Minnesota Administrative Rules
Agency 167 - Pollution Control Agency
Chapter 7037 - PETROLEUM CONTAMINATED SOIL MANAGEMENT
Part 7037.3100 - ANALYSIS OF PETROLEUM CONTAMINATED SOIL SAMPLES
Universal Citation: MN Rules 7037.3100
Current through Register Vol. 48, No. 39, March 25, 2024
Subpart 1. General requirements.
All petroleum contaminated soil samples must be analyzed using a United States Environmental Protection Agency approved laboratory method or equivalent, unless an alternative method is specified in subpart 2.
Subp. 2. Specific analysis requirements.
Specific laboratory analysis requirements are given in items A to E for selected parameters.
A.
Analysis for the parameters of parameter code A in part
7037.0500, subpart
2, must be done using
purge-and-trap laboratory methodology in conjunction with EPA method 8010,
Minnesota Department of Health method 466A, or an equivalent gas chromatography
method.
B. Analysis for the
parameters of parameter code B in part
7037.0500, subpart
2, must be done using
purge-and-trap laboratory methodology in conjunction with EPA method 8020 or an
equivalent gas chromatography method.
C. Total petroleum hydrocarbons as gasoline,
code D in part
7037.0500, subpart
2, must be done using the
Wisconsin Department of Natural Resources Modified Gasoline Range Organics
(GRO) method.
D. Total petroleum
hydrocarbons as fuel oil, code E in part
7037.0500, subpart
2, must be done using the
Wisconsin Department of Natural Resources Modified Diesel Range Organics (DRO)
method.
E. PCBs, code H in part
7037.0500, subpart
2, must be done using EPA
method 8080 or an equivalent gas chromatography method.
Statutory Authority: MS s 116.07
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