Louisiana Administrative Code
Title 7 - AGRICULTURE AND ANIMALS
Part XIII - Seeds
Chapter 13 - Industrial Hemp
Subchapter H - Sampling, Testing, Remediation, and Destruction
Section XIII-1335 - THC Sampling and Testing
Universal Citation: LA Admin Code XIII-1335
Current through Register Vol. 50, No. 9, September 20, 2024
A. All industrial hemp plants or plant parts, whether harvested or unharvested, shall be subject to sampling and testing for THC levels by LDAF as set forth in this Section.
B. The licensee shall be responsible for the cost of all sample testing fees, as set forth in this Chapter.
C. Sample Collection
1. Licensees shall submit a Harvest Report
for each field, greenhouse or indoor growing structure to LDAF prior to
harvesting any industrial hemp plants.
2. LDAF will attempt to notify the licensee
of the date and approximate time when samples will be collected.
3. The licensee or designated responsible
party shall be present during the sample collection.
4. LDAF will collect samples from each plot
within any field, greenhouse, or indoor growing structure.
5. LDAF may retain and transport samples of
industrial hemp plants and plant parts collected from an industrial hemp
licensee as required by the Industrial Hemp Law (R.S.
3:1461 et seq.) and this Chapter.
6. All samples collected by LDAF become the
property of the LDAF and are non-returnable. No compensation shall be owed by
LDAF for samples collected under this Chapter.
7. The licensee shall not harvest industrial
hemp plants or plant parts prior to samples being collected by LDAF.
8. The licensee shall harvest industrial hemp
plants or plant parts within 30 days of the sample collection by LDAF, unless
an exception is authorized in writing by LDAF. Should a licensee fail to
complete harvest within 30 days and no exception was authorized by LDAF, a
second sample and test of the plot shall be performed and the licensee shall be
assessed an additional testing fee per sample in an amount not to exceed $250
per sample.
D. Performance-based Sampling
1. Industrial hemp
lots produced for research purposes may not be subject to sampling and testing
requirements outlined in this Section when all of the following requirements
are met:
a. LDAF has a confidence level that
95 percent of the industrial hemp plants in each lot subject to alternate
method will not test above the acceptable industrial hemp THC level;
b. no industrial hemp will enter the stream
of commerce;
c. the research
institution has submitted and received written approval of an industrial hemp
research plan from LDAF;
d. the
research institution maintains records documenting the strain or variety's
compliance with the acceptable industrial hemp THC level.
2. LDAF may inspect, sample, and test any
industrial hemp plants or plant parts, at any time to ensure compliance with
this Chapter.
3. LDAF shall conduct
random inspections, including records reviews on research institutions,
regardless of whether or not they are subject to the sampling and testing
requirements.
E. Laboratory Testing
1. Quantitative
determination of THC levels measured using liquid chromatography with
ultraviolet detection (LC-UV) or mass spectral detection if required by matrix
interference (LC/MS/MS) shall be the accepted analytical technique to avoid the
risk of incomplete decarboxylation, therefore, removing the need for any
post-decarboxylation.
2. The
testing methodology shall consider the potential conversion of THC-A in
industrial hemp into THC and the test result shall measure the total available
THC derived from the sum of the THC and THC-A content. Appropriately, the THC-A
result will be modified by the molecular weight conversion factor 0.877 prior
to summation with THC. The total THC concentration level shall be reported on a
dry weight basis.
3. Analytical
testing for purposes of detecting the concentration levels of THC shall meet
the following standards:
a. laboratory quality
assurance must ensure the validity and reliability of test results;
b. analytical method selection, validation,
and verification must ensure that the testing method used is appropriate (fit
for purpose), and that the laboratory can successfully perform the
testing;
c. the demonstration of
testing validity must ensure consistent, accurate analytical
performance;
d. method performance
specifications must ensure analytical tests are sufficiently sensitive for the
purposes of detectability requirements of this Chapter;
e. an effective disposal procedure in
accordance with DEA regulations for samples of industrial hemp plants and
industrial hemp plant parts that do not meet the requirements of
R.S.
3:1461 et seq. or this Chapter.
f. the measurement of uncertainty shall be
estimated and reported with the results.
4. All testing of industrial hemp samples
shall be conducted by LDAF or by any public postsecondary education institution
in which LDAF has entered into a contract, cooperative endeavor agreement,
memorandum of understanding, or other agreement for THC testing.
5. The results of the THC analysis shall be
reported to the licensee and, if tested by an approved third party laboratory,
to LDAF.
6. A notification of
analysis shall be issued for samples with a THC concentration that do not
exceed the acceptable industrial hemp THC level and no further action shall be
required. The plot or harvested plant material from which the sample was
obtained shall be released for marketing or further processing.
7. A notification of analysis shall be issued
for samples that exceed the acceptable industrial hemp THC level and a licensee
may request a resample of any harvested cannabis that has undergone remediation
as set forth in
§1337 of this Chapter. If no request is
made within 10 calendar days of the sample results being reported to the
licensee, or the retested sample results exceed the acceptable industrial hemp
THC level, then the plot or harvested plant material from which the sample was
taken shall be subject to destruction as set forth in §1337
8. A notification of analysis for official
LDAF collected samples shall not be released until the licensee has submitted a
valid FSA 578 form to LDAF for the lot represented by the sample.
9. No industrial plants or plant parts for
which a THC analysis is pending shall be transferred, transported, sold,
marketed, or otherwise disposed of until approved by LDAF.
AUTHORITY NOTE: Promulgated in accordance with R.S. 3:1462, R.S. 3:1464, R.S. 3:1467, and R.S. 3:1468.
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