California Code of Regulations
Title 8 - Industrial Relations
Division 1 - Department of Industrial Relations
Chapter 4 - Division of Industrial Safety
Subchapter 7 - General Industry Safety Orders
Group 16 - Control of Hazardous Substances
Article 110 - Regulated Carcinogens
Appendix E - Attachment B
Universal Citation: 8 CA Code of Regs E
Current through Register 2024 Notice Reg. No. 38, September 20, 2024
Instrumental Parameters for HGA Analysis
Atomic Absorption Spectrophotometer (Perkin-Elmer Model 5100)
Signal Type: | Zeeman AA | |
Slitwidth: | 0.7 nm | |
Wavelength: | 228.8 nm | |
Measurement: | Peak Area | |
Integration Time: | 6.0 sec | |
BOC Time: | 5 sec |
BOC = Background Offset Correction
Zeeman Graphite Furnace (Perkin-Elmer Model HGA-600)
Step |
Ramp Time (sec) |
Hold Time (sec) |
Temp. (°C) |
Argon Flow (mL/min) |
Read (sec) |
1)Predry | 5 | 10 | 90 | 300 | -- |
2)Dry | 30 | 10 | 140 | 300 | -- |
3)Char | 10 | 20 | 900 | 300 | -- |
4)Cool Down | 1 | 8 | 30 | 300 | -- |
5)Atomize | 0 | 5 | 1600 | 0 | -1 |
6)Burnout | 1 | 8 | 2500 | 300 | -- |
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