Current through Register Vol. 48, No. 38, September 20, 2024
The laboratory must analyze for the Section
611.311(a) VOCs
under Section 611.646, the Section
611.311(c) SOCs
under Section 611.648, the Section
611.310 State-only MCLs under
Section 611.641, and the Section
611.312 MCL for TTHMs under
Section 611.381 using the methods in
this Section. All methods are incorporated by reference in Section
611.102. USEPA Technical Notes,
incorporated by reference in Section 611.102, contains other required
analytical test procedures germane to conducting these analyses.
a) Volatile Organic Chemical Contaminants
(VOCs)
1) Benzene
A) Purge and Trap Gas Chromatography. USEPA
502.2
(95).
B) Purge and Trap Gas Chromatography-Mass
Spectrometry. USEPA 524.2 (95),
524.3 (09), or
524.4(13).
2) Carbon tetrachloride
A) Purge and Trap Capillary Column Gas
Chromatography. USEPA
502.2
(95).
B) Purge and Trap Gas Chromatography-Mass
Spectrometry. USEPA 524.2 (95),
524.3 (09), or
524.4
(13).
C) Liquid-Liquid Extraction and Gas
Chromatography. USEPA
551.1
(95).
3) Chlorobenzene
A) Purge and Trap Capillary Column Gas
Chromatography. USEPA
502.2
(95).
B) Purge and Trap Gas Chromatography-Mass
Spectrometry. USEPA 524.2 (95),
524.3 (09), or
524.4
(13).
4) 1,2-Dichlorobenzene
A) Purge and Trap Capillary Column Gas
Chromatography. USEPA
502.2
(95).
B) Purge and Trap Gas Chromatography-Mass
Spectrometry. USEPA 524.2 (95),
524.3 (09), or
524.4
(13).
5) 1,4-Dichlorobenzene
A) Purge and Trap Capillary Column Gas
Chromatography. USEPA
502.2
(95).
B) Purge and Trap Gas Chromatography-Mass
Spectrometry. USEPA 524.2 (95),
524.3 (09), or
524.4
(13).
6) 1,2-Dichloroethane
A) Purge and Trap Capillary Column Gas
Chromatography. USEPA
502.2
(95).
B) Purge and Trap Gas Chromatography-Mass
Spectrometry. USEPA 524.2 (95),
524.3 (09), or
524.4
(13).
7) 1,1-Dichloroethylene
A) Purge and Trap Capillary Column Gas
Chromatography. USEPA
502.2
(95).
B) Purge and Trap Gas Chromatography-Mass
Spectrometry. USEPA 524.2 (95),
524.3 (09), or
524.4
(13).
8) cis-Dichloroethylene
A) Purge and Trap Capillary Column Gas
Chromatography. USEPA
502.2
(95).
B) Purge and Trap Gas Chromatography-Mass
Spectrometry. USEPA 524.2 (95),
524.3 (09), or
524.4
(13).
9) trans-Dichloroethylene
A) Purge and Trap Capillary Column Gas
Chromatography. USEPA
502.2
(95).
B) Purge and Trap Gas Chromatography-Mass
Spectrometry. USEPA 524.2 (95),
524.3 (09), or
524.4
(13).
10) Dichloromethane
A) Purge and Trap Capillary Column Gas
Chromatography. USEPA
502.2
(95).
B) Purge and Trap Gas Chromatography-Mass
Spectrometry. USEPA 524.2 (95),
524.3 (09), or
524.4
(13).
11) 1,2-Dichloropropane
A) Purge and Trap Capillary Column Gas
Chromatography. USEPA
502.2
(95).
B) Purge and Trap Gas Chromatography-Mass
Spectrometry. USEPA 524.2 (95),
524.3 (09), or
524.4
(13).
12) Ethylbenzene
A) Purge and Trap Capillary Column Gas
Chromatography. USEPA
502.2
(95).
B) Purge and Trap Gas Chromatography-Mass
Spectrometry. USEPA 524.2 (95),
524.3 (09), or
524.4
(13).
13) Styrene
A) Purge and Trap Capillary Column Gas
Chromatography. USEPA
502.2 (95)
B) Purge and Trap Gas
Chromatography-Mass Spectrometry. USEPA
524.2 (95),
524.3(09), or
524.4
(13).
14) Tetrachloroethylene
A) Purge and Trap Capillary Column Gas
Chromatography. USEPA
502.2
(95).
B) Purge and Trap Gas Chromatography-Mass
Spectrometry. USEPA 524.2 (95),
524.3 (09), or
524.4
(13).
C) Liquid-Liquid Extraction and Gas
Chromatography. USEPA
551.1
(95).
15) Toluene
A) Purge and Trap Capillary Column Gas
Chromatography. USEPA
502.2
(95).
B) Purge and Trap Gas Chromatography-Mass
Spectrometry. USEPA 524.2 (95),
524.3 (09), or
524.4
(13).
16) 1,2,4-Trichlorobenzene
A) Purge and Trap Capillary Column Gas
Chromatography. USEPA
502.2
(95).
B) Purge and Trap Gas Chromatography-Mass
Spectrometry. USEPA 524.2 (95),
524.3 (09), or
524.4
(13).
17) 1,1,1-Trichloroethane
A) Purge and Trap Capillary Column Gas
Chromatography. USEPA
502.2
(95).
B) Purge and Trap Gas Chromatography-Mass
Spectrometry. USEPA 524.2 (95),
524.3 (09), or
524.4
(13).
C) Liquid-Liquid Extraction and Gas
Chromatography. USEPA
551.1
(95).
18) 1,1,2-Trichloroethane
A) Purge and Trap Capillary Column Gas
Chromatography. USEPA
502.2
(95).
B) Purge and Trap Gas Chromatography-Mass
Spectrometry. USEPA 524.2 (95),
524.3 (09), or
524.4
(13).
C) Liquid-Liquid Extraction and Gas
Chromatography. USEPA
551.1
(95).
19) Trichloroethylene
A) Purge and Trap Capillary Column Gas
Chromatography. USEPA
502.2
(95).
B) Purge and Trap Gas Chromatography-Mass
Spectrometry. USEPA 524.2 (95),
524.3 (09), or
524.4
(13).
C) Liquid-Liquid Extraction and Gas
Chromatography. USEPA
551.1
(95).
20) Vinyl chloride
A) Purge and Trap Capillary Column Gas
Chromatography. USEPA
502.2
(95).
B) Purge and Trap Gas Chromatography-Mass
Spectrometry. USEPA 524.2 (95),
524.3 (09), or
524.4
(13).
21) Xylenes (total)
A) Purge and Trap Capillary Column Gas
Chromatography. USEPA
502.2
(95).
B) Purge and Trap Gas Chromatography-Mass
Spectrometry. USEPA 524.2 (95),
524.3 (09), or
524.4
(13).
b) Synthetic Organic Chemical Contaminants
(SOCs)
1) 2,3,7,8-Tetrachlorodibenzodioxin
(2,3,7,8-TCDD or Dioxin). Isotope Dilution High Resolution Gas
Chromatography-High Resolution Mass Spectrometry. USEPA 1613 (94).
2) 2,4-D
A)
Gas Chromatography with Electron Capture Detector. ASTM D5317-93, ASTM
D5317-98(2003), ASTM D5317-20, SM 6640 B (01), or SM 6640 B (06).
B) Liquid-Liquid Extraction Gas
Chromatography with Electron Capture Detector. USEPA
515.1 (89) or
USEPA 515.3
(96).
C) Liquid-Solid Extraction Gas Chromatography
with Electron Capture Detector. USEPA
515.2
(95).
D) Liquid-Liquid Microextraction,
Derivatization, and Fast Gas Chromatography with Electron Capture Detector.
USEPA 515.4
(00).
E) High Performance Liquid Chromatography
with Photodiode Array Ultraviolet Detector. USEPA 555 (92).
3) 2,4,5-TP (Silvex)
A) Gas Chromatography with Electron Capture
Detector. ASTM D5317-93, ASTM D5317-98(2003), ASTM D5317-20, SM 6640 B (01), or
SM 6640 B (06).
B) Liquid-Liquid
Extraction Gas Chromatography with Electron Capture Detector. USEPA
515.1 (89) or
USEPA 515.3
(96).
C) Liquid-Solid Extraction Gas Chromatography
with Electron Capture Detector. USEPA
515.2
(95).
D) Liquid-Liquid Microextraction,
Derivatization, and Fast Gas Chromatography with Electron Capture Detector.
USEPA 515.4
(00).
E) High Performance Liquid Chromatography
with Photodiode Array Ultraviolet Detector. USEPA 555 (92).
4) Alachlor
A) Microextraction and Gas Chromatography.
USEPA 505 (95)1.
B) Gas
Chromatography with Nitrogen-Phosphorus Detector. USEPA 507 (95).
C) Liquid-Solid Extraction Gas Chromatography
with Electron Capture Detector. USEPA
508.1
(95).
D) Liquid-Solid Extraction and Capillary
Column Gas Chromatography-Mass Spectrometry. USEPA
525.2
(95).
E) Solid Phase Extraction and Capillary
Column Gas Chromatography-Mass Spectrometry. USEPA
525.3
(12).
F) Liquid-Liquid Extraction and Gas
Chromatography. USEPA
551.1
(95).
5) Atrazine
A) Microextraction and Gas Chromatography.
USEPA 505 (95)1.
B) Gas
Chromatography with Nitrogen-Phosphorus Detector. USEPA 507 (95).
C) Liquid-Solid Extraction Gas Chromatography
with Electron Capture Detector. USEPA
508.1
(95).
D) Liquid-Solid Extraction Gas Chromatography
with Electron Capture Detector. USEPA 523 (11).
E) Liquid-Solid Extraction and Capillary
Column Gas Chromatography-Mass Spectrometry. USEPA
525.2
(95).
F) Solid Phase Extraction and Capillary
Column Gas Chromatography-Mass Spectrometry. USEPA
525.3
(12).
G) Liquid Chromatography Electrospray
Ionization Tandem Mass Spectrometry. USEPA 536 (07).
H) Liquid-Liquid Extraction and Gas
Chromatography. USEPA
551.1
(95).
I) Immunoassay. Syngenta AG-6252.
6) Benzo(a)pyrene
A) Gas Chromatography-Mass Spectrometry.
USEPA 525.2
(95).
B) Solid Phase Extraction and Capillary
Column Gas Chromatography-Mass Spectrometry. USEPA
525.3
(12).
C) Liquid Liquid Extraction and HPLC with
Coupled Ultraviolet and Fluorescence Detection. USEPA 550 (90) or USEPA
550.1
(90).
7) Carbofuran.
A) Direct Aqueous Injection HPLC with
Post-Column Derivatization. SM 6610 (92), 6610 (96), 6610 B (99), SM 6610 B
(04), USEPA 531.1 (95), or
USEPA 531.2
(01).
B) Liquid Chromatography/Mass Spectrometry.
ME 531 (19).
8) Chlordane
A) Microextraction and Gas Chromatography.
USEPA 505 (95)1.
B) Gas
Chromatography with Electron Capture Detector. USEPA 508 (95).
C) Liquid-Solid Extraction Gas Chromatography
with Electron Capture Detector. USEPA
508.1
(95).
D) Gas Chromatography-Mass Spectrometry.
USEPA 525.2
(95).
E) Solid Phase Extraction and Capillary
Column Gas Chromatography-Mass Spectrometry. USEPA
525.3
(12).
9) Dalapon
A) Liquid-Liquid Extraction Gas
Chromatography with Electron Capture Detector. USEPA
515.1 (89) or
USEPA 515.3(96).
B) Liquid-Liquid Microextraction,
Derivatization, and Fast Gas Chromatography with Electron Capture Detector. SM
6640 B (01), SM 6640 B (06), or USEPA
515.4(00).
C) Solid Phase Extractor (Acidic Methanol),
Gas Chromatography, Electron Capture Detector. USEPA
552.1(92).
D) Liquid-Liquid Extraction (Acidic
Methanol), Gas Chromatography, Electron Capture Detector. USEPA
552.2(95) or
USEPA 552.3
(03).
E) Ion Chromatography, Electrospray
Ionization, Tandem Mass Spectrometry. USEPA 557 (09).
10) Dibromochloropropane (DBCP)
A) Microextraction and Gas Chromatography.
USEPA 504.1
(95).
B) Purge and Trap Gas Chromatography-Mass
Spectrometry. USEPA 524.3
(09).
C) Liquid-Liquid Extraction, Gas
Chromatography, Electron Capture Detector. USEPA
551.1
(95).
11) Di(2-ethylhexyl)adipate
A) Liquid-Liquid or Liquid-Solid Extraction
and Gas Chromatography with Photoionization Detection. USEPA 506
(95).
B) Liquid-Solid Extraction
and Capillary Column Gas Chromatography-Mass Spectrometry. USEPA
525.2
(95).
C) Solid Phase Extraction and Capillary
Column Gas Chromatography-Mass Spectrometry. USEPA
525.3
(12).
12) Di(2-ethylhexyl)phthalate
A) Liquid-Liquid or Liquid-Solid Extraction
and Gas Chromatography with Photoionization Detection. USEPA 506
(95).
B) Liquid-Solid Extraction
and Capillary Column Gas Chromatography-Mass Spectrometry. USEPA
525.2
(95).
C) Solid Phase Extraction and Capillary
Column Gas Chromatography-Mass Spectrometry. USEPA
525.3
(12).
13) Dinoseb
A) Liquid-Liquid Extraction Gas
Chromatography with Electron Capture Detector. USEPA
515.1 (89) or
USEPA 515.3(96).
B) Liquid-Solid Extraction Gas Chromatography
with Electron Capture Detector. USEPA
515.2
(95).
C) Liquid-Liquid Microextraction,
Derivatization, and Fast Gas Chromatography with Electron Capture Detector. SM
6640 B (01), SM 6640 B (06), or USEPA
515.4
(00).
D) High Performance Liquid Chromatography
with Photodiode Array Ultraviolet Detector. USEPA 555 (92).
14) Diquat. Liquid-Solid
Extraction and HPLC with Ultraviolet Detection. USEPA
549.2
(97).
15) Endothall. Ion-Exchange Extraction,
Acidic Methanol Methylation and Gas Chromatography/Mass Spectrometry. USEPA
548.1
(92).
16) Endrin
A) Microextraction and Gas Chromatography.
USEPA 505 (95)1.
B) Gas
Chromatography with Electron Capture Detector. USEPA 508 (95).
C) Liquid-Solid Extraction Gas Chromatography
with Electron Capture Detector. USEPA
508.1
(95).
D) Liquid-Solid Extraction and Capillary
Column Gas Chromatography-Mass Spectrometry. USEPA
525.2
(95).
E) Solid Phase Extraction and Capillary
Column Gas Chromatography-Mass Spectrometry. USEPA
525.3
(12).
F) Liquid-Liquid Extraction and Gas
Chromatography. USEPA
551.1
(95).
17) Ethylene Dibromide (EDB)
A) Microextraction and Gas Chromatography.
USEPA 504.1
(95).
B) Purge and Trap Gas Chromatography-Mass
Spectrometry. USEPA 524.3
(09).
C) Liquid-Liquid Extraction, Gas
Chromatography, Electron Capture Detector. USEPA
551.1
(95).
18) Glyphosate
A) Direct Aqueous Injection HPLC, Post-Column
Derivatization, and Fluorescence Detection. USEPA 547 (90).
B) Anion- or Cation-Exchange HPLC and
Post-Column Derivatization with Ultraviolet Fluorescence Detector. SM 6651 B
(91), SM 6651 B (96), SM 6651 B (00), or SM 6651 B (05).
19) Heptachlor
A) Microextraction and Gas Chromatography.
USEPA 505 (95)1.
B) Gas
Chromatography with Electron Capture Detector. USEPA 508 (95).
C) Liquid-Solid Extraction Gas Chromatography
with Electron Capture Detector. USEPA
508.1
(95).
D) Liquid-Solid Extraction and Capillary
Column Gas Chromatography-Mass Spectrometry. USEPA
525.2
(95).
E) Solid Phase Extraction and Capillary
Column Gas Chromatography-Mass Spectrometry. USEPA
525.3
(12).
F) Liquid-Liquid Extraction and Gas
Chromatography. USEPA
551.1
(95).
20) Heptachlor Epoxide
A) Microextraction and Gas Chromatography.
USEPA 505 (95)1.
B) Gas
Chromatography with Electron Capture Detector. USEPA 508 (95).
C) Liquid-Solid Extraction Gas Chromatography
with Electron Capture Detector. USEPA
508.1
(95).
D) Liquid-Solid Extraction and Capillary
Column Gas Chromatography-Mass Spectrometry. USEPA
525.2
(95).
E) Solid Phase Extraction and Capillary
Column Gas Chromatography-Mass Spectrometry. USEPA
525.3
(12).
F) Liquid-Liquid Extraction and Gas
Chromatography. USEPA
551.1
(95).
21) Hexachlorobenzene
A) Microextraction and Gas Chromatography.
USEPA 505 (95)1.
B) Gas
Chromatography with Electron Capture Detector. USEPA 508 (95).
C) Liquid-Solid Extraction Gas Chromatography
with Electron Capture Detector. USEPA
508.1
(95).
D) Liquid-Solid Extraction and Capillary
Column Gas Chromatography-Mass Spectrometry. USEPA
525.2
(95).
E) Solid Phase Extraction and Capillary
Column Gas Chromatography-Mass Spectrometry. USEPA
525.3
(12).
F) Liquid-Liquid Extraction and Gas
Chromatography. USEPA
551.1
(95).
22) Hexachlorocyclopentadiene
A) Microextraction and Gas Chromatography.
USEPA 505 (95)1.
B) Gas
Chromatography with Electron Capture Detector. USEPA 508 (95).
C) Liquid-Solid Extraction Gas Chromatography
with Electron Capture Detector. USEPA
508.1
(95).
D) Liquid-Solid Extraction and Capillary
Column Gas Chromatography-Mass Spectrometry. USEPA
525.2
(95).
E) Solid Phase Extraction and Capillary
Column Gas Chromatography-Mass Spectrometry. USEPA
525.3
(12).
F) Liquid-Liquid Extraction and Gas
Chromatography. USEPA
551.1
(95).
23) Lindane
A) Microextraction and Gas Chromatography.
USEPA 505 (95)1.
B) Gas
Chromatography with Electron Capture Detector. USEPA 508 (95).
C) Liquid-Solid Extraction Gas Chromatography
with Electron Capture Detector. USEPA
508.1
(95).
D) Liquid-Solid Extraction and Capillary
Column Gas Chromatography-Mass Spectrometry. USEPA
525.2
(95).
E) Solid Phase Extraction and Capillary
Column Gas Chromatography-Mass Spectrometry. USEPA
525.3
(12).
F) Liquid-Liquid Extraction and Gas
Chromatography. USEPA
551.1
(95).
24) Methoxychlor
A) Microextraction and Gas Chromatography.
USEPA 505 (95)1.
B) Gas
Chromatography with Electron Capture Detector. USEPA 508 (95).
C) Liquid-Solid Extraction Gas Chromatography
with Electron Capture Detector. USEPA
508.1
(95).
D) Gas Chromatography-Mass Spectrometry.
USEPA 525.2
(95).
E) Solid Phase Extraction and Capillary
Column Gas Chromatography-Mass Spectrometry. USEPA
525.3
(12).
F) Liquid-Liquid Extraction and Gas
Chromatography. USEPA
551.1
(95).
25) Oxamyl.
A) Direct Aqueous Injection HPLC with
Post-Column Derivatization. SM 6610 (92), 6610 (96), 6610 B (99), SM 6610 B
(04), USEPA 531.1 (95), or
USEPA 531.2
(01).
B) Liquid Chromatography/Mass Spectrometry.
ME 531 (19).
26) PCBs
(measured for compliance purposes as decachlorobiphenyl). Screening by
Perchlorination and Gas Chromatography. USEPA 508A (89).
27) PCBs (qualitatively identified as
alachlors)
A) Microextraction and Gas
Chromatography. USEPA 505 (95)1.
B)
Gas Chromatography with Electron Capture Detector. USEPA 508 (95).
C) Liquid-Solid Extraction Gas Chromatography
with Electron Capture Detector. USEPA
508.1
(95).
D) Gas Chromatography-Mass Spectrometry.
USEPA 525.2
(95).
E) Solid Phase Extraction and Capillary
Column Gas Chromatography-Mass Spectrometry. USEPA
525.3
(12).
28) Pentachlorophenol
A) Gas Chromatography with Electron Capture
Detector. ASTM D5317-93, ASTM D5317-98(2003), ASTM D5317-20, SM 6640 B (01), or
SM 6640 B (06).
B) Liquid-Liquid
Extraction Gas Chromatography with Electron Capture Detector. USEPA
515.1 (89) or
USEPA 515.3(96).
C) Liquid-Solid Extraction Gas Chromatography
with Electron Capture Detector. USEPA
515.2
(95).
D) Liquid-Liquid Microextraction,
Derivatization, and Fast Gas Chromatography with Electron Capture Detector.
USEPA 515.4
(00).
E) Gas Chromatography-Mass Spectrometry.
USEPA 525.2
(95).
F) Solid Phase Extraction and Capillary
Column Gas Chromatography-Mass Spectrometry. USEPA
525.3
(12).
G) High Performance Liquid Chromatography
with Photodiode Array Ultraviolet Detector. USEPA 555 (92).
29) Picloram
A) Gas Chromatography with Electron Capture
Detector. ASTM D5317-93, ASTM D5317-98(2003), ASTM D5317-20, SM 6640 B (01), or
SM 6640 B (06).
B) Liquid-Liquid
Extraction Gas Chromatography with Electron Capture Detector. USEPA
515.1 (89) or
USEPA 515.3
(96).
C) Liquid-Solid Extraction Gas Chromatography
with Electron Capture Detector. USEPA
515.2
(95).
D) Liquid-Liquid Microextraction,
Derivatization, and Fast Gas Chromatography with Electron Capture Detector.
USEPA 515.4
(00).
E) High Performance Liquid Chromatography
with Photodiode Array Ultraviolet Detector. USEPA 555 (92).
30) Simazine
A) Microextraction and Gas Chromatography.
USEPA 505 (95)1.
B) Gas
Chromatography with Electron Capture Detector. USEPA 507 (95).
C) Liquid-Solid Extraction Gas Chromatography
with Electron Capture Detector. USEPA
508.1
(95).
D) Liquid-Solid Extraction Gas Chromatography
with Electron Capture Detector. USEPA 523 (11).
E) Gas Chromatography-Mass Spectrometry.
USEPA 525.2
(95).
F) Solid Phase Extraction and Capillary
Column Gas Chromatography-Mass Spectrometry. USEPA
525.3
(12).
G) Liquid Chromatography Electrospray
Ionization Tandem Mass Spectrometry. USEPA 536 (07).
H) Liquid-Liquid Extraction and Gas
Chromatography. USEPA
551.1
(95).
31) Toxaphene
A) Microextraction and Gas Chromatography.
USEPA 505 (95)1.
B) Gas
Chromatography with Electron Capture Detector. USEPA 508 (95).
C) Liquid-Solid Extraction Gas Chromatography
with Electron Capture Detector. USEPA
508.1
(95).
D) Gas Chromatography-Mass Spectrometry.
USEPA 525.2
(95).
E) Solid Phase Extraction and Capillary
Column Gas Chromatography-Mass Spectrometry. USEPA
525.3
(12).
e) The following endnotes are appended to
method entries in subsections (a) and (b):
1 denotes that, for the particular
contaminant, the laboratory should substitute a nitrogen-phosphorus detector
for the electron capture detector in USEPA 505 (95) (or use another approved
method) to determine alachlor, atrazine, and simazine if it needs a lower
detection limit.
2 denotes that the laboratory may
not use Syngenta AG-625 (01) for atrazine in any system using chlorine dioxide
for treatment. In samples from all other systems, the laboratory must confirm
any result for atrazine using Syngenta AG-625 (01) that is greater than
one-half the maximum contaminant level (MCL) (in other words, greater than
0.0015 mg/L or
1.5
µg/L) using another
approved method and additional volume of the original sample the supplier
collected. If a result from Syngenta AG-625 (01) triggers confirmatory testing,
the supplier must use the confirmatory result to determine compliance.
BOARD NOTE: This Section derives from
40 CFR
141.24(e) and appendix A to
subpart C of 40 CFR
141. The Board did not separately list
approved alternative methods from Standard Methods Online that are the same
version as a method appearing in a printed edition of Standard Methods. Using
the Standard Methods Online copy is acceptable.
Standard Methods Online, Method 6610 B-04 appears in the
22nd and 23rd editions as
Method 6610 B. This appears in this Section as SM 6610 B (04).
Standard Methods Online, Method 6640 B-01 appears in the
21st edition as Method 6640 B. This appears in this
Section as SM 6640 B (01).
Standard Methods Online, Method 6640 B-06 appears in the
22nd and 23rd editions as
Method 6640 B. This appears in this Section as SM 6640 B (06).
Standard Methods Online, Method 6651 B-00 appears in the
21st edition as Method 6651 B. This appears in this
Section as SM 6651 B (00).
Standard Methods Online, Method 6651 B-05 appears in the
22nd and 23rd editions as
Method 6651 B. This appears in this Section as SM 6651 B (05).
BOARD NOTE: Derived from
40 CFR
141.24(e) and appendix A to
subpart C of 40 CFR 141 (2016).