Current through Register Vol. 46, No. 12, March 20, 2024
(a) Standard
conditions for testing. Flame tests shall be performed under or upon immediate
removal from standard atmospheric conditions and on specimens in moisture
equilibrium under standard atmospheric conditions.
(b) Preconditioning. In the event of dispute
concerning the results of tests that may be affected by the moisture content,
the material shall be preconditioned by being brought to moisture equilibrium
with an atmosphere having a relative humidity of not over 10 percent and a
temperature not over 125° F. (52° C.). The material shall then be
brought to moisture equilibrium under standard atmospheric conditions and then
tested.
(c) Leaching. Tests in
sections
80-8.6
and
80-8.7
of this Subpart shall be performed both before and after leaching.
(1) Test specimen. Test specimens to be
leached shall be of the following dimensions:
(i) Each flooring material test specimen
shall be a 9 inch by 9 inch (+-1/16 inch) section of the flooring material to
be tested.
(ii) Wall and top
material test specimens shall be rectangles of cloth 2 3/4 inches by 12 inches.
(+- 1/16 inch) with the long dimensions parallel to either the warp or filling
directions of the material.
(2) Apparatus. The following apparatus shall
be used in the leaching process.
(i) Water
container or tank of such shape and size that the specimen can be submerged
therein with all surfaces of the specimen having full access to the water. For
cloth specimens the container shall allow not less than 1/2 gallon of water for
each square foot of specimen. The water shall be changed by a continuous flow
or by emptying and refilling so that there shall be at least six complete
changes of water in a 72-hour period.
(ii) Means of maintaining water at a
temperature of 60° F. to 70° F. (15.5° C. to 21.1° C.) and a pH
of 6.0 to 8.0 during the test.
(iii) Means for holding the specimen
submerged throughout the leaching period.
(3) Procedure. The specimens shall be
immersed in water at a temperature of 60° F. to 70° F. (15.5° C. to
21.1° C.) and a pH of 6.0 to 8.0 for 72 hours. The specimen shall then be
removed, air-dried, and brought to standard atmospheric conditions prior to
further testing.
(d)
Accelerated weathering. Tests in sections
80-8.6
and
80-8.7
shall be performed both before and after accelerated weathering.
(1) Test specimen. Test specimens to be
weathered shall be of the following dimensions:
(i) Each flooring material test specimen
shall be a 9 inch by 9 inch (+-1/16 inch) section of the flooring material to
be tested.
(ii) Wall and top
material test specimens shall be rectangles of cloth 2 3/4 inches by 12 inches
(+-1/16 inch) with the long dimensions parallel to either the warp or filling
directions of the material.
(2) Apparatus. The following apparatus shall
be used in the accelerated weathering process:
(i) Vertical carbon arc mounted at the center
or a vertical cylinder. The arc shall be designed to accommodate either two or
three pairs of carbons but shall burn only one pair at a time, automatically
transferring from one pair to another as the carbons are consumed. The carbons
shall be sunshine-cored and copper-coated, No. 22 for the upper pair and 13 for
the lower pair. The arc shall be operated on 60 amperes and 50 volts across the
arc for alternating current and on 50 amperes and 60 volts across the arc for
direct current.
(ii) A rotating
rack with holder in which the specimens are suspended vertically and normally
to radiation from the arc with the center of the face of the specimen at a
radial distance of approximately 18 inches from the arc.
(iii) Water-spray nozzles shall be mounted
horizontally (the water-spray assembly vertically) in the test chamber inside
the specimen rack and so placed that the water shall strike the specimens
evenly over their entire length in the form of a fine spray in sufficient
volume to cover specimens immediately on impact. The apparatus shall be so
operated that the specimens are exposed to successive cycles of 102 minutes of
light without spray and 18 minutes of light with spray.
(iv) Means for maintaining the required
temperature of water in the spray.
(v) Means of maintaining the required
pressure of water entering the spray.
(vi) Means for delivering the required
quantity of water per spray nozzle to the specimen.
(vii) Exhaust fan to ventilate the arc
effectively.
(viii) Black panel
thermometer unit for measuring the temperature within the machine. This unit
shall consist of a metal panel to the base of which is attached the sensitive
portion of a bimetallic dia-type thermometer. The entire base is then coated
twice with long lasting baked enamel paint.
(3) Procedure. The following procedure shall
be followed:
(i) The rack shall rotate about
the arc at a uniform speed of one revolution per minute.
(ii) The temperature of water in the spray
shall be 80° +- 10° F. (26.7° +- 5.6° C).
(iii) The pressure of the water entering the
spray shall be 1-18 psi inclusive.
(iv) The quantity of water delivered to the
specimen shall be.12 to.25 gallons, inclusive, per hour per spray
nozzel.
(v) The black panel
temperature at the exposure plane of the specimen rack shall be 155°
+-10° F. (68° +- 5.7° C.) When measured in the following manner:
(a) Before reading the temperature, the
machine shall be full of specimens and shall be in operation long enough for
thermal equilibrium to be established. The black panel shall be mounted in the
test-panel rack and readings taken at the point where water spray is not
striking the panel.
(vi)
The specimen shall be suspended on the rotating rack without tension and in
such a way that the ends or corners cannot curl. The long dimension of the
specimen shall be in the vertical position and shall be indicated on the
reverse side of the cloth. No test portion of the specimen shall be over seven
inches above or below the horizontal plane of the arc.
(vii) The specimen shall be exposed to normal
radiation from the arc for 100 hours.
(viii) At the end of the exposure period, the
specimen shall be removed from the machine, allowed to dry, and brought to
standard atmospheric conditions prior to further testing.