Expedited Approval of Alternative Test Procedures for the Analysis of Contaminants Under the Safe Drinking Water Act; Analysis and Sampling Procedures, 37463-37468 [C1-2013-12729]

Download as PDF 37463 Federal Register / Vol. 78, No. 120 / Friday, June 21, 2013 / Rules and Regulations EPA-APPROVED MISSOURI NONREGULATORY SIP PROVISIONS—Continued Applicable geographic or nonattainment area State submittal date (60) Section 128 Declaration: Missouri Air Conservation Commission Representation and Conflicts of Interest Provisions; Missouri Revised Statutes (RSMo) RSMo 105.450, RSMo 105.452, RSMo 105.454, RSMo 105.462, RSMo 105.463, RSMo 105.466, RSMo 105.472, and RSMo 643.040.2. Statewide .......... 8/08/2012 [FR Doc. 2013–14755 Filed 6–20–13; 8:45 am] ENVIRONMENTAL PROTECTION AGENCY issue of Friday, May 31, 2013, make the following correction: 40 CFR Part 141 PART 141—[CORRECTED] [EPA–HQ–OW–2013–0300; FRL–9818–2] Beginning on page 32570, with the table entitled ‘‘ALTERNATIVE TESTING METHODS FOR CONTAMINANTS LISTED AT 40 CFR 141.25(A)’’, the tables are corrected to read as set forth below: Name of non-regulatory SIP revision BILLING CODE 6560–50–P EPA approval date Explanation 6/21/2013 [INSERT CITATION OF PUBLICATION]. Expedited Approval of Alternative Test Procedures for the Analysis of Contaminants Under the Safe Drinking Water Act; Analysis and Sampling Procedures Correction In rule document 2013–12729, appearing on pages 32558–32574 in the ALTERNATIVE TESTING METHODS FOR CONTAMINANTS LISTED AT 40 CFR 141.25(a) Methodology SM 21st Edition 1 SM 22nd Edition 28 Evaporation ..................................................... Coprecipitation ................................................ Radon emanation ............................................ Radiochemical ................................................. Radiochemical ................................................. Radiochemical ................................................. ICP–MS ........................................................... Alpha spectrometry ......................................... Laser Phosphorimetry ..................................... Alpha Liquid Scintillation Spectrometry .......... 7110 B ................ 7110 C ................ 7500–Ra C .......... 7500–Ra B .......... 7500–Ra D .......... 7500–U B ............ 3125 .................... 7500–U C ............ ............................. ............................. 7110 B ................ 7110 C ................ 7500–Ra C .......... 7500–Ra B .......... 7500–Ra D .......... 7500–U B ............ ............................. 7500–U C ............ ............................. ............................. Radioactive Iodine ....................... Radiochemical ................................................. Gamma Ray Spectrometry ............................. Radiochemical ................................................. Radioactive Strontium 89, 90 ...... Tritium .......................................... Gamma Emitters ......................... Gamma Ray Spectrometry ............................. Radiochemical ................................................. Liquid Scintillation ........................................... Gamma Ray Spectrometry ............................. 7500–Cs B .......... 7120 .................... 7500–I B ............. 7500–I C ............. 7500–I D ............. 7120 .................... 7500–Sr B ........... 7500–3H B .......... 7120 .................... 7500–Cs B .......... 7500–I B ............. 7500–Cs B .......... 7120 .................... 7500–I B ............. 7500–I C ............. 7500–I D ............. 7120 .................... 7500–Sr B ........... 7500–3H B .......... 7120 .................... 7500–Cs B .......... 7500–I B ............. Contaminant Naturally Occurring: Gross alpha and beta .................. Gross alpha ................................. Radium 226 ................................. Radium 228 ................................. Uranium ....................................... Man-Made: Radioactive Cesium .................... ASTM 4 D3454–05 D2460–07 D5673–05, 10 D3972–09 D5174–07 D6239–09 D3649–06 D3649–06 D4785–08 D4107–08 D3649–06 D4785–08 ALTERNATIVE TESTING METHODS FOR CONTAMINANTS LISTED AT 40 CFR 141.74(a)(1) SM 21st Edition 1 TKELLEY on DSK3SPTVN1PROD with RULES Organism Methodology Total Coliform .............................. Total Coliform Fermentation Technique ......... Total Coliform Membrane Filter Technique .... ONPG–MUG Test ........................................... Fecal Coliform Procedure ............................... Fecal Coliform Filter Procedure ...................... Pour Plate Method .......................................... Nephelometric Method .................................... Fecal Coliforms ........................... Heterotrophic bacteria ................. Turbidity ....................................... VerDate Mar<15>2010 16:03 Jun 20, 2013 Jkt 229001 PO 00000 Frm 00027 Fmt 4700 Sfmt 4700 9221 9222 9223 9221 9222 9215 2130 A, B, C ....... A, B, C. .................... E ................ D ................ B ................ B ................ E:\FR\FM\21JNR1.SGM SM 22nd Edition 28 9221 A, B, C ....... 9223 9221 9222 9215 2130 B E D B B 21JNR1 ................ ................ ................ ................ ................ Other 37464 Federal Register / Vol. 78, No. 120 / Friday, June 21, 2013 / Rules and Regulations ALTERNATIVE TESTING METHODS FOR CONTAMINANTS LISTED AT 40 CFR 141.74(a)(1)—Continued Methodology SM 21st Edition 1 SM 22nd Edition 28 Laser Nephelometry (on-line) ......................... LED Nephelometry (on-line) ........................... LED Nephelometry (on-line) ........................... LED Nephelometry (portable) ......................... ............................. ............................. ............................. ............................. ............................. ............................. ............................. ............................. Organism Other Mitchell M5271 10 Mitchell M5331 11 AMI Turbiwell 15 Orion AQ4500 12 ALTERNATIVE TESTING METHODS FOR DISINFECTANT RESIDUALS LISTED AT 40 CFR 141.74(a)(2) Residual Methodology SM 21st Edition 1 Free Chlorine ............ Amperometric Titration .................................................. DPD Ferrous Titrimetric ................................................ DPD Colorimetric .......................................................... Syringaldazine (FACTS) ............................................... On-line Chlorine Analyzer ............................................. Amperometric Sensor ................................................... Amperometric Titration .................................................. Amperometric Titration (Low level measurement) ........ DPD Ferrous Titrimetric ................................................ DPD Colorimetric .......................................................... Iodometric Electrode ..................................................... On-line Chlorine Analyzer ............................................. Amperometric Sensor ................................................... Amperometric Titration .................................................. Amperometric Titration .................................................. Indigo Method ............................................................... 4500–Cl D ... 4500–Cl F ... 4500–Cl G ... 4500–Cl H ... ..................... ..................... 4500–Cl D ... 4500–Cl E ... 4500–Cl F ... 4500–Cl G ... 4500–Cl I ..... ..................... ..................... 4500–ClO2 C 4500–ClO2 E 4500–O3 B .. Total Chlorine ........... Chlorine Dioxide ....... Ozone ....................... SM 22nd Edition 28 ASTM 4 4500–Cl D ... D 1253–08. 4500–Cl F. 4500–Cl G. 4500–Cl H. ..................... ..................... ..................... ..................... 4500–Cl D ... D 1253–08. 4500–Cl E. 4500–Cl F. 4500–Cl G. 4500–Cl I. ..................... ..................... ..................... ..................... 4500–ClO2 C. 4500–ClO2 E. 4500–O3 B. Other EPA 334.0 16 ChloroSense 17 EPA 334.0 16 ChloroSense 17 ALTERNATIVE TESTING METHODS FOR CONTAMINANTS LISTED AT 40 CFR 141.131(b)(1) Contaminant Methodology EPA method ASTM 4 SM 21st Edition 1 TTHM ........................................................ P&T/GC/MS .................................. HAA5 ........................................................ LLE (diazomethane)/GC/ECD ....... Ion Chromatography Electrospray Ionization Tandem Mass Spectrometry (IC–ESI–MS/MS). Two-Dimensional Ion Chromatography (IC). Ion Chromatography Electrospray Ionization Tandem Mass Spectrometry (IC–ESI–MS/MS). Chemically Suppressed Ion Chromatography. Electrolytically Suppressed Ion Chromatography. Chemically Suppressed Ion Chromatography. Electrolytically Suppressed Ion Chromatography. Amperometric Titration .................. 524.3 9, 524.4 29. ..................... 557 14. ..................... 6251 B ......... 6251 B. 4500–ClO2 E 4500–ClO2 E. Bromate .................................................... Chlorite ..................................................... Chlorite—daily monitoring as prescribed in 40 CFR 141.132(b)(2)(i)(A). SM 22nd Edition 28 302.0 18. 557 14. ..................... D 6581–08 A. ..................... D 6581–08 B. ..................... D 6581–08 A. ..................... D 6581–08 B. ..................... ..................... ALTERNATIVE TESTING METHODS FOR DISINFECTANT RESIDUALS LISTED AT 40 CFR 141.131(c)(1) Methodology SM 21st Edition 1 SM 22nd Edition 28 Free Chlorine ............................... TKELLEY on DSK3SPTVN1PROD with RULES Residual Amperometric Titration .............................. DPD Ferrous Titrimetric ............................ DPD Colorimetric ....................................... Syringaldazine (FACTS) ............................ Amperometric Sensor ................................ On-line Chlorine Analyzer ......................... Amperometric Titration .............................. DPD Ferrous Titrimetric ............................ DPD Colorimetric ....................................... Amperometric Titration .............................. 4500–Cl D ... 4500–Cl F ... 4500–Cl G ... 4500–Cl H ... ..................... ..................... 4500–Cl D ... 4500–Cl F ... 4500–Cl G ... 4500–Cl D ... 4500–Cl D ... 4500–Cl F. 4500–Cl G. 4500–Cl H. ..................... ..................... 4500–Cl D ... 4500–Cl F. 4500–Cl G. 4500–Cl D ... Combined Chlorine ...................... Total Chlorine ............................... VerDate Mar<15>2010 16:40 Jun 20, 2013 Jkt 229001 PO 00000 Frm 00028 Fmt 4700 Sfmt 4700 E:\FR\FM\21JNR1.SGM 21JNR1 ASTM 4 Other D 1253–08. ..................... ..................... D 1253–08. D 1253–08. ChloroSense.17 EPA 334.0.16 37465 Federal Register / Vol. 78, No. 120 / Friday, June 21, 2013 / Rules and Regulations ALTERNATIVE TESTING METHODS FOR DISINFECTANT RESIDUALS LISTED AT 40 CFR 141.131(c)(1)—Continued Residual Methodology SM 21st Edition 1 SM 22nd Edition 28 Chlorine Dioxide ........................... Low level Amperometric Titration .............. DPD Ferrous Titrimetric ............................ DPD Colorimetric ....................................... Iodometric Electrode ................................. Amperometric Sensor ................................ On-line Chlorine Analyzer ......................... Amperometric Method II ............................ 4500–Cl E ... 4500–Cl F ... 4500–Cl G ... 4500–Cl I ..... ..................... ..................... 4500–ClO2 E 4500–Cl E. 4500–Cl F. 4500–Cl G. 4500–Cl I. ..................... ..................... 4500–ClO2 E. * * * * ASTM 4 Other ..................... ..................... ChloroSense.17 EPA 334.0.16 * ALTERNATIVE TESTING METHODS FOR PARAMETERS LISTED AT 40 CFR 141.131(d) Parameter Methodology SM 21st Edition 1 SM 22nd Edition 28 Total Organic Carbon (TOC) ...................... High Temperature Combustion ................... Persulfate-Ultraviolet or Heated Persulfate Oxidation. Wet Oxidation ............................................. Calculation using DOC and UV254 data ...... High Temperature Combustion ................... Persulfate-Ultraviolet or Heated Persulfate Oxidation. Wet Oxidation ............................................. Spectrophotometry ...................................... 5310 B ......... 5310 C ........ 5310 B ........ 5310 C ........ 415.3, Rev 1.2 19 415.3, Rev 1.2 19 5310 D ........ ..................... 5310 B ........ 5310 C ........ 5310 D ........ ..................... 5310 B ........ 5310 C ........ 415.3, 415.3, 415.3, 415.3, 5310 D ........ 5910 B ......... 5310 D ........ 5910 B ........ 415.3, Rev 1.2 19 415.3, Rev 1.2 19 Specific Ultraviolet Absorbance (SUVA) ..... Dissolved Organic Carbon (DOC) ....... Ultraviolet absorption at 254 nm (UV254) .... * * * * EPA Rev Rev Rev Rev 1.2 19 1.2 19 1.2 19 1.2 19 * ALTERNATIVE TESTING METHODS FOR CONTAMINANTS LISTED AT 40 CFR 141.402(c)(2) Organism Methodology SM 20th Edition 6 SM 21st Edition 1 SM 22nd Edition 28 SM Online 3 E. coli ........................................ Colilert® .................................... Colisure® .................................. Colilert-18 ................................. Readycult® ................................ ..................... ..................... 9223 B ........ ..................... 9223 B ........ 9223 B ........ 9223 B ......... ..................... 9223 B ......... 9223 B ........ 9223 B ........ ..................... 9223 B–97. 9223 B–97. 9223 B–97. ..................... Colitag ....................................... ..................... ..................... ..................... ..................... Chromocult® ............................. ..................... ..................... ..................... ..................... EC–MUG .................................. Multiple-Tube Technique .......... Two-Step Enrichment Presence-Absence Procedure. ..................... ..................... ..................... ..................... ..................... ..................... 9221 F. ..................... ..................... 9230 B–04. ..................... Enterococci ............................... Coliphage .................................. * * * * Other Ready cult® 20 Modified ColitagTM 13 Chromo cult® 21 Fast Phage 30 * ALTERNATIVE TESTING METHODS FOR CONTAMINANTS LISTED AT 40 CFR 141.852(a)(5) SM 22nd Edition 28 Organism Methodology category Method Total Coliforms ..................................... Lactose Fermentation Methods ........... Standard Total Coliform Fermentation Technique. Colilert® ............................................... Colisure® ............................................. EC–MUG medium ............................... 9223 B 9223 B 9221 F.1 Colilert® ............................................... Colisure® ............................................. 9223 B 9223 B TKELLEY on DSK3SPTVN1PROD with RULES Enzyme Substrate Methods ................ Escherichia coli .................................... VerDate Mar<15>2010 17:22 Jun 20, 2013 Escherichia coli Procedure (following Lactose Fermentation Methods). Enzyme Substrate Methods ................ Jkt 229001 PO 00000 Frm 00029 Fmt 4700 Sfmt 4700 E:\FR\FM\21JNR1.SGM 21JNR1 9221 B.1, B.2 37466 Federal Register / Vol. 78, No. 120 / Friday, June 21, 2013 / Rules and Regulations ALTERNATIVE TESTING METHODS FOR CONTAMINANTS LISTED AT 40 CFR 143.4(b) ASTM 4 SM 21st Edition 1 .................................... ......................... 3111 D ............ 3111 D. .................................... ......................... 3113 B ............ 3113 B ............ .................................... ......................... 3120 B ............ 3120 B. .................................... .................................... .................................... D 512–04 B .... ......................... ......................... 4500-Cl- B ....... 4110 B ............ 4500-Cl D .. 4500-Cl- B. 4110 B. 4500-Cl D. .................................... .................................... ......................... ......................... 2120 B ............ 5540 C ............ 2120 B. 5540 C. .................................... ......................... 3111 B ............ 3111 B. .................................... ......................... 3113 B ............ 3113 B ............ .................................... ......................... 3120 B ............ 3120 B. .................................... ......................... 3111 B ............ 3111 B. .................................... ......................... 3113 B ............ 3113 B ............ .................................... ......................... 3120 B ............ 3120 B. .................................... 200.5, Revision 4.2 2 ......................... 2150 B ............ 2150 B. .................................... ......................... 3111 B ............ 3111 B. .................................... ......................... 3113 B ............ 3113 B ............ .................................... ......................... 3120 B ............ 3120 B. .................................... .................................... ......................... ......................... .................................... ......................... .................................... D 516–07, 11 .. .................................... ......................... 4110 B ............ 4500–SO4 2¥ C. 4500–SO4 2¥ D. 4500–SO4 2¥ E. 4500–SO4 2¥ F 4110 B. 4500–SO4 C. 4500–SO4 D. 4500–SO4 E. 4500–SO4 .................................... ......................... 2540 C ............ 2540 C. ......................... 3111 B ............ 3111 B. Contaminant Methodology Aluminum ............ Axially viewed inductively coupled plasma-atomic emission spectrometry (AVICP–AES). Atomic Absorption; Direct. Atomic Absorption; Furnace. Inductively Coupled Plasma. Silver Nitrate Titration Ion Chromatography .. Potentiometric Titration. Visual Comparison ..... Methylene Blue Active Substances (MBAS). Axially viewed inductively coupled plasma-atomic emission spectrometry (AVICP–AES). Atomic Absorption; Direct. Atomic Absorption; Furnace. Inductively Coupled Plasma. Axially viewed inductively coupled plasma-atomic emission spectrometry (AVICP–AES). Atomic Absorption; Direct. Atomic Absorption; Furnace. Inductively Coupled Plasma. Threshold Odor Test .. Axially viewed inductively coupled plasma-atomic emission spectrometry (AVICP–AES). Atomic Absorption; Direct. Atomic Absorption; Furnace. Inductively Coupled Plasma. Ion Chromatography .. Gravimetric with ignition of residue. Gravimetric with drying of residue. Turbidimetric method Automated methylthymol blue method. Total Dissolved Solids Dried at 180 deg C. Axially viewed inductively coupled plasma-atomic emission spectrometry (AVICP–AES). Atomic Absorption; Direct Aspiration. Color ................... Foaming Agents .. Iron ...................... Manganese ......... Odor .................... Silver ................... Sulfate ................. TKELLEY on DSK3SPTVN1PROD with RULES SM 22nd Edition 28 SM online 3 200.5, Revision 4.22 Chloride ............... Total Dissolved Solids. Zinc ..................... VerDate Mar<15>2010 17:14 Jun 20, 2013 Jkt 229001 EPA method 200.5, Revision 4.2 200.5, Revision 4.2 200.5, Revision 4.2 2 Frm 00030 3113 B–04 2 2 .................................... PO 00000 3113 B–04 Fmt 4700 Sfmt 4700 E:\FR\FM\21JNR1.SGM 21JNR1 3113 B–04 3113 B–04 2¥ 4500–SO4 2¥ C–97 2¥ 4500–SO4 2¥ D–97 2¥ 4500–SO4 2¥ E–97 4500–SO4 2¥ F–97 2¥ F 37467 Federal Register / Vol. 78, No. 120 / Friday, June 21, 2013 / Rules and Regulations ALTERNATIVE TESTING METHODS FOR CONTAMINANTS LISTED AT 40 CFR 143.4(b)—Continued Contaminant Methodology Inductively Coupled Plasma. EPA method ASTM 4 SM 21st Edition 1 .................................... ......................... 3120 B ............ SM 22nd Edition 28 SM online 3 3120 B. TKELLEY on DSK3SPTVN1PROD with RULES 1 Standard Methods for the Examination of Water and Wastewater, 21st edition (2005). Available from American Public Health Association, 800 I Street NW., Washington, DC 20001–3710. 2 EPA Method 200.5, Revision 4.2. ‘‘Determination of Trace Elements in Drinking Water by Axially Viewed Inductively Coupled Plasma-Atomic Emission Spectrometry.’’ 2003. EPA/600/R–06/115. (Available at https://www.epa.gov/nerlcwww/ordmeth.htm.) 3 Standard Methods Online are available at https://www.standardmethods.org. The year in which each method was approved by the Standard Methods Committee is designated by the last two digits in the method number. The methods listed are the only online versions that may be used. 4 Available from ASTM International, 100 Barr Harbor Drive, West Conshohocken, PA 19428–2959 or https://astm.org. The methods listed are the only alternative versions that may be used. * * * * * * * 6 Standard Methods for the Examination of Water and Wastewater, 20th edition (1998). Available from American Public Health Association, 800 I Street NW., Washington, DC 20001–3710. 7 Method ME355.01, Revision 1.0. ‘‘Determination of Cyanide in Drinking Water by GC/MS Headspace,’’ May 26, 2009. Available at https:// www.nemi.gov or from James Eaton, H & E Testing Laboratory, 221 State Street, Augusta, ME 04333. (207) 287–2727. 8 Systea Easy (1-Reagent). ‘‘Systea Easy (1-Reagent) Nitrate Method,’’ February 4, 2009. Available at https://www.nemi.gov or from Systea Scientific, LLC., 900 Jorie Blvd., Suite 35, Oak Brook, IL 60523. 9 EPA Method 524.3, Version 1.0. ‘‘Measurement of Purgeable Organic Compounds in Water by Capillary Column Gas Chromatography/Mass Spectrometry,’’ June 2009. EPA 815–B–09–009. Available at https://water.epa.gov/drink/. 10 Mitchell Method M5271, Revision 1.1. ‘‘Determination of Turbidity by Laser Nephelometry,’’ March 5, 2009. Available at https://www.nemi.gov or from Leck Mitchell, Ph.D., PE, 656 Independence Valley Dr., Grand Junction, CO 81507. 11 Mitchell Method M5331, Revision 1.1. ‘‘Determination of Turbidity by LED Nephelometry,’’ March 5, 2009. Available at https://www.nemi.gov or from Leck Mitchell, Ph.D., PE, 656 Independence Valley Dr., Grand Junction, CO 81507. 12 Orion Method AQ4500, Revision 1.0. ‘‘Determination of Turbidity by LED Nephelometry,’’ May 8, 2009. Available at https://www.nemi.gov or from Thermo Scientific, 166 Cummings Center, Beverly, MA 01915, https://www.thermo.com. 13 Modified Colitag TM Method. ‘‘Modified Colitag TM Test Method for the Simultaneous Detection of E. coli and other Total Coliforms in Water (ATP D05–0035),’’ August 28, 2009. Available at https://www.nemi.gov or from CPI International, 5580 Skylane Boulevard, Santa Rosa, CA 95403. 14 EPA Method 557. ‘‘Determination of Haloacetic Acids, Bromate, and Dalapon in Drinking Water by Ion Chromatography Electrospray Ionization Tandem Mass Spectrometry (IC–ESI–MS/MS),’’ September 2009. EPA 815–B–09–012. Available at https://water.epa.gov/drink/. 15 AMI Turbiwell, ‘‘Continuous Measurement of Turbidity Using a SWAN AMI Turbiwell Turbidimeter,’’ August 2009. Available at https:// www.nemi.gov or from Markus Bernasconi, SWAN Analytische Instrumente AG, Studbachstrasse 13, CH–8340 Hinwil, Switzerland. 16 EPA Method 334.0. ‘‘Determination of Residual Chlorine in Drinking Water Using an On-line Chlorine Analyzer,’’ September 2009. EPA 815– B–09–013. Available at https://water.epa.gov/drink/. 17 ChloroSense. ‘‘Measurement of Free and Total Chlorine in Drinking Water by Palintest ChloroSense,’’ August 2009. Available at https:// www.nemi.gov or from Palintest Ltd., 21 Kenton Lands Road, P.O. Box 18395, Erlanger, KY 41018. 18 EPA Method 302.0. ‘‘Determination of Bromate in Drinking Water using Two-Dimensional Ion Chromatography with Suppressed Conductivity Detection,’’ September 2009. EPA 815–B–09–014. Available at https://water.epa.gov/drink/. 19 EPA 415.3, Revision 1.2. ‘‘Determination of Total Organic Carbon and Specific UV Absorbance at 254 nm in Source Water and Drinking Water,’’ September 2009. EPA/600/R–09/122. Available at https://www.epa.gov/nerlcwww/ordmeth.htm. 20 Readycult® Method, ‘‘Readycult® Coliforms 100 Presence/Absence Test for Detection and Identification of Coliform Bacteria and Escherichia coli in Finished Waters,’’ January, 2007. Version 1.1. Available from EMD Millipore (division of Merck KGaA, Darmstadt, Germany), 290 Concord Road, Billerica, MA 01821. 21 Chromocult® Method, ‘‘Chromocult® Coliform Agar Presence/Absence Membrane Filter Test Method for Detection and Identification of Coliform Bacteria and Escherichia coli in Finished Waters,’’ November, 2000. Version 1.0. EMD Millipore (division of Merck KGaA, Darmstadt, Germany), 290 Concord Road, Billerica, MA 01821. 22 Hach Company. ‘‘Hach Company SPADNS 2 (Arsenite-Free) Fluoride Method 10225—Spectrophotometric Measurement of Fluoride in Water and Wastewater,’’ January 2011. 5600 Lindbergh Drive, P.O. Box 389, Loveland, Colorado 80539. (Available at https://www.hach.com.) 23 Hach Company. ‘‘Hach Company TNTplusTM 835/836 Nitrate Method 10206—Measurement of Nitrate in Water and Wastewater,’’ January 2011. 5600 Lindbergh Drive, P.O. Box 389, Loveland, Colorado. (Available at https://www.hach.com.) 24 EPA Method 525.3. ‘‘Determination of Semivolatile Organic Chemicals in Drinking Water by Solid Phase Extraction and Capillary Column Gas Chromatography/Mass Spectrometry (GC/MS),’’ February 2012. EPA/600/R–12/010. Available at https://www.epa.gov/nerlcwww/ordmeth.htm. 25 EPA Method 536. ‘‘Determination of Triazine Pesticides and their Degradates in Drinking Water by Liquid Chromatography Electrospray Ionization Tandem Mass Spectrometry (LC/ESI–MS/MS),’’ October 2007. EPA 815–B–07–002. Available at https://water.epa.gov/drink. 26 EPA Method 523. ‘‘Determination of Triazine Pesticides and their Degradates in Drinking Water by Gas Chromatography/Mass Spectrometry (GC/MS),’’ February 2011. EPA 815–R–11–002. Available at https://water.epa.gov/drink. 27 EPA Method 1623.1. ‘‘Cryptosporidium and Giardia in Water by Filtration/IMS/FA,’’ 2012. EPA–816–R–12–001. (Available at https:// water.epa.gov/drink.) 28 Standard Methods for the Examination of Water and Wastewater, 22nd edition (2012). Available from American Public Health Association, 800 I Street NW., Washington, DC 20001–3710. 29 EPA Method 524.4, Version 1.0. ‘‘Measurement of Purgeable Organic Compounds in Water by Gas Chromatography/Mass Spectrometry using Nitrogen Purge Gas,’’ May 2013. EPA 815–R–13–002. Available at https://water.epa.gov/drink. 30 Charm Sciences Inc. ‘‘Fast Phage Test Procedure. Presence/Absence for Coliphage in Ground Water with Same Day Positive Prediction’’. Version 009. November 2012. 659 Andover Street, Lawrence, MA 01843. Available at www.charmsciences.com. VerDate Mar<15>2010 17:22 Jun 20, 2013 Jkt 229001 PO 00000 Frm 00031 Fmt 4700 Sfmt 4700 E:\FR\FM\21JNR1.SGM 21JNR1 37468 Federal Register / Vol. 78, No. 120 / Friday, June 21, 2013 / Rules and Regulations [FR Doc. C1–2013–12729 Filed 6–20–13; 8:45 am] BILLING CODE 1505–01–D ENVIRONMENTAL PROTECTION AGENCY 40 CFR Part 180 [EPA–HQ–OPP–2012–0177; FRL–9387–3] Cyproconazole; Pesticide Tolerances Environmental Protection Agency (EPA). ACTION: Final rule. AGENCY: This regulation establishes tolerances for residues of cyproconazole in or on peanut and peanut, hay. Syngenta Crop Protection, LLC. requested these tolerances under the Federal Food, Drug, and Cosmetic Act (FFDCA). SUMMARY: This regulation is effective June 21, 2013. Objections and requests for hearings must be received on or before August 20, 2013, and must be filed in accordance with the instructions provided in 40 CFR part 178 (see also Unit I.C. of the SUPPLEMENTARY INFORMATION). DATES: The docket for this action, identified by docket identification (ID) number EPA–HQ–OPP–2012–0177, is available at https://www.regulations.gov or at the Office of Pesticide Programs Regulatory Public Docket (OPP Docket) in the Environmental Protection Agency Docket Center (EPA/DC), EPA West Bldg., Rm. 3334, 1301 Constitution Ave. NW., Washington, DC 20460–0001. The Public Reading Room is open from 8:30 a.m. to 4:30 p.m., Monday through Friday, excluding legal holidays. The telephone number for the Public Reading Room is (202) 566–1744, and the telephone number for the OPP Docket is (703) 305–5805. Please review the visitor instructions and additional information about the docket available at https://www.epa.gov/dockets. FOR FURTHER INFORMATION CONTACT: Shaunta Hill, Registration Division (7505P), Office of Pesticide Programs, Environmental Protection Agency, 1200 Pennsylvania Ave. NW., Washington, DC 20460–0001; telephone number: (703) 347–8961; email address: hill.shaunta@epa.gov. ADDRESSES: TKELLEY on DSK3SPTVN1PROD with RULES SUPPLEMENTARY INFORMATION: I. General Information A. Does this action apply to me? You may be potentially affected by this action if you are an agricultural producer, food manufacturer, or pesticide manufacturer. The following VerDate Mar<15>2010 16:03 Jun 20, 2013 Jkt 229001 list of North American Industrial Classification System (NAICS) codes is not intended to be exhaustive, but rather provides a guide to help readers determine whether this document applies to them. Potentially affected entities may include: • Crop production (NAICS code 111). • Animal production (NAICS code 112). • Food manufacturing (NAICS code 311). • Pesticide manufacturing (NAICS code 32532). B. How can I get electronic access to other related information? You may access a frequently updated electronic version of EPA’s tolerance regulations at 40 CFR part 180 through the Government Printing Office’s eCFR site at https://www.ecfr.gov/cgi-bin/textidx?&c=ecfr&tpl=/ecfrbrowse/Title40/ 40tab_02.tpl. To access the OCSPP test guidelines referenced in this document electronically, please go to https:// www.epa.gov/ocspp and select ‘‘Test Methods and Guidelines.’’ C. How can I file an objection or hearing request? Under FFDCA section 408(g), 21 U.S.C. 346a, any person may file an objection to any aspect of this regulation and may also request a hearing on those objections. You must file your objection or request a hearing on this regulation in accordance with the instructions provided in 40 CFR part 178. To ensure proper receipt by EPA, you must identify docket ID number EPA–HQ– OPP–2012–0177 in the subject line on the first page of your submission. All objections and requests for a hearing must be in writing, and must be received by the Hearing Clerk on or before August 20, 2013. Addresses for mail and hand delivery of objections and hearing requests are provided in 40 CFR 178.25(b). In addition to filing an objection or hearing request with the Hearing Clerk as described in 40 CFR part 178, please submit a copy of the filing (excluding any Confidential Business Information (CBI)) for inclusion in the public docket. Information not marked confidential pursuant to 40 CFR part 2 may be disclosed publicly by EPA without prior notice. Submit the non-CBI copy of your objection or hearing request, identified by docket ID number EPA–HQ–OPP– 2012–0177, by one of the following methods: • Federal eRulemaking Portal: https:// www.regulations.gov. Follow the online instructions for submitting comments. Do not submit electronically any information you consider to be CBI or PO 00000 Frm 00032 Fmt 4700 Sfmt 4700 other information whose disclosure is restricted by statute. • Mail: OPP Docket, Environmental Protection Agency Docket Center (EPA/ DC), (28221T), 1200 Pennsylvania Ave. NW., Washington, DC 20460–0001. • Hand Delivery: To make special arrangements for hand delivery or delivery of boxed information, please follow the instructions at https:// www.epa.gov/dockets/contacts.htm. Additional instructions on commenting or visiting the docket, along with more information about dockets generally, is available at https://www.epa.gov/ dockets. II. Summary of Petitioned-for Tolerance In the Federal Register of May 23, 2012 (77 FR 30481) (FRL–9347–8), EPA issued a document pursuant to FFDCA section 408(d)(3), 21 U.S.C. 346a(d)(3), announcing the filing of a pesticide petition (PP 1F7956) by Syngenta Crop Protection, LLC., P.O. Box 18300, Greensboro, NC 24719. The petition requested that 40 CFR 180.485 be amended by establishing tolerances for residues of the fungicide cyproconazole, in or on peanut, hay at 6.0 parts per million (ppm), and peanut, nutmeat; peanut, meal; peanut, butter; and peanut, refined oil at 0.03 ppm. That document referenced a summary of the petition prepared by Syngenta Crop Protection, the registrant, which is available in the docket, https:// www.regulations.gov. There were no substantive comments received in response to the notice of filing. Based upon review of the data supporting the petition, EPA has modified the requested tolerance levels and crops for which tolerances were needed. The reasons for these changes are explained in Unit IV.C. III. Aggregate Risk Assessment and Determination of Safety Section 408(b)(2)(A)(i) of FFDCA allows EPA to establish a tolerance (the legal limit for a pesticide chemical residue in or on a food) only if EPA determines that the tolerance is ‘‘safe.’’ Section 408(b)(2)(A)(ii) of FFDCA defines ‘‘safe’’ to mean that ‘‘there is a reasonable certainty that no harm will result from aggregate exposure to the pesticide chemical residue, including all anticipated dietary exposures and all other exposures for which there is reliable information.’’ This includes exposure through drinking water and in residential settings, but does not include occupational exposure. Section 408(b)(2)(C) of FFDCA requires EPA to give special consideration to exposure of infants and children to the pesticide chemical residue in establishing a E:\FR\FM\21JNR1.SGM 21JNR1

Agencies

[Federal Register Volume 78, Number 120 (Friday, June 21, 2013)]
[Rules and Regulations]
[Pages 37463-37468]
From the Federal Register Online via the Government Printing Office [www.gpo.gov]
[FR Doc No: C1-2013-12729]


-----------------------------------------------------------------------

ENVIRONMENTAL PROTECTION AGENCY

40 CFR Part 141

[EPA-HQ-OW-2013-0300; FRL-9818-2]


Expedited Approval of Alternative Test Procedures for the 
Analysis of Contaminants Under the Safe Drinking Water Act; Analysis 
and Sampling Procedures

Correction

    In rule document 2013-12729, appearing on pages 32558-32574 in the 
issue of Friday, May 31, 2013, make the following correction:

PART 141--[CORRECTED]

    Beginning on page 32570, with the table entitled ``ALTERNATIVE 
TESTING METHODS FOR CONTAMINANTS LISTED AT 40 CFR 141.25(A)'', the 
tables are corrected to read as set forth below:

                     Alternative Testing Methods for Contaminants Listed at 40 CFR 141.25(a)
----------------------------------------------------------------------------------------------------------------
                                                          SM 21st Edition    SM 22nd  Edition
          Contaminant                  Methodology              \1\                \28\             ASTM \4\
----------------------------------------------------------------------------------------------------------------
Naturally Occurring:
Gross alpha and beta...........  Evaporation...........  7110 B...........  7110 B...........  .................
Gross alpha....................  Coprecipitation.......  7110 C...........  7110 C...........  .................
Radium 226.....................  Radon emanation.......  7500-Ra C........  7500-Ra C........  D3454-05
                                 Radiochemical.........  7500-Ra B........  7500-Ra B........  D2460-07
Radium 228.....................  Radiochemical.........  7500-Ra D........  7500-Ra D........  .................
Uranium........................  Radiochemical.........  7500-U B.........  7500-U B.........  .................
                                 ICP-MS................  3125.............  .................  D5673-05, 10
                                 Alpha spectrometry....  7500-U C.........  7500-U C.........  D3972-09
                                 Laser Phosphorimetry..  .................  .................  D5174-07
                                 Alpha Liquid            .................  .................  D6239-09
                                  Scintillation
                                  Spectrometry.
Man-Made:
Radioactive Cesium.............  Radiochemical.........  7500-Cs B........  7500-Cs B........  .................
                                 Gamma Ray Spectrometry  7120.............  7120.............  D3649-06
Radioactive Iodine.............  Radiochemical.........  7500-I B.........  7500-I B.........  D3649-06
                                                         7500-I C.........  7500-I C.........  .................
                                                         7500-I D.........  7500-I D.........  .................
                                 Gamma Ray Spectrometry  7120.............  7120.............  D4785-08
Radioactive Strontium 89, 90...  Radiochemical.........  7500-Sr B........  7500-Sr B........  .................
Tritium........................  Liquid Scintillation..  7500-\3\H B......  7500-\3\H B......  D4107-08
Gamma Emitters.................  Gamma Ray Spectrometry  7120.............  7120.............  D3649-06
                                                         7500-Cs B........  7500-Cs B........  D4785-08
                                                         7500-I B.........  7500-I B.........  .................
----------------------------------------------------------------------------------------------------------------


                   Alternative Testing Methods for Contaminants Listed at 40 CFR 141.74(a)(1)
----------------------------------------------------------------------------------------------------------------
                                                          SM 21st Edition    SM 22nd  Edition
            Organism                   Methodology              \1\                \28\              Other
----------------------------------------------------------------------------------------------------------------
Total Coliform.................  Total Coliform          9221 A, B, C.....  9221 A, B, C.....  .................
                                  Fermentation
                                  Technique.
                                 Total Coliform          9222 A, B, C.....
                                  Membrane Filter
                                  Technique.
                                 ONPG-MUG Test.........  9223.............  9223 B...........  .................
Fecal Coliforms................  Fecal Coliform          9221 E...........  9221 E...........  .................
                                  Procedure.
                                 Fecal Coliform Filter   9222 D...........  9222 D...........  .................
                                  Procedure.
Heterotrophic bacteria.........  Pour Plate Method.....  9215 B...........  9215 B...........  .................
Turbidity......................  Nephelometric Method..  2130 B...........  2130 B...........  .................

[[Page 37464]]

 
                                 Laser Nephelometry (on- .................  .................  Mitchell M5271
                                  line).                                                        \10\
                                 LED Nephelometry (on-   .................  .................  Mitchell M5331
                                  line).                                                        \11\
                                 LED Nephelometry (on-   .................  .................  AMI Turbiwell
                                  line).                                                        \15\
                                 LED Nephelometry        .................  .................  Orion AQ4500 \12\
                                  (portable).
----------------------------------------------------------------------------------------------------------------


                                  Alternative Testing Methods for Disinfectant Residuals Listed at 40 CFR 141.74(a)(2)
--------------------------------------------------------------------------------------------------------------------------------------------------------
             Residual                    Methodology       SM 21st  Edition \1\   SM 22nd Edition \28\         ASTM \4\                  Other
--------------------------------------------------------------------------------------------------------------------------------------------------------
Free Chlorine.....................  Amperometric          4500-Cl D............  4500-Cl D............  D 1253-08............
                                     Titration.
                                    DPD Ferrous           4500-Cl F............  4500-Cl F............
                                     Titrimetric.
                                    DPD Colorimetric....  4500-Cl G............  4500-Cl G............
                                    Syringaldazine        4500-Cl H............  4500-Cl H............
                                     (FACTS).
                                    On-line Chlorine      .....................  .....................  .....................  EPA 334.0 \16\
                                     Analyzer.
                                    Amperometric Sensor.  .....................  .....................  .....................  ChloroSense \17\
Total Chlorine....................  Amperometric          4500-Cl D............  4500-Cl D............  D 1253-08............
                                     Titration.
                                    Amperometric          4500-Cl E............  4500-Cl E............
                                     Titration (Low
                                     level measurement).
                                    DPD Ferrous           4500-Cl F............  4500-Cl F............
                                     Titrimetric.
                                    DPD Colorimetric....  4500-Cl G............  4500-Cl G............
                                    Iodometric Electrode  4500-Cl I............  4500-Cl I............
                                    On-line Chlorine      .....................  .....................  .....................  EPA 334.0 \16\
                                     Analyzer.
                                    Amperometric Sensor.  .....................  .....................  .....................  ChloroSense \17\
Chlorine Dioxide..................  Amperometric          4500-ClO2 C..........  4500-ClO2 C..........
                                     Titration.
                                    Amperometric          4500-ClO2 E..........  4500-ClO2 E..........
                                     Titration.
Ozone.............................  Indigo Method.......  4500-O3 B............  4500-O3 B............
--------------------------------------------------------------------------------------------------------------------------------------------------------


                                       Alternative Testing Methods for Contaminants Listed at 40 CFR 141.131(b)(1)
--------------------------------------------------------------------------------------------------------------------------------------------------------
            Contaminant                  Methodology            EPA method              ASTM \4\         SM 21st  Edition \1\    SM 22nd  Edition \28\
--------------------------------------------------------------------------------------------------------------------------------------------------------
TTHM..............................  P&T/GC/MS...........  524.3 \9\,
                                                          524.4 \29\...........
HAA5..............................  LLE (diazomethane)/   .....................  .....................  6251 B...............  6251 B.
                                     GC/ECD.
                                    Ion Chromatography    557 \14\.............
                                     Electrospray
                                     Ionization Tandem
                                     Mass Spectrometry
                                     (IC-ESI-MS/MS).
Bromate...........................  Two-Dimensional Ion   302.0 \18\...........
                                     Chromatography (IC).
                                    Ion Chromatography    557 \14\.............
                                     Electrospray
                                     Ionization Tandem
                                     Mass Spectrometry
                                     (IC-ESI-MS/MS).
                                    Chemically            .....................  D 6581-08 A..........
                                     Suppressed Ion
                                     Chromatography.
                                    Electrolytically      .....................  D 6581-08 B..........
                                     Suppressed Ion
                                     Chromatography.
Chlorite..........................  Chemically            .....................  D 6581-08 A..........
                                     Suppressed Ion
                                     Chromatography.
                                    Electrolytically      .....................  D 6581-08 B..........
                                     Suppressed Ion
                                     Chromatography.
Chlorite--daily monitoring as       Amperometric          .....................  .....................  4500-ClO2 E..........  4500-ClO2 E.
 prescribed in 40 CFR                Titration.
 141.132(b)(2)(i)(A).
--------------------------------------------------------------------------------------------------------------------------------------------------------


                                  Alternative Testing Methods for Disinfectant Residuals Listed at 40 CFR 141.131(c)(1)
--------------------------------------------------------------------------------------------------------------------------------------------------------
             Residual                    Methodology       SM 21st  Edition \1\  SM 22nd  Edition \28\         ASTM \4\                  Other
--------------------------------------------------------------------------------------------------------------------------------------------------------
Free Chlorine.....................  Amperometric          4500-Cl D............  4500-Cl D............  D 1253-08............
                                     Titration.
                                    DPD Ferrous           4500-Cl F............  4500-Cl F............
                                     Titrimetric.
                                    DPD Colorimetric....  4500-Cl G............  4500-Cl G............
                                    Syringaldazine        4500-Cl H............  4500-Cl H............
                                     (FACTS).
                                    Amperometric Sensor.  .....................  .....................  .....................  ChloroSense.\17\
                                    On-line Chlorine      .....................  .....................  .....................  EPA 334.0.\16\
                                     Analyzer.
Combined Chlorine.................  Amperometric          4500-Cl D............  4500-Cl D............  D 1253-08............
                                     Titration.
                                    DPD Ferrous           4500-Cl F............  4500-Cl F............
                                     Titrimetric.
                                    DPD Colorimetric....  4500-Cl G............  4500-Cl G............
Total Chlorine....................  Amperometric          4500-Cl D............  4500-Cl D............  D 1253-08............
                                     Titration.

[[Page 37465]]

 
                                    Low level             4500-Cl E............  4500-Cl E............
                                     Amperometric
                                     Titration.
                                    DPD Ferrous           4500-Cl F............  4500-Cl F............
                                     Titrimetric.
                                    DPD Colorimetric....  4500-Cl G............  4500-Cl G............
                                    Iodometric Electrode  4500-Cl I............  4500-Cl I............
                                    Amperometric Sensor.  .....................  .....................  .....................  ChloroSense.\17\
                                    On-line Chlorine      .....................  .....................  .....................  EPA 334.0.\16\
                                     Analyzer.
Chlorine Dioxide..................  Amperometric Method   4500-ClO2 E..........  4500-ClO2 E..........
                                     II.
--------------------------------------------------------------------------------------------------------------------------------------------------------

* * * * *

                     Alternative Testing Methods for Parameters Listed at 40 CFR 141.131(d)
----------------------------------------------------------------------------------------------------------------
                                                  SM 21st  Edition  SM 22nd  Edition
          Parameter               Methodology           \1\               \28\                    EPA
----------------------------------------------------------------------------------------------------------------
Total Organic Carbon (TOC)...  High Temperature  5310 B...........  5310 B..........  415.3, Rev 1.2 \19\
                                Combustion.
                               Persulfate-       5310 C...........  5310 C..........  415.3, Rev 1.2 \19\
                                Ultraviolet or
                                Heated
                                Persulfate
                                Oxidation.
                               Wet Oxidation...  5310 D...........  5310 D..........  415.3, Rev 1.2 \19\
Specific Ultraviolet           Calculation       .................  ................  415.3, Rev 1.2 \19\
 Absorbance (SUVA).             using DOC and
                                UV254 data.
    Dissolved Organic Carbon   High Temperature  5310 B...........  5310 B..........  415.3, Rev 1.2 \19\
     (DOC).                     Combustion.
                               Persulfate-       5310 C...........  5310 C..........  415.3, Rev 1.2 \19\
                                Ultraviolet or
                                Heated
                                Persulfate
                                Oxidation.
                               Wet Oxidation...  5310 D...........  5310 D..........  415.3, Rev 1.2 \19\
Ultraviolet absorption at 254  Spectrophotometr  5910 B...........  5910 B..........  415.3, Rev 1.2 \19\
 nm (UV254).                    y.
----------------------------------------------------------------------------------------------------------------

* * * * *

                                       Alternative Testing Methods for Contaminants Listed at 40 CFR 141.402(c)(2)
--------------------------------------------------------------------------------------------------------------------------------------------------------
                                                       SM 20th  Edition    SM 21st  Edition    SM 22nd  Edition
            Organism                 Methodology             \6\                  \1\                \28\            SM Online \3\           Other
--------------------------------------------------------------------------------------------------------------------------------------------------------
E. coli........................  Colilert[supreg]..  ...................  9223 B............  9223 B............  9223 B-97.........
                                 Colisure[supreg]..  ...................  9223 B............  9223 B............  9223 B-97.........
                                 Colilert-18.......  9223 B.............  9223 B............  9223 B............  9223 B-97.........
                                 Readycult[supreg].  ...................  ..................  ..................  ..................  Ready
                                                                                                                                      cult[supreg] \20\
                                 Colitag...........  ...................  ..................  ..................  ..................  Modified ColitagTM
                                                                                                                                       \13\
                                 Chromocult[supreg]  ...................  ..................  ..................  ..................  Chromo
                                                                                                                                      cult[supreg] \21\
                                 EC-MUG............  ...................  ..................  9221 F............
Enterococci....................  Multiple-Tube       ...................  ..................  ..................  9230 B-04.........
                                  Technique.
Coliphage......................  Two-Step            ...................  ..................  ..................  ..................  Fast Phage \30\
                                  Enrichment
                                  Presence-Absence
                                  Procedure.
--------------------------------------------------------------------------------------------------------------------------------------------------------

* * * * *

                   Alternative Testing Methods for Contaminants Listed at 40 CFR 141.852(a)(5)
----------------------------------------------------------------------------------------------------------------
             Organism                Methodology category         Method               SM 22nd Edition \28\
----------------------------------------------------------------------------------------------------------------
Total Coliforms...................  Lactose Fermentation   Standard Total        9221 B.1, B.2
                                     Methods.               Coliform
                                                            Fermentation
                                                            Technique.
                                    Enzyme Substrate       Colilert[supreg]....  9223 B
                                     Methods.
                                                           Colisure[supreg]....  9223 B
Escherichia coli..................  Escherichia coli       EC-MUG medium.......  9221 F.1
                                     Procedure (following
                                     Lactose Fermentation
                                     Methods).
                                    Enzyme Substrate       Colilert[supreg]....  9223 B
                                     Methods.
                                                           Colisure[supreg]....  9223 B
----------------------------------------------------------------------------------------------------------------


[[Page 37466]]


                                         Alternative Testing Methods for Contaminants Listed at 40 CFR 143.4(b)
--------------------------------------------------------------------------------------------------------------------------------------------------------
                                                                                         SM 21st  Edition    SM 22nd  Edition
         Contaminant              Methodology       EPA method           ASTM \4\               \1\                \28\               SM online \3\
--------------------------------------------------------------------------------------------------------------------------------------------------------
Aluminum.....................  Axially viewed    200.5, Revision
                                inductively       4.2\2\
                                coupled plasma-
                                atomic emission
                                spectrometry
                                (AVICP-AES).
                               Atomic            ................  ...................  3111 D............  3111 D............
                                Absorption;
                                Direct.
                               Atomic            ................  ...................  3113 B............  3113 B............  3113 B-04
                                Absorption;
                                Furnace.
                               Inductively       ................  ...................  3120 B............  3120 B............
                                Coupled Plasma.
Chloride.....................  Silver Nitrate    ................  D 512-04 B.........  4500-Cl- B........  4500-Cl- B........
                                Titration.
                               Ion               ................  ...................  4110 B............  4110 B............
                                Chromatography.
                               Potentiometric    ................  ...................  4500-Cl\-\ D......  4500-Cl\-\ D......
                                Titration.
Color........................  Visual            ................  ...................  2120 B............  2120 B............
                                Comparison.
Foaming Agents...............  Methylene Blue    ................  ...................  5540 C............  5540 C............
                                Active
                                Substances
                                (MBAS).
Iron.........................  Axially viewed    200.5, Revision
                                inductively       4.2 \2\
                                coupled plasma-
                                atomic emission
                                spectrometry
                                (AVICP-AES).
                               Atomic            ................  ...................  3111 B............  3111 B............
                                Absorption;
                                Direct.
                               Atomic            ................  ...................  3113 B............  3113 B............  3113 B-04
                                Absorption;
                                Furnace.
                               Inductively       ................  ...................  3120 B............  3120 B............
                                Coupled Plasma.
Manganese....................  Axially viewed    200.5, Revision
                                inductively       4.2 \2\
                                coupled plasma-
                                atomic emission
                                spectrometry
                                (AVICP-AES).
                               Atomic            ................  ...................  3111 B............  3111 B............
                                Absorption;
                                Direct.
                               Atomic            ................  ...................  3113 B............  3113 B............  3113 B-04
                                Absorption;
                                Furnace.
                               Inductively       ................  ...................  3120 B............  3120 B............
                                Coupled Plasma.
Odor.........................  Threshold Odor    ................  ...................  2150 B............  2150 B............
                                Test.
Silver.......................  Axially viewed    200.5, Revision
                                inductively       4.2 \2\
                                coupled plasma-
                                atomic emission
                                spectrometry
                                (AVICP-AES).
                               Atomic            ................  ...................  3111 B............  3111 B............
                                Absorption;
                                Direct.
                               Atomic            ................  ...................  3113 B............  3113 B............  3113 B-04
                                Absorption;
                                Furnace.
                               Inductively       ................  ...................  3120 B............  3120 B............
                                Coupled Plasma.
Sulfate......................  Ion               ................  ...................  4110 B............  4110 B............
                                Chromatography.
                               Gravimetric with  ................  ...................  4500-SO4 2- C.....  4500-SO4 2- C.....  4500-SO4 2- C-97
                                ignition of
                                residue.
                               Gravimetric with  ................  ...................  4500-SO4 2- D.....  4500-SO4 2- D.....  4500-SO4 2- D-97
                                drying of
                                residue.
                               Turbidimetric     ................  D 516-07, 11.......  4500-SO4 2- E.....  4500-SO4 2- E.....  4500-SO4 2- E-97
                                method.
                               Automated         ................  ...................  4500-SO4 2- F.....  4500-SO4 2- F.....  4500-SO4 2- F-97
                                methylthymol
                                blue method.
Total Dissolved Solids.......  Total Dissolved   ................  ...................  2540 C............  2540 C............
                                Solids Dried at
                                180 deg C.
Zinc.........................  Axially viewed    200.5, Revision
                                inductively       4.2 \2\
                                coupled plasma-
                                atomic emission
                                spectrometry
                                (AVICP-AES).
                               Atomic            ................  ...................  3111 B............  3111 B............
                                Absorption;
                                Direct
                                Aspiration.

[[Page 37467]]

 
                               Inductively       ................  ...................  3120 B............  3120 B............
                                Coupled Plasma.
--------------------------------------------------------------------------------------------------------------------------------------------------------
\1\ Standard Methods for the Examination of Water and Wastewater, 21st edition (2005). Available from American Public Health Association, 800 I Street
  NW., Washington, DC 20001-3710.
\2\ EPA Method 200.5, Revision 4.2. ``Determination of Trace Elements in Drinking Water by Axially Viewed Inductively Coupled Plasma-Atomic Emission
  Spectrometry.'' 2003. EPA/600/R-06/115. (Available at https://www.epa.gov/nerlcwww/ordmeth.htm.)
\3\ Standard Methods Online are available at https://www.standardmethods.org. The year in which each method was approved by the Standard Methods
  Committee is designated by the last two digits in the method number. The methods listed are the only online versions that may be used.
\4\ Available from ASTM International, 100 Barr Harbor Drive, West Conshohocken, PA 19428-2959 or https://astm.org. The methods listed are the only
  alternative versions that may be used.
 * * * * * * *
\6\ Standard Methods for the Examination of Water and Wastewater, 20th edition (1998). Available from American Public Health Association, 800 I Street
  NW., Washington, DC 20001-3710.
\7\ Method ME355.01, Revision 1.0. ``Determination of Cyanide in Drinking Water by GC/MS Headspace,'' May 26, 2009. Available at https://www.nemi.gov or
  from James Eaton, H & E Testing Laboratory, 221 State Street, Augusta, ME 04333. (207) 287-2727.
\8\ Systea Easy (1-Reagent). ``Systea Easy (1-Reagent) Nitrate Method,'' February 4, 2009. Available at https://www.nemi.gov or from Systea Scientific,
  LLC., 900 Jorie Blvd., Suite 35, Oak Brook, IL 60523.
\9\ EPA Method 524.3, Version 1.0. ``Measurement of Purgeable Organic Compounds in Water by Capillary Column Gas Chromatography/Mass Spectrometry,''
  June 2009. EPA 815-B-09-009. Available at https://water.epa.gov/drink/.
\10\ Mitchell Method M5271, Revision 1.1. ``Determination of Turbidity by Laser Nephelometry,'' March 5, 2009. Available at https://www.nemi.gov or from
  Leck Mitchell, Ph.D., PE, 656 Independence Valley Dr., Grand Junction, CO 81507.
\11\ Mitchell Method M5331, Revision 1.1. ``Determination of Turbidity by LED Nephelometry,'' March 5, 2009. Available at https://www.nemi.gov or from
  Leck Mitchell, Ph.D., PE, 656 Independence Valley Dr., Grand Junction, CO 81507.
\12\ Orion Method AQ4500, Revision 1.0. ``Determination of Turbidity by LED Nephelometry,'' May 8, 2009. Available at https://www.nemi.gov or from
  Thermo Scientific, 166 Cummings Center, Beverly, MA 01915, https://www.thermo.com.
\13\ Modified Colitag TM Method. ``Modified Colitag TM Test Method for the Simultaneous Detection of E. coli and other Total Coliforms in Water (ATP D05-
  0035),'' August 28, 2009. Available at https://www.nemi.gov or from CPI International, 5580 Skylane Boulevard, Santa Rosa, CA 95403.
\14\ EPA Method 557. ``Determination of Haloacetic Acids, Bromate, and Dalapon in Drinking Water by Ion Chromatography Electrospray Ionization Tandem
  Mass Spectrometry (IC-ESI-MS/MS),'' September 2009. EPA 815-B-09-012. Available at https://water.epa.gov/drink/.
\15\ AMI Turbiwell, ``Continuous Measurement of Turbidity Using a SWAN AMI Turbiwell Turbidimeter,'' August 2009. Available at https://www.nemi.gov or
  from Markus Bernasconi, SWAN Analytische Instrumente AG, Studbachstrasse 13, CH-8340 Hinwil, Switzerland.
\16\ EPA Method 334.0. ``Determination of Residual Chlorine in Drinking Water Using an On-line Chlorine Analyzer,'' September 2009. EPA 815-B-09-013.
  Available at https://water.epa.gov/drink/.
\17\ ChloroSense. ``Measurement of Free and Total Chlorine in Drinking Water by Palintest ChloroSense,'' August 2009. Available at https://www.nemi.gov
  or from Palintest Ltd., 21 Kenton Lands Road, P.O. Box 18395, Erlanger, KY 41018.
\18\ EPA Method 302.0. ``Determination of Bromate in Drinking Water using Two-Dimensional Ion Chromatography with Suppressed Conductivity Detection,''
  September 2009. EPA 815-B-09-014. Available at https://water.epa.gov/drink/.
\19\ EPA 415.3, Revision 1.2. ``Determination of Total Organic Carbon and Specific UV Absorbance at 254 nm in Source Water and Drinking Water,''
  September 2009. EPA/600/R-09/122. Available at https://www.epa.gov/nerlcwww/ordmeth.htm.
\20\ Readycult[supreg] Method, ``Readycult[supreg] Coliforms 100 Presence/Absence Test for Detection and Identification of Coliform Bacteria and
  Escherichia coli in Finished Waters,'' January, 2007. Version 1.1. Available from EMD Millipore (division of Merck KGaA, Darmstadt, Germany), 290
  Concord Road, Billerica, MA 01821.
\21\ Chromocult[supreg] Method, ``Chromocult[supreg] Coliform Agar Presence/Absence Membrane Filter Test Method for Detection and Identification of
  Coliform Bacteria and Escherichia coli in Finished Waters,'' November, 2000. Version 1.0. EMD Millipore (division of Merck KGaA, Darmstadt, Germany),
  290 Concord Road, Billerica, MA 01821.
\22\ Hach Company. ``Hach Company SPADNS 2 (Arsenite-Free) Fluoride Method 10225--Spectrophotometric Measurement of Fluoride in Water and Wastewater,''
  January 2011. 5600 Lindbergh Drive, P.O. Box 389, Loveland, Colorado 80539. (Available at https://www.hach.com.)
\23\ Hach Company. ``Hach Company TNTplus\TM\ 835/836 Nitrate Method 10206--Measurement of Nitrate in Water and Wastewater,'' January 2011. 5600
  Lindbergh Drive, P.O. Box 389, Loveland, Colorado. (Available at https://www.hach.com.)
\24\ EPA Method 525.3. ``Determination of Semivolatile Organic Chemicals in Drinking Water by Solid Phase Extraction and Capillary Column Gas
  Chromatography/Mass Spectrometry (GC/MS),'' February 2012. EPA/600/R-12/010. Available at https://www.epa.gov/nerlcwww/ordmeth.htm.
\25\ EPA Method 536. ``Determination of Triazine Pesticides and their Degradates in Drinking Water by Liquid Chromatography Electrospray Ionization
  Tandem Mass Spectrometry (LC/ESI-MS/MS),'' October 2007. EPA 815-B-07-002. Available at https://water.epa.gov/drink.
\26\ EPA Method 523. ``Determination of Triazine Pesticides and their Degradates in Drinking Water by Gas Chromatography/Mass Spectrometry (GC/MS),''
  February 2011. EPA 815-R-11-002. Available at https://water.epa.gov/drink.
\27\ EPA Method 1623.1. ``Cryptosporidium and Giardia in Water by Filtration/IMS/FA,'' 2012. EPA-816-R-12-001. (Available at https://water.epa.gov/drink drink.)
\28\ Standard Methods for the Examination of Water and Wastewater, 22nd edition (2012). Available from American Public Health Association, 800 I Street
  NW., Washington, DC 20001-3710.
\29\ EPA Method 524.4, Version 1.0. ``Measurement of Purgeable Organic Compounds in Water by Gas Chromatography/Mass Spectrometry using Nitrogen Purge
  Gas,'' May 2013. EPA 815-R-13-002. Available at https://water.epa.gov/drink.
\30\ Charm Sciences Inc. ``Fast Phage Test Procedure. Presence/Absence for Coliphage in Ground Water with Same Day Positive Prediction''. Version 009.
  November 2012. 659 Andover Street, Lawrence, MA 01843. Available at www.charmsciences.com.


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[FR Doc. C1-2013-12729 Filed 6-20-13; 8:45 am]
BILLING CODE 1505-01-D
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