7.5 Manufacture, preparation, or transfer for
commercial distribution of radioactive drugs containing radioactive material for
medical use under Part IV.
2.7.5.1 An application
for a specific license to manufacture, prepare, or transfer for commercial
distribution radioactive drugs containing radioactive material for use by persons
licensed pursuant to Part IV of these regulations will be approved if:
2.7.5.1.1 The applicant satisfies the general
requirements specified in
RHA 2.6;
2.7.5.1.2 The applicant submits evidence that the
applicant is at least one of the following:
2.7.5.1.2.1 Registered with the U.S. Food and Drug
Administration (FDA) as the owner or operator of a drug establishment that engages
in the manufacture, preparation, propagation, compounding, or processing of a drug
under 21 CFR 207.20(a);
2.7.5.1.2.3
Licensed as a pharmacy by a State Board of Pharmacy;
2.7.5.1.2.4 Operating as a nuclear pharmacy within
a Federal medical institution; or
2.7.5.1.2.5 A Positron Emission Tomography (PET)
drug production facility registered with a State agency.
2.7.5.1.3 The applicant submits information on the
radionuclide; the chemical and physical form; the maximum activity per vial,
syringe, generator, or other container of the radioactive drug; and the shielding
provided by the packaging to show it is appropriate for the safe handling and
storage of the radioactive drugs by medical use licensees; and
2.7.5.1.4 The applicant commits to the following
labeling requirements:
2.7.5.1.4.1 A label is
affixed to each transport radiation shield, whether it is constructed of lead glass,
plastic, or other material, of a radioactive drug to be transferred for commercial
distribution. The label must include the radiation symbol and the words "CAUTION,
RADIOACTIVE MATERIAL" or "DANGER, RADIOACTIVE MATERIAL"; the name of the radioactive
drug or its abbreviation; and the quantity of radioactivity at a specified date and
time. For radioactive drugs with a half life greater than 100 days, the time may be
omitted.
2.7.5.1.4.2 A label is affixed
to each syringe, vial, or other container used to hold a radioactive drug to be
transferred for commercial distribution. The label must include the radiation symbol
and the words "CAUTION, RADIOACTIVE MATERIAL" or "DANGER RADIOACTIVE MATERIAL" and
an identifier that ensures that the syringe, vial, or other container can be
correlated with the information on the transport radiation shield
label.
2.7.5.2 A
licensee described by paragraph 2.7.5.1.2.3 or 2.7.5.1.2.4 of this section:
2.7.5.2.1 May prepare radioactive drugs for
medical use, as defined in RHA 4.2 provided that the radioactive drug is prepared by
either an authorized nuclear pharmacist, as specified in 2.7.5.2.2 and 2.7.5.2.4 of
this section, or an individual under the supervision of an authorized nuclear
pharmacist as specified in RHA 4.15.
2.7.5.2.2 May allow a pharmacist to work as an
authorized nuclear pharmacist if:
2.7.5.2.2.1 This
individual qualifies as an authorized nuclear pharmacist as defined in RHA
4.2.
2.7.5.2.2.2 This individual meets
the requirements specified in Part 4 of this Regulation, and the licensee has
received an approved license amendment identifying this individual as an authorized
nuclear pharmacist; or
2.7.5.2.2.3 This
individual is designated as an authorized nuclear pharmacist in accordance with
2.7.5.2.4 of this section.
2.7.5.2.3 The actions authorized in 2.7.5.2.1 and
2.7.5.2.2 of this section are permitted in spite of more restrictive language in
license conditions.
2.7.5.2.4 May
designate a pharmacist (as defined in RHA 4.2) as an authorized nuclear pharmacist
if:
2.7.5.2.4.1 The individual was a nuclear
pharmacist preparing only radioactive drugs containing accelerator-produced
radioactive material; and
2.7.5.2.4.2
The individual practiced at a pharmacy at a Government agency or Federally
recognized Indian Tribe before November 30, 2007 or at all other pharmacies before
August 8, 2009, or an earlier date as noticed by the NRC.
2.7.5.2.5 Shall provide to the Department:
2.7.5.2.5.1 A copy of each individual's
certification by a specialty board whose certification process has been recognized
by the Nuclear Regulatory Commission or an Agreement State as specified in RHA
4.22.1; or
2.7.5.2.5.2 The Commission or
Agreement State license; or
2.7.5.2.5.3
Commission master materials licensee permit; or
2.7.5.2.5.4 The permit issued by a licensee or
Commission master materials permittee of broad scope or the authorization from a
commercial nuclear pharmacy authorized to list its own authorized nuclear
pharmacist; or
2.7.5.2.5.5 Documentation
that only accelerator-produced radioactive materials were used in the practice of
nuclear pharmacy at a Government agency or Federally recognized Indian Tribe before
November 30, 2007 or at all other locations of use before August 8, 2009, or an
earlier date as noticed by the NRC; and
2.7.5.2.5.6 A copy of the State pharmacy licensure
or registration, no later than 30 days after the date that the licensee allows,
under paragraphs RHA 2.7.5.2.2.1 and 2.7.5.2.2.3, the individual to work as an
authorized nuclear pharmacist.
2.7.5.3 A licensee shall possess and use
instrumentation to measure the radioactivity of radioactive drugs. The licensee
shall have procedures for use of the instrumentation. The licensee shall measure, by
direct measurement or by combination of measurements and calculations, the amount of
radioactivity in dosages of alpha-, beta-, or photon-emitting radioactive drugs
prior to transfer for commercial distribution. In addition, the licensee shall:
2.7.5.3.1 Perform tests before initial use,
periodically, and following repair, on each instrument for accuracy, linearity, and
geometry dependence, as appropriate for the use of the instrument; and make
adjustments when necessary; and
2.7.5.3.2 Check each instrument for constancy and
proper operation at the beginning of each day of use.
2.7.5.4 A licensee shall satisfy the labeling
requirements in paragraph 2.7.5.1.4 of this section.
2.7.5.5 Nothing in this section relieves the
licensee from complying with applicable FDA, other Federal, and State requirements
governing radioactive drugs.
2.7.7 Manufacture and Distribution of Sources or
Devices Containing Radioactive Material for Medical Use
2.7.7.1 An application for a specific license to
manufacture and distribute sources and devices containing radioactive material to
persons licensed pursuant to Part IV of these regulations for use as a calibration,
transmission, or reference source or for the uses listed in RHA 4.46, 4.56, 4.58 and
4.88 of Part IV of these regulations will be approved if:
2.7.7.1.1 The applicant satisfies the general
requirements in
RHA 2.6 of this Part; and
2.7.7.1.2 The applicant submits sufficient
information regarding each type of source or device pertinent to an evaluation of
its radiation safety, including:
2.7.7.1.2.1 The
radioactive material contained, its chemical and physical form, and
amount;
2.7.7.1.2.2 Details of design
and construction of the source or device;
2.7.7.1.2.3 Procedures for, and results of,
prototype tests to demonstrate that the source or device will maintain its integrity
under stresses likely to be encountered in normal use and accidents;
2.7.7.1.2.4 For devices containing radioactive
material, the radiation profile of a prototype device;
2.7.7.1.2.5 Details of quality control procedures
to assure that production sources and devices meet the standards of design and
prototype tests;
2.7.7.1.2.6 Procedures
and standards for calibrating sources and devices;
2.7.7.1.2.7 Legend and methods for labeling
sources and devices as to their radioactive content;
2.7.7.1.2.8 Instruction for handling and storing
the source or device from the radiation safety standpoint; these instructions are to
be included on a durable label attached to a permanent storage container for the
source or device; provided, that instructions which are too lengthy for such label
may be summarized on the label and printed in detail on a brochure which is
referenced on the label;
2.7.7.1.3 The label affixed to the source or
device, or to the permanent storage container for the source or device, contains
information on the radionuclide, quantity, and date of assay, and a statement that
(insert name of source or device) is licensed by the Department for distribution to
persons licensed pursuant to RHA 4.28, RHA 4.46, 4.56 and 4.58 of Part IV of these
regulations or under equivalent licenses of the U.S. Nuclear Regulatory Commission,
an Agreement State, or a Licensing State.
2.7.7.1.4 The source or device has been registered
in the Sealed Source and Device Registry.
2.7.7.2 In the event the applicant desires that
the source or device be required to be tested for leakage of radioactive material at
intervals longer than six months, he shall include in his application sufficient
information to demonstrate that such longer interval is justified by performance
characteristics of the source or device or similar sources or devices and by design
features that have a significant bearing on the probability or consequences of
leakage of radioactive material from the source. In determining the acceptable
interval for test of leakage of radioactive material, the Department will consider
information that includes, but is not limited to:
2.7.7.2.1 Primary containment (source
capsule);
2.7.7.2.2 Protection of
primary containment;
2.7.7.2.3 Method of
sealing containment;
2.7.7.2.4
Containment construction materials;
2.7.7.2.5 Form of contained radioactive
material;
2.7.7.2.6 Maximum temperature
withstood during prototype tests;
2.7.7.2.7 Maximum pressure withstood during
prototype tests;
2.7.7.2.8 Maximum
quantity of contained radioactive material;
2.7.7.2.9 Radiotoxicity of contained radioactive
material; and
2.7.7.2.10 Operating
experience with identical sources or devices or similarly designed and constructed
sources or devices.
2.7.7.3 If
an application is filed pursuant to RHA 2.7.7.1 on or before August 9, 1977, for a
license to manufacture and distribute a source or device that was distributed
commercially on or before July 9, 1977, the applicant may continue the distribution
of such source or device to authorized licenses until the Department issues the
license or notifies the applicant otherwise.
2.7.8 Manufacture and distribution of radioactive
materials for medical use under general license. In addition to the requirements set
forth in
RHA 2.6 above, a specific license
authorizing the distribution of radioactive material for use by physicians under the
general license of 2.4.6 will be issued only if:
2.7.8.1 The applicant submits evidence that the
radioactive material is to be manufactured, labeled and packaged in accordance with
a new drug application which the Commissioner of Food and Drug Administration, has
approved, or in accordance with a license for a biologic product issued by the
Secretary, Department of Health, Education, and Welfare; and,
2.7.8.2 The following statement, or a
substantially similar statement which contains information called for in the
following statement, appears on the label affixed to the container or appears in the
leaflet or brochure which accompanies the package:
"This radioactive drug may be received, possessed, and used only
by physicians licensed to dispense drugs in the practice of medicine. Its receipt,
possession, use and transfer are subject to the regulations and a general license or
the equivalent of the U.S. Nuclear Regulatory Commission, an Agreement State, or a
Licensing State.
__________
(Name of Manufacturer)
2.7.9 Manufacture and Distribution of Radioactive
Materials for Certain in Vitro Clinical, or Laboratory Testing Under General
License. An application for a specific license to manufacture or distribute
radioactive material for use under the general license of 2.4.3 of this Part will be
approved if:
2.7.9.1 The applicant satisfies the
general requirements specified in
RHA 2.6.
2.7.9.2 The radioactive material is to be prepared
for distribution in prepackaged units of:
2.7.9.2.1 Iodine 125 in units not exceeding 10
microcuries each.
2.7.9.2.2 Iodine 131
in units not exceeding 10 microcuries each.
2.7.9.2.3 Carbon 14 in units not exceeding 10
microcuries each.
2.7.9.2.4 Hydrogen 3
(tritium) in units not exceeding 50 microcuries each.
2.7.9.2.5 Iron 59 in units not exceeding 20
microcuries each.
2.7.9.2.6 Cobalt-57 in
units not exceeding 10 microcuries each.
2.7.9.2.7 Selenium-75 in units not exceeding 10
microcuries each.
2.7.9.2.8 Mock
Iodine-125 in units not exceeding 0.05 microcuries of Iodine-129 and 0.005
microcuries of Americium-241 each.
2.7.9.3 Each prepackaged unit bears a durable,
clearly visible label:
2.7.9.3.1 Identifying the
radioactive contents as to chemical form and radionuclide, and indicating that the
amount of radioactivity does not exceed 10 microcuries of iodine-125, Iodine-131,
Carbon-14, Cobalt-57, Selenium-75; 50 microcuries of Hydrogen-3; 20 microcuries of
Iron-59; or Mock Iodine-125 in units not exceeding 0.05 microcurie of Iodine-129 and
0.005 microcurie of Americium-241 each; and
2.7.9.3.2 Displaying the radiation caution symbol
described in RHA 3.8 (3.8.1) of Part III and the words, "CAUTION, RADIOACTIVE
MATERIAL," and "Not for Internal or External Use in Humans or
Animals."
2.7.9.4 The
following statement, or a substantially similar statement which contains the
information called for in the following statement, appears on a label affixed to
each prepackaged unit or appears in a leaflet or brochure which accompanies the
package.
This radioactive material may be received, acquired, possessed,
and used only by physicians, veterinarians in the practice of veterinary medicine,
clinical laboratories, or hospitals and only for In Vitro clinical or laboratory
tests not involving internal or external administration of the material, or the
radiation therefrom, to human beings or animals. Its receipt, acquisition,
possession, use and transfer are subject to the regulations and a general license of
the United States Nuclear Regulatory Commission, an Agreement State, or a Licensing
State.
__________
Name of Manufacturer
2.7.9.5 The label affixed to the unit, or the
leaflet or brochure which accompanies the package, contains adequate information as
to the precautions to be observed in handling and storing such radioactive
material.
2.7.10 Manufacture
and Distribution of Radiopharmaceuticals Containing Radioactive Material for Medical
Use Under Group Licenses.
2.7.10.1 An application
for a specific license to manufacture and distribute radiopharmaceuticals containing
radioactive material for use by persons licensed pursuant to RHA 2.7.3 for the uses
listed in Group I, Group II, IV, or V of
RHA 2.26 Schedule D of this part
will be approved if:
2.7.10.1.1 The applicant
satisfies the general requirements specified in
RHA 2.6 of this part;
2.7.10.1.2 The applicant submits evidence that:
2.7.10.1.2.1 The radiopharmaceutical containing
radioactive material will be manufactured, labeled and packed in accordance with the
Federal Food, Drug and Cosmetic Act or the Public Health Service Act, such as a new
drug application (NDA) approved by the Food and Drug Administration (FDA), a
biologic product license issued by FDA or a "Notice of Claimed Investigational
Exemption for a New Drug" (IND) that has been accepted by the FDA; or
2.7.10.1.2.2 The manufacture and distribution of
the radiopharmaceutical containing radioactive material is not subject to the
Federal Food, Drug, and Cosmetic Act and the Public Health Service
Act.
2.7.10.1.3 The applicant
submits information on the radionuclide, chemical and physical form, packaging
including maximum activity per package, and shielding provided by the packaging of
the radioactive material which is appropriate for safe handling and storage of
radiopharmaceuticals by group licensees; and
2.7.10.1.4 The label affixed to each package of
the radiopharmaceutical contains information on the radionuclide, quantity, and date
of assay and the label affixed to each package, or the leaflet or brochure which
accompanies each package, contains a statement that the radiopharmaceutical is
licensed by the Department for distribution to persons licensed pursuant to RHA
2.7.3 and
RHA 2.26 Schedule D, Group I, Group
II, Group IV, and V of Part II, as appropriate, or under equivalent licenses of the
U.S. Nuclear Regulatory Commission, an Agreement State, or a Licensing State or that
an application for such license has been filed with the Department on or before
August 9, 1977 and is still pending.
The labels, leaflets, or brochures required by this paragraph are
in addition to the labeling required by the Food and Drug Administration (FDA) and
they may be separate from or, with the approval of FDA, may be combined with the
labeling required by FDA.
2.7.10.2 If an application is filed pursuant to
RHA 2.7.10.1 on or before [FN**] [Aug. 9, 1977], for a license to manufacture and
distribute a radiopharmaceutical that was distributed commercially on or before
[FN*] the applicant may continue the distribution of such radiopharmaceutical to
group licensees until the Department issues the license or notifies the applicant
otherwise.
2.7.11 Manufacture
and Distribution of Generators or Reagent Kits for Preparation of
Radiopharmaceuticals Containing Radioactive Material.
2.7.11.1 An application for a specific license to
manufacture and distribute generators or reagent kits containing radioactive
material for preparation of radiopharmaceuticals by persons licensed pursuant to RHA
2.7.3 for the uses listed in Group III of
RHA 2.26 Schedule D of this part
will be approved if:
2.7.11.1.1 The applicant
satisfies the general requirements specified in
RHA 2.6 of this part;
2.7.11.1.2 The applicant submits evidence that:
The generator or reagent kit is to be manufactured, labeled and
packaged in accordance with the Federal Food, Drug, and Cosmetic Act or the Public
Health Service Act, such as a new drug application (NDA) approved by the Food and
Drug Administration (FDA), a biologic product license issued by FDA, or a "Notice of
Claimed Investigational Exemption for a New Drug" (IND) that has been accepted by
the FDA; or
The manufacture and distribution of the generator or reagent kit
are not subject to the Federal Food, Drug, and Cosmetic Act and the Public Health
Service Act.
2.7.11.1.3 The
applicant submits information on the radionuclide, chemical and physical form,
packaging including maximum activity per package, and shielding provided by the
packaging of the radioactive material contained in the generator or reagent
kit;
2.7.11.1.4 The label affixed to the
generator or reagent kit contains information on the radionuclide, quantity, and
date of assay; and
2.7.11.1.5 The label
affixed to the generator or reagent kit, or the leaflet or brochure which
accompanies the generator or reagent kit, contains:
2.7.11.1.5.1 Adequate information, from a
radiation safety standpoint, on the procedures to be followed and the equipment and
shielding to be used in eluting the generator or processing radioactive material
with the reagent kit, and
2.7.11.1.5.2 A
statement that this generator reagent kit (as appropriate) is approved for use by
persons licensed by the Department pursuant to RHA 2.7.3 and
RHA 2.26 Schedule D, Group III of
Part II or under equivalent licenses of the U.S. Nuclear Regulatory Commission, an
Agreement State, or a Licensing State or that an application for such license has
been filed with the Department on or before August 9, 1977 and is still pending. The
labels, leaflets or brochures required by this paragraph are in addition to the
labeling required by FDA and they may be separate from or, with the approval of FDA,
may be combined with the labeling required by FDA.
2.7.11.2 If an application is filed pursuant to
RHA 2.7.11.1 on or before
** [Aug. 9, 1977], for a license to
manufacture and distribute a generator or reagent kit that was distributed
commercially on or before
* the applicant may continue the distribution
of such generator or reagent kit until the Department issues the license or notifies
the applicant otherwise.
2.7.12 Manufacture and Distribution of Sources or
Devices Containing Radioactive Material for Medical Use.
2.7.12.1 An application for a specific license to
manufacture and distribute sources and devices containing radioactive material to
persons licensed pursuant to RHA 2.7.3 for use as a calibration or reference source
or for the uses listed in Group VI of
RHA 2.26 Schedule D of this part
will be approved if:
2.7.12.1.1 The applicant
satisfies the general requirements in
RHA 2.6 of this Part; and
2.7.12.1.2 The applicant submits sufficient
information regarding each type of source or device pertinent to an evaluation of
its radiation safety, including:
NOTE: Although the Department does not regulate the manufacture
and distribution of reagent kits that do not contain radioactive material, it does
regulate the use of such reagent kits for the preparation of radiopharmaceuticals
containing radioactive material as part of its licensing and regulation of the users
of radioactive material. Any manufacturer of reagent kits that do not contain
radioactive material who desires to have his reagent kits approved by the Department
for use by persons licensed pursuant to RHA 2.7.3 and Group III of
RHA 2.26 Schedule D of this part
may submit the pertinent information specified in RHA 2.7.11.
2.7.12.1.2.1 The radioactive material contained,
its chemical and physical form, and amount;
2.7.12.1.2.2 Details of design and construction of
the source or device;
2.7.12.1.2.3
Procedures for, and results of, prototype tests to demonstrate that the source or
device will maintain its integrity under stresses likely to be encountered in normal
use and accidents;
2.7.12.1.2.4 For
devices containing radioactive material, the radiation profile of a prototype
device;
2.7.12.1.2.5 Details of quality
control procedures to assure that production sources and devices meet the standards
of the design and prototype tests;
2.7.12.1.2.6 Procedures and standards for
calibrating sources and devices;
2.7.12.1.2.7 Legend and methods for labeling
sources and devices as to their radioactive content;
2.7.12.1.2.8 Instruction for handling and storing
the source or device from the radiation safety standpoint; these instructions are to
be included on a durable label attached to the source or device or attached to a
permanent storage container for the source or device; Provided, that instructions
which are too lengthy for such label and printed in detail on a brochure which is
referenced on the label;
2.7.12.1.3 The label affixed to the source or
device, or to the permanent storage container for the source or device, contains
information on the radionuclide, quantity, and date of assay, and a statement that
the (name of source or device) is licensed by the Department for distribution to
persons licensed pursuant to RHA 2.7.3 and
RHA 2.26 Schedule D, Group VI of
this part or under equivalent licenses of the U.S. Nuclear Regulatory Commission, an
Agreement State, or a Licensing State, or that a pending application for such
license has been filed with the Department on or before August 9, 1977; provided,
that such labeling for sources which do not require long term storage (e.g.,
gold-198 seeds) may be on a leaflet or brochure which accompanies the
source.
2.7.12.2 In the event
the applicant desires that the source or device be required to be tested for leakage
of radioactive material at intervals longer than six months, he shall include in his
application sufficient information to demonstrate that such longer interval is
justified by performance characteristics of the source or device or similar sources
or devices and by design features that have a significant bearing on the probability
or consequences of leakage of radioactive material from the source.
In determining the acceptable interval for test of leakage of
radioactive material, the Department will consider information that includes, but is
not limited to:
2.7.12.2.1 Primary
containment (source capsule);
2.7.12.2.2
Protection of primary containment;
2.7.12.2.3 Method of sealing
containment;
2.7.12.2.4 Containment
construction materials;
2.7.12.2.5 Form
of contained radioactive material;
2.7.12.2.6 Maximum temperature withstood during
prototype tests;
2.7.12.2.7 Maximum
pressure withstood during prototype tests;
2.7.12.2.8 Maximum quantity of contained
radioactive material;
2.7.12.2.9
Radiotoxicity of contained radioactive material; and
2.7.12.2.10 Operating experience with identical
sources or devices or similarly designed and constructed sources or
devices.
2.7.12.3 If an
application is filed pursuant to RHA 2.7.12.1 on or before
** [Aug. 9, 1977], for a license to
manufacture and distribute a source or device that was distributed commercially on
or before*, the applicant may continue the distribution
of such source or device to group licensees until the Department issues the license
or notifies the applicant otherwise.
2.7.13 Calibration or reference sources containing
Americium-241 or Radium-226: Requirements for license to manufacture or initially
transfer.
2.7.13.1 An application for a specific
license to manufacture or initially transfer calibration or reference sources
containing Americium-241 or Radium-226, for distribution to persons generally
licensed under RHA 2.4, will be approved if:
2.7.13.1.1 The applicant satisfies the general
requirements of
RHA 2.6;
2.7.13.1.2 The applicant submits sufficient
information regarding each type of calibration or reference source pertinent to
evaluation of the potential radiation exposure, including:
2.7.13.1.2.1 Chemical and physical form and
maximum quantity of Americium 241 or Radium-226 in the source;
2.7.13.1.2.2 Details of construction and
design;
2.7.13.1.2.3 Details of the
method of incorporation and binding of the Americium-241 or Radium-226 in the
source;
2.7.13.1.2.4 Procedures for and
results of prototype testing of sources, which are designed to contain more than
0.005 microcurie of Americium-241 or Radium-226, to demonstrate that the
Americium-241 or Radium-226 contained in each source will not be released or be
removed from the source under normal conditions of use;
2.7.13.1.2.5 Details of quality control procedures
to be followed in manufacture of the source;
2.7.13.1.2.6 Description of labeling to be affixed
to the source or the storage container for the source;
2.7.13.1.2.7 Any additional information, including
experimental studies and tests, required by the Department to facilitate a
determination of the safety of the source.
2.7.13.1.3 Each source will contain no more than 5
microcuries of Americium-241 or Radium-226.
2.7.13.1.4 The Department determines, with respect
to any type of source containing more than 0.005 microcuries of Americium-241 or
Radium-226, that:
2.7.13.1.4.1 The method of
incorporation and binding of the Americium-241 or Radium-226 in the source is such
that the Americium-241 will not be released or be removed from the source under
normal conditions of use and handling of the source; and
2.7.13.1.4.2 The source has been subjected to and
has satisfactorily passed the appropriate tests prescribed by 2.7.8.4.
2.7.13.1.5 The applicant shall
subject at least five prototypes of each source that is designed to contain more
than 0.185 kilobecquerel (0.005 microcurie) of americium-241 or radium-226 to tests
as follows:
2.7.13.1.5.1 The initial quantity of
radioactive material deposited on each source is measured by direct counting of the
source.
2.7.13.1.5.2 The sources are
subjected to tests that adequately take into account the individual, aggregate, and
cumulative effects of environmental conditions expected in service that could
adversely affect the effective containment or binding of americium-241 or
radium-226, such as physical handling, moisture, and water immersion.
2.7.13.1.5.3 The sources are inspected for
evidence of physical damage and for loss of americium-241 or radium-226, after each
stage of testing, using methods of inspection adequate for determining compliance
with the criteria in RHA 2.7.8.1.5.4.
2.7.13.1.5.4 Source designs are rejected for which
the following has been detected for any unit: removal of more than 0.185
kilobecquerel (0.005 microcurie) of americium-241 or radium-226 from the source or
any other evidence of physical damage.
2.7.13.2 Each person licensed under this Section
shall affix to each source, or storage container for the source, a label which shall
contain sufficient information relative to safe use and storage of the source and
shall include the following statement or a substantially similar statement which
contains the information called for in the following statement:
The receipt, possession, use, and transfer of this source, Model,
Serial No., are subject to a general license and the regulations of the United
States Nuclear Regulatory Commission or of a State with which the Commission has
entered into an agreement for the exercise of regulatory authority. Do not remove
this label.
CAUTION-RADIOACTIVE MATERIAL-THIS SOURCE CONTAINS AMERICIUM-241
(or RADIUM-226). DO NOT TOUCH RADIOACTIVE PORTION OF THIS SOURCE.
Name of manufacturer or initial transferor
2.7.13.3 Each person licensed under RHA 2.7.8
shall perform a dry wipe test upon each source containing more than 3.7
kilobecquerels (0.1 microcurie) of Americium-241 or Radium-226 before transferring
the source to a general licensee under RHA 2.4.5, or comparable regulation. This
test shall be performed by wiping the entire radioactive surface of the source with
a filter paper with the application of moderate finger pressure. The radioactivity
on the paper shall be measured by using methods capable of detecting 0.185
kilobecquerel (0.005 microcurie) of Americium-241 or Radium-226. If a source has
been shown to be leaking or losing more than 0.185 kilobecquerel (0.005 microcurie)
of americium-241 or radium-226 by the methods described in this section, the source
must be rejected and must not be transferred to a general licensee RHA 2.4.5 or
comparable regulation.
2.7.13.4 An
applicant for a license under this Section shall, for any type of source which is
designed to contain more than 0.185 kilobecquerel (0.005 microcurie) of
Americium-241 or Radium-226, conduct prototype tests, in the order listed, on each
of five prototypes of the source, which contains more than 0.185 kilobecquerel
(0.005 microcurie) of Americium-241 or Radium-226, as follows:
2.7.13.4.1 Initial measurement. The quantity of
radioactive material deposited on the source shall be measured by direct counting of
the source.
2.7.13.4.2 Dry wipe test.
The entire radioactive surface of the source shall be wiped with filter paper with
the application of moderate finger pressure. Removal of radioactive material from
the source shall be determined by measuring the radioactivity on the filter paper or
by direct measurement of the radioactivity on the source following the dry
wipe.
2.7.13.4.3 Wet wipe test. The
entire radioactive surface of the source shall be wiped with filter paper, moistened
with water, with the application of moderate finger pressure. Removal of radioactive
material from the source shall be determined by measuring the radioactivity on the
filter paper after it has dried or by direct measurement of the radioactivity on the
source following the wet wipe.
2.7.13.4.4 Water soak test. The source shall be
immersed in water at room temperature for a period of 24 consecutive hours. The
source shall then be removed from the water. Removal of radioactive material from
the source shall be determined by direct measurement of the radioactivity on the
source after it has dried or by measuring the radioactivity in the residue obtained
by evaporation of the water in which the source was immersed.
2.7.13.4.5 Dry wipe test. On completion of the
preceding test in this section, the dry wipe test described in 2.7.13.4.2 shall be
repeated.
2.7.13.4.6 Observations.
Removal of more than 0.005 microcurie of radioactivity in any test prescribed by
this section shall be cause for rejection of the source design. Results of prototype
tests submitted to the Commission shall be given in terms of radioactivity in
microcuries and percent of removal from the total amount of radioactive material
deposited on the source.
[FN3*] The model, serial number, and name of manufacturer,
assembler, or initial transferor may be omitted from this label provided they are
elsewhere specified in labeling affixed to the device.
[FN**] Adoption date of these Regulatory changes
[FN*] 30 days prior to adoption date
2.7.14 Luminous safety devices
for use in aircraft: Requirements for license to manufacture, assemble, repair or
initially transfer. An application for a specific license to manufacture, assemble,
repair or initially transfer luminous safety devices containing tritium or
promethium-147 for use in aircraft, for distribution to persons generally licensed
under RHA 2.4.4, will be approved if:
2.7.14.1 The
applicant satisfies the general requirements specified in
RHA 2.6;
2.7.14.2 The applicant submits sufficient
information regarding each device pertinent to evaluation of the potential radiation
exposure, including:
2.7.14.2.1 Chemical and
physical form and maximum quantity of tritium or promethium-147 in each
device;
2.7.14.2.2 Details of
construction and design;
2.7.14.2.3
Details of the method of binding or containing the tritium or
promethium-147;
2.7.14.2.4 Procedures
for and results of prototype testing to demonstrate that the tritium or promethium
147 will not be released to the environment under the most severe conditions likely
to be encountered in normal use;
2.7.14.2.5 Quality assurance procedures to be
followed that are sufficient to ensure compliance with § 32.55;
2.7.14.2.6 Any additional information, including
experimental studies and tests, required by the Department to facilitate a
determination of the safety of the device.
2.7.14.3 Each device will contain no more than 10
curies of tritium or 300 millicuries of promethium 147. The levels of radiation from
each device containing promethium-147 will not exceed 0.5 millirad per hour at 10
centimeters from any surface when measured through 50 milligrams per square
centimeter of absorber.
2.7.14.4 The
Department determines that:
2.7.14.4.1 The method
of incorporation and binding of the tritium or promethium-147 in the device is such
that the tritium or promethium-147 will not be released under the most severe
conditions which are likely to be encountered in normal use and handling of the
device;
2.7.14.4.2 The tritium or
promethium-147 is incorporated or enclosed so as to preclude direct physical contact
by any person with it;
2.7.14.4.3 The
device is so designed that it cannot easily be disassembled; and
2.7.14.4.4 Prototypes of the device have been
subjected to and have satisfactorily passed the tests required by
2.7.14.5.
2.7.14.5 The
applicant shall subject at least five prototypes of the device to tests as follows:
2.7.14.5.1 The devices are subjected to tests that
adequately take into account the individual, aggregate, and cumulative effects of
environmental conditions expected in service that could adversely affect the
effective containment of tritium or promethium-147, such as temperature, moisture,
absolute pressure, water immersion, vibration, shock, and weathering.
2.7.14.5.2 The devices are inspected for evidence
of physical damage and for loss of tritium or promethium-147, after each stage of
testing, using methods of inspection adequate for determining compliance with the
criteria in RHA 2.7.14.5.3.
2.7.14.5.3
Device designs are rejected for which the following has been detected for any unit:
2.7.14.5.3.1 A leak resulting in a loss of 0.1
percent or more of the original amount of tritium or promethium-147 from the device;
or
2.7.14.5.3.2 Surface contamination of
tritium or promethium-147 on the device of more than 2,200 disintegrations per
minute per 100 square centimeters of surface area; or
2.7.14.5.3.3 Any other evidence of physical
damage.
2.7.14.6 The
device has been registered in the Sealed Source and Device Registry.
2.7.14.7 Quality assurance and prohibition of
transfer for luminous safety devices for use in aircraft.
2.7.14.7.1 Each person licensed under RHA 2.7.14
shall visually inspect each device and shall reject any that has an observable
physical defect that could adversely affect containment of the tritium or
promethium-147.
2.7.14.7.2 Each person
licensed under RHA 2.7.14 shall:
2.7.14.7.2.1
Maintain quality assurance systems in the manufacture of the luminous safety device
in a manner sufficient to provide reasonable assurance that the safety-related
components of the distributed devices are capable of performing their intended
functions; and
2.7.14.7.2.2 Subject
inspection lots to acceptance sampling procedures, by procedures specified in
paragraph (c) of this section and in the license issued under RHA 2.7.14, to provide
at least 95 percent confidence that the Lot Tolerance Percent Defective of 5.0
percent will not be exceeded.
2.7.14.7.3 The licensee shall subject each
inspection lot to:
2.7.14.7.3.1 Tests that
adequately take into account the individual, aggregate, and cumulative effects of
environmental conditions expected in service that could adversely affect the
effective containment of tritium or promethium-147, such as absolute pressure and
water immersion.
2.7.14.7.3.2 Inspection
for evidence of physical damage, containment failure, or for loss of tritium or
promethium-147 after each stage of testing, using methods of inspection adequate for
applying the following criteria for defective:
2.7.14.7.3.2.1 A leak resulting in a loss of 0.1
percent or more of the original amount of tritium or promethium-147 from the
device;
2.7.14.7.3.2.2 Levels of
radiation in excess of 5 microgray (0.5 millirad) per hour at 10 centimeters from
any surface when measured through 50 milligrams per square centimeter of absorber,
if the device contains promethium-147; and
2.7.14.7.3.2.3 Any other criteria specified in the
license issued under RHA 2.7.14.
2.7.14.7.4 No person licensed under RHA 2.7.14
shall transfer to persons generally licensed under RHA 2.4.4, or under an equivalent
general license of an Agreement State:
2.7.14.7.4.1 Any luminous safety device tested and
found defective under any condition of a license issued under RHA 2.7.14, or RHA
2.7.14.8, unless the defective luminous safety device has been repaired or reworked,
retested, and determined by an independent inspector to meet the applicable
acceptance criteria; or
2.7.14.7.4.2 Any
luminous safety device contained within any lot that has been sampled and rejected
as a result of the procedures in RHA 2.7.14.8.2, unless:
2.7.14.7.4.2.1 A procedure for defining sub-lot
size, independence, and additional testing procedures is contained in the license
issued under RHA 2.7.14; and
2.7.14.7.4.2.2 Each individual sub-lot is sampled,
tested, and accepted in accordance with RHA 2.7.14.8.2 and RHA 2.7.14.10.2.1 and any
other criteria that may be required as a condition of the license issued under RHA
2.7.14.
2.7.14.8 Material transfer reports for luminous
safety devices for use in aircraft.
2.7.14.8.1
Each person licensed under RHA 2.7.14 shall file an annual report with the Director,
Division of Radioactive Material, Bureau of Radiological Health, which must state
the total quantity of tritium or promethium-147 transferred to persons generally
licensed under RHA 2.4.4. The report must identify each general licensee by name,
state the kinds and numbers of luminous devices transferred, and specify the
quantity of tritium or promethium-147 in each kind of device. Each report must cover
the year ending June 30 and must be filed within thirty (30) days thereafter. If no
transfers have been made to persons generally licensed under RHA 2.4.4 during the
reporting period, the report must so indicate.
2.7.14.8.2 Each person licensed under RHA 2.7.14
shall report annually all transfers of devices to persons for use under a general
license in an NRC or Agreement State's regulations that are equivalent to RHA 2.4.4
to the NRC or responsible Agreement State agency. The report must state the total
quantity of tritium or promethium-147 transferred, identify each general licensee by
name, state the kinds and numbers of luminous devices transferred, and specify the
quantity of tritium or promethium-147 in each kind of device. If no transfers have
been made to a particular NRC licensee or Agreement State during the reporting
period, this information must be reported to the NRC or responsible Agreement State
agency upon request of the Department.
2.7.15 Ice detection devices containing
strontium-90; requirements for license to manufacture or initially transfer. An
application for a specific license to manufacture or initially transfer ice
detection devices containing strontium-90 for distribution to persons generally
licensed under RHA 2.4.7 will be approved if:
2.7.15.1 The applicant satisfies the general
requirements specified in RHA 2.6
2.7.15.2 The applicant submits sufficient
information regarding each type of device pertinent to evaluation of the potential
radiation exposure, including:
2.7.15.2.1 Chemical
and physical form and maximum quantity of strontium-90 in the device;
2.7.15.2.2 Details of construction and design of
the source of radiation and its shielding;
2.7.15.2.3 Radiation profile of a prototype
device;
2.7.15.2.4 Procedures for and
results of prototype testing of devices to demonstrate that the strontium90
contained in each device will not be released or be removed from the device under
the most severe conditions likely to be encountered in normal handling and
use;
2.7.15.2.5 Details of quality
control procedures to be followed in manufacture of the device;
2.7.15.2.6 Description of labeling to be affixed
to the device;
2.7.15.2.7 Instructions
for handling and installation of the device;
2.7.15.2.8 Any additional information, including
experimental studies and tests, required by the Department to facilitate a
determination of the safety of the device;
2.7.15.3 Each device will contain no more than 50
microcuries of strontium-90 in an insoluble form;
2.7.15.4 Each device will bear durable, legible
labeling which includes the radiation caution symbol prescribed by Part 3, a
statement that the device contains strontium-90 and the quantity thereof,
instructions for disposal and statements that the device may be possessed pursuant
to a general license, that the manufacturer or civil authorities should be notified
if the device is found, that removal of the labeling is prohibited and that
disassembly and repair of the device may be performed only by a person holding a
specific license to manufacture or service such devices;
2.7.15.5 The Department determines that:
2.7.15.5.1 The method of incorporation and binding
of the strontium-90 in the device is such that the strontium-90 will not be released
from the device under the most severe conditions which are likely to be encountered
in normal use and handling of the device;
2.7.15.5.2 The strontium-90 is incorporated or
enclosed so as to preclude direct physical contact by any individual with it and is
shielded so that no individual will receive a radiation exposure to a major portion
of his body in excess of 0.5 rem in a year under ordinary circumstances of
use;
2.7.15.5.3 The device is so
designed that it cannot be easily disassembled;
2.7.15.5.4 Prototypes of the device have been
subjected to and have satisfactorily passed the tests required by RHA 2.7.15.6 of
this section.
2.7.15.5.5 Quality control
procedures have been established to satisfy the requirements of
10 CFR
32.62.
2.7.15.6 The applicant shall subject at least five
prototypes of the device to tests as follows:
2.7.15.6.1 The devices are subjected to tests that
adequately take into account the individual, aggregate, and cumulative effects of
environmental conditions expected in service that could adversely affect the
effective containment of strontium-90, such as temperature, moisture, absolute
pressure, water immersion, vibration, shock, and weathering.
2.7.15.6.2 The devices are inspected for evidence
of physical damage and for loss of strontium- 90 after each stage of testing, using
methods of inspection adequate for determining compliance with the criteria in RHA
2.7.15.6.3.
2.7.15.6.3 Device designs
are rejected for which the following has been detected for any unit:
2.7.15.6.3.1 A leak resulting in a loss of 0.1
percent or more of the original amount of strontium-90 from the device; or
2.7.15.6.3.2 Surface contamination of strontium-90
on the device of more than 2,200 disintegrations per minute per 100 square
centimeters of surface area; or
2.7.15.6.3.3 Any other evidence of physical
damage.
2.7.15.7 The
device has been registered in the Sealed Source and Device
Registry.
2.7.16 Requirements
for license to initially transfer source material for use under the 'small
quantities of source material' general license
2.7.16.1 An application for a specific license to
initially transfer source material for use under
RHA
2.3, or equivalent regulations of the U.S. Nuclear
Regulatory Commission or an Agreement State, will be approved if:
2.7.16.1.1 The applicant satisfies the general
requirements specified in
RHA 2.6; and
2.7.16.1.2 The applicant submits adequate
information on, and the Department approves the methods to be used for quality
control, labeling, and providing safety instructions to recipients.
2.7.16.2 Conditions of licenses to
initially transfer source material for use under the 'small quantities of source
material' general license: Quality control, labeling, safety instructions, and
records and reports
2.7.16.2.1 Each person
licensed under RHA 2.7.16 shall label the immediate container of each quantity of
source material with the type of source material and quantity of material and the
words, "radioactive material."
2.7.16.2.2 Each person licensed under RHA 2.7.16
shall ensure that the quantities and concentrations of source material are as
labeled and indicated in any transfer records.
2.7.16.2.3 Each person licensed under RHA 2.7.16
shall provide the information specified in this paragraph to each person to whom
source material is transferred for use under
RHA
2.3, or equivalent regulations of the U.S. Nuclear
Regulatory Commission or an Agreement State provisions. This information must be
transferred before the source material is transferred for the first time in each
calendar year to the particular recipient. The required information includes:
2.7.16.2.3.1 A copy of
RHA
2.3 and RHA 2.18, or relevant equivalent regulations of the
Agreement State.
2.7.16.2.3.2
Appropriate radiation safety precautions and instructions relating to handling, use,
storage, and disposal of the material.
2.7.16.2.4 Each person licensed under RHA 2.7.16
shall report transfers as follows:
2.7.16.2.4.1
File a report with the Department. The report shall include the following
information:
2.7.16.2.4.1.1 The name, address, and
license number of the person who transferred the source material;
2.7.16.2.4.1.2 For each general licensee under
RHA
2.3,or equivalent regulations of the U.S. Nuclear
Regulatory Commission or an Agreement State provisions, to whom greater than 50
grams (0.11 lb) of source material has been transferred in a single calendar
quarter, the name and address of the general licensee to whom source material is
distributed; a responsible agent, by name and/or position and phone number, of the
general licensee to whom the material was sent; and the type, physical form, and
quantity of source material transferred; and
2.7.16.2.4.1.3 The total quantity of each type and
physical form of source material transferred in the reporting period to all such
generally licensed recipients.
2.7.16.2.4.2 File a report with each responsible
Agreement State agency that identifies all persons, operating under provisions
equivalent to
RHA
2.3, to whom greater than 50 grams (0.11 lb) of source
material has been transferred within a single calendar quarter. The report shall
include the following information specific to those transfers made to the Agreement
State being reported to:
2.7.16.2.4.2.1 The name,
address, and license number of the person who transferred the source material;
and
2.7.16.2.4.2.2 The name and address
of the general licensee to whom source material was distributed; a responsible
agent, by name and/or position and phone number, of the general licensee to whom the
material was sent; and the type, physical form, and quantity of source material
transferred.
2.7.16.2.4.2.3 The total
quantity of each type and physical form of source material transferred in the
reporting period to all such generally licensed recipients within the Agreement
State.
2.7.16.2.4.3 Submit
each report by January 31 of each year covering all transfers for the previous
calendar year. If no transfers were made to persons generally licensed under
RHA
2.3, or equivalent regulations of the U.S. Nuclear
Regulatory Commission or an Agreement State provisions, during the current period, a
report shall be submitted to the Department indicating so. If no transfers have been
made to general licensees during the reporting period, this information shall be
reported to the Department upon request.
2.7.16.2.5 Each person licensed under RHA 2.7.16
shall maintain all information that supports the reports required concerning each
transfer to a general licensee for a period of 1 year after the event is included in
a report to the Department.