Etoxazole; Notice of Filing a Pesticide Petition to Establish a Tolerance for a Certain Pesticide Chemical in or on Food, 19446-19452 [05-7223]
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19446
Federal Register / Vol. 70, No. 70 / Wednesday, April 13, 2005 / Notices
EPA’s level of concern for acute dietary
exposure.
Regarding dietary cancer risk
assessment, EPA’s Cancer Peer Review
Committee has classified 2,4-D as a
Group D chemical (‘‘not classifiable as
to human carcinogenicity’’) on the basis
that, ‘‘the evidence is inadequate and
cannot be interpreted as showing either
the presence or absence of a
carcinogenic effect.’’
2. Infants and children. The data base
on 2,4-D relative to pre-and post-natal
toxicity is complete with respect to
current data requirements. Since the
developmental NOELs for rats and
rabbits are 25–fold greater and 90–fold
greater, respectively, than the RfD NOEL
of 1 mg/kg/day in the one–year oral
toxicity study in dogs, an additional
uncertainty factor to protect infants and
children is not warranted.
Using conservative EPA calculations
underlying the most recent final rule
establishing tolerances for 2,4-D cited
above, which included soybeans and all
other existing uses, aggregate acute
MOEs for exposure to 2,4-D from food
are 214 for infants less than 1–year old
and 399 for females 13 and older. The
maximum estimated concentrations of
2,4-D in surface and ground water are
less than EPA’s Drinking Water Level of
Comparison (DWLOC) figures for 2,4-D
as a contribution to acute aggregate
exposure. EPA concluded with
reasonable certainty that residues of 2,4D in drinking water do not contribute
significantly to the aggregate acute
human health risk.
Using the same conservative
assumptions described earlier to
estimate chronic risk from aggregate
chronic exposure to 2,4-D from food,
11.4% of the reference dose (RfD) is
utilized for nursing infants less than one
year old up to 49.2% of the RfD for nonnursing infants less than one–year old.
Further refinement using additional
anticipated residue values in crops and
percent crop-treated information would
result in lower chronic dietary (food)
exposure estimates, thus reducing the
aggregate risk estimate. Despite the
potential for exposure to 2,4-D in
drinking water and from non-dietary,
non-occupational exposure, EPA
concluded that, it did not expect the
aggregate exposure to exceed 100% of
the RfD.
F. International Tolerances
There are no Codex, Canadian, or
Mexican maximum residue limits
(MRLs) for use of 2,4-D on hops.
[FR Doc. 05–7224 Filed 4–12–05; 8:45 am]
BILLING CODE 6560–50–S
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ENVIRONMENTAL PROTECTION
AGENCY
[OPP–2005–0047; FRL–7699–9]
Etoxazole; Notice of Filing a Pesticide
Petition to Establish a Tolerance for a
Certain Pesticide Chemical in or on
Food
Environmental Protection
Agency (EPA).
ACTION: Notice.
AGENCY:
SUMMARY: This notice announces the
initial filing of a pesticide petition
proposing the establishment of
regulations for residues of a certain
pesticide chemical in or on various food
commodities.
DATES: Comments, identified by docket
identification (ID) number OPP–2005–
0047, must be received on or before May
13, 2005.
ADDRESSES: Comments may be
submitted electronically, by mail, or
through hand delivery/courier. Follow
the detailed instructions as provided in
Unit I. of the SUPPLEMENTARY
INFORMATION.
FOR FURTHER INFORMATION CONTACT:
Kable Bo Davis, Registration Division
(7505C), Office of Pesticide Programs,
Environmental Protection Agency, 1200
Pennsylvania Ave., NW., Washington,
DC 20460–0001; telephone number:
(703) 306–0415; e-mail address:
davis.kable@epa.gov.
SUPPLEMENTARY INFORMATION:
I. General Information
A. Does this Action Apply to Me?
You may be potentially affected by
this action if you an agricultural
producer, food manufacturer, or
pesticide manufacturer. Potentially
affected entities may include, but are
not limited to:
• Crop production (NAICS 111)
• Animal production (NAICS 112)
• Food manufacturing (NAICS 311)
• Pesticide manufacturing (NAICS
32532)
This listing is not intended to be
exhaustive, but rather provides a guide
for readers regarding entities likely to be
affected by this action. Other types of
entities not listed in this unit could also
be affected. The North American
Industrial Classification System
(NAICS) codes have been provided to
assist you and others in determining
whether this action might apply to
certain entities. If you have any
questions regarding the applicability of
this action to a particular entity, consult
the person listed under FOR FURTHER
INFORMATION CONTACT.
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B. How Can I Get Copies of this
Document and Other Related
Information?
1. Docket. EPA has established an
official public docket for this action
under docket ID number OPP–2005–
0047. The official public docket consists
of the documents specifically referenced
in this action, any public comments
received, and other information related
to this action. Although, a part of the
official docket, the public docket does
not include Confidential Business
Information (CBI) or other information
whose disclosure is restricted by statute.
The official public docket is the
collection of materials that is available
for public viewing at the Public
Information and Records Integrity
Branch (PIRIB), Rm. 119, Crystal Mall
#2, 1801 S. Bell St., Arlington, VA. This
docket facility is open from 8:30 a.m. to
4 p.m., Monday through Friday,
excluding legal holidays. The docket
telephone number is (703) 305–5805.
2. Electronic access. You may access
this Federal Register document
electronically through the EPA Internet
under the ‘‘Federal Register’’ listings at
https://www.epa.gov/fedrgstr/.
An electronic version of the public
docket is available through EPA’s
electronic public docket and comment
system, EPA Dockets. You may use EPA
Dockets at https://www.epa.gov/edocket/
to submit or view public comments,
access the index listing of the contents
of the official public docket, and to
access those documents in the public
docket that are available electronically.
Although, not all docket materials may
be available electronically, you may still
access any of the publicly available
docket materials through the docket
facility identified in Unit I.B.1. Once in
the system, select ‘‘search,’’ then key in
the appropriate docket ID number.
Certain types of information will not
be placed in the EPA Dockets.
Information claimed as CBI and other
information whose disclosure is
restricted by statute, which is not
included in the official public docket,
will not be available for public viewing
in EPA’s electronic public docket. EPA’s
policy is that copyrighted material will
not be placed in EPA’s electronic public
docket but will be available only in
printed, paper form in the official public
docket. To the extent feasible, publicly
available docket materials will be made
available in EPA’s electronic public
docket. When a document is selected
from the index list in EPA Dockets, the
system will identify whether the
document is available for viewing in
EPA’s electronic public docket.
Although, not all docket materials may
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be available electronically, you may still
access any of the publicly available
docket materials through the docket
facility identified in Unit I.B. EPA
intends to work towards providing
electronic access to all of the publicly
available docket materials through
EPA’s electronic public docket.
For public commenters, it is
important to note that EPA’s policy is
that public comments, whether
submitted electronically or on paper,
will be made available for public
viewing in EPA’s electronic public
docket as EPA receives them and
without change, unless the comment
contains copyrighted material, CBI, or
other information whose disclosure is
restricted by statute. When EPA
identifies a comment containing
copyrighted material, EPA will provide
a reference to that material in the
version of the comment that is placed in
EPA’s electronic public docket. The
entire printed comment, including the
copyrighted material, will be available
in the public docket.
Public comments submitted on
computer disks that are mailed or
delivered to the docket will be
transferred to EPA’s electronic public
docket. Public comments that are
mailed or delivered to the docket will be
scanned and placed in EPA’s electronic
public docket. Where practical, physical
objects will be photographed, and the
photograph will be placed in EPA’s
electronic public docket along with a
brief description written by the docket
staff.
C. How and to Whom Do I Submit
Comments?
You may submit comments
electronically, by mail, or through hand
delivery/courier. To ensure proper
receipt by EPA, identify the appropriate
docket ID number in the subject line on
the first page of your comment. Please
ensure that your comments are
submitted within the specified comment
period. Comments received after the
close of the comment period will be
marked ‘‘late.’’ EPA is not required to
consider these late comments. If you
wish to submit CBI or information that
is otherwise protected by statute, please
follow the instructions in Unit I.D. Do
not use EPA Dockets or e-mail to submit
CBI or information protected by statute.
1. Electronically. If you submit an
electronic comment as prescribed in this
unit, EPA recommends that you include
your name, mailing address, and an email address or other contact
information in the body of your
comment. Also, include this contact
information on the outside of any disk
or CD ROM you submit, and in any
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cover letter accompanying the disk or
CD ROM. This ensures that you can be
identified as the submitter of the
comment and allows EPA to contact you
in case EPA cannot read your comment
due to technical difficulties or needs
further information on the substance of
your comment. EPA’s policy is that EPA
will not edit your comment, and any
identifying or contact information
provided in the body of a comment will
be included as part of the comment that
is placed in the official public docket,
and made available in EPA’s electronic
public docket. If EPA cannot read your
comment due to technical difficulties
and cannot contact you for clarification,
EPA may not be able to consider your
comment.
i. EPA Dockets. Your use of EPA’s
electronic public docket to submit
comments to EPA electronically is
EPA’s preferred method for receiving
comments. Go directly to EPA Dockets
at https://www.epa.gov/edocket/, and
follow the online instructions for
submitting comments. Once in the
system, select ‘‘search,’’ and then key in
docket ID number OPP–2005–0047. The
system is an ‘‘anonymous access’’
system, which means EPA will not
know your identity, e-mail address, or
other contact information unless you
provide it in the body of your comment.
ii. E-mail. Comments may be sent by
e-mail to opp-docket@epa.gov,
Attention: Docket ID number OPP–
2005–0047. In contrast to EPA’s
electronic public docket, EPA’s e-mail
system is not an ‘‘anonymous access’’
system. If you send an e-mail comment
directly to the docket without going
through EPA’s electronic public docket,
EPA’s e-mail system automatically
captures your e-mail address. E-mail
addresses that are automatically
captured by EPA’s e-mail system are
included as part of the comment that is
placed in the official public docket, and
made available in EPA’s electronic
public docket.
iii. Disk or CD ROM. You may submit
comments on a disk or CD ROM that
you mail to the mailing address
identified in Unit I.C.2. These electronic
submissions will be accepted in
WordPerfect or ASCII file format. Avoid
the use of special characters and any
form of encryption.
2. By mail. Send your comments to:
Public Information and Records
Integrity Branch (PIRIB) (7502C), Office
of Pesticide Programs (OPP),
Environmental Protection Agency, 1200
Pennsylvania Ave., NW., Washington,
DC 20460–0001, Attention: Docket ID
number OPP–2005–0047.
3. By hand delivery or courier. Deliver
your comments to: Public Information
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and Records Integrity Branch (PIRIB),
Office of Pesticide Programs (OPP),
Environmental Protection Agency, Rm.
119, Crystal Mall #2, 1801 S. Bell St.,
Arlington, VA, Attention: Docket ID
number OPP–2005–0047. Such
deliveries are only accepted during the
docket’s normal hours of operation as
identified in Unit I.B.1.
D. How Should I Submit CBI to the
Agency?
Do not submit information that you
consider to be CBI electronically
through EPA’s electronic public docket
or by e-mail. You may claim
information that you submit to EPA as
CBI by marking any part or all of that
information as CBI (if you submit CBI
on disk or CD ROM, mark the outside
of the disk or CD ROM as CBI and then
identify electronically within the disk or
CD ROM the specific information that is
CBI). Information so marked will not be
disclosed except in accordance with
procedures set forth in 40 CFR part 2.
In addition to one complete version of
the comment that includes any
information claimed as CBI, a copy of
the comment that does not contain the
information claimed as CBI must be
submitted for inclusion in the public
docket and EPA’s electronic public
docket. If you submit the copy that does
not contain CBI on disk or CD ROM,
mark the outside of the disk or CD ROM
clearly that it does not contain CBI.
Information not marked as CBI will be
included in the public docket and EPA’s
electronic public docket without prior
notice. If you have any questions about
CBI or the procedures for claiming CBI,
please consult the person listed under
FOR FURTHER INFORMATION CONTACT.
E. What Should I Consider as I Prepare
My Comments for EPA?
You may find the following
suggestions helpful for preparing your
comments:
1. Explain your views as clearly as
possible.
2. Describe any assumptions that you
used.
3. Provide copies of any technical
information and/or data you used that
support your views.
4. If you estimate potential burden or
costs, explain how you arrived at the
estimate that you provide.
5. Provide specific examples to
illustrate your concerns.
6. Make sure to submit your
comments by the deadline in this
notice.
7. To ensure proper receipt by EPA,
be sure to identify the docket ID number
assigned to this action in the subject
line on the first page of your response.
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You may also provide the name, date,
and Federal Register citation.
II. What Action is the Agency Taking?
EPA has received a pesticide petition
as follows proposing the establishment
and/or amendment of regulations for
residues of a certain pesticide chemical
in or on various food commodities
under section 408 of the Federal Food,
Drug, and Cosmetic Act (FFDCA), 21
U.S.C. 346a. EPA has determined that
this petition contains data or
information regarding the elements set
forth in FFDCA section 408(d)(2);
however, EPA has not fully evaluated
the sufficiency of the submitted data at
this time or whether the data support
granting of the petition. Additional data
may be needed before EPA rules on the
petition.
List of Subjects
Environmental protection,
Agricultural commodities, Feed
additives, Food additives, Pesticides
and pests, Reporting and recordkeeping
requirements.
Dated: April 1, 2005.
Lois Rossi,
Director, Registration Division, Office of
PesticidePrograms.
Summary of Petition
The petitioner’s summary of the
pesticide petition is printed below as
required by FFDCA section 408(d)(3).
The summary of the petition was
prepared by Valent U.S.A. Corporation
and represents the view of the
petitioner. The petition summary
announces the availability of a
description of the analytical methods
available to EPA for the detection and
measurement of the pesticide chemical
residues or an explanation of why no
such method is needed.
Valent U.S.A. Corporation
PP 3F6739
EPA has received a pesticide petition
PP 3F6739 from Valent U.S.A.
Corporation, 1333 North California
Boulevard, Suite 600, Walnut Creek, CA
94596–8025 proposing, pursuant to
section 408(d) of the Federal Food,
Drug, and Cosmetic Act (FFDCA), 21
U.S.C. 346a(d), to amend 40 CFR part
180, by establishing a tolerance for
residues of the chemical etoxazole, 2(2,6-difluorophenyl)-4-[4-(1,1dimethylethyl)-2-ethoxyphenyl]-4,5dihydrooxazole, in or on the raw
agricultural commodities nut, tree (Crop
Group 14), including pistachios at 0.01
parts per million (ppm), almond, hulls
at 2.0 ppm, grapes at 0.5 ppm, and
raisins at 1.5 ppm. EPA has determined
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that the petition contains data or
information regarding the elements set
forth in section 408(d)(2) of the FFDCA;
however, EPA has not fully evaluated
the sufficiency of the submitted data at
this time or whether the data support
granting of the petition. Additional data
may be needed before EPA rules on the
petition.
A. Residue Chemistry
1. Plant metabolism. The metabolism
of etoxazole is adequately understood
for the purpose of the proposed
tolerances.
2. Analytical methods. Practical
analytical methods for detecting and
measuring levels of etoxazole have been
developed and validated in/on all
appropriate agricultural commodities
and respective processing fractions. The
extraction methodology has been
validated using aged radiochemical
residue samples from 14C-metabolism
studies. The enforcement methods have
been validated in cottonseed, cotton gin
trash, and in fresh mandarin oranges at
independent laboratories. The LOQ of
etoxazole in these methods is 0.01 ppm
in grapes and nutmeats and 0.05 ppm in
almond, hulls, which will allow
monitoring of food with residues at the
levels proposed for the tolerances.
3. Magnitude of residues. An
extensive crop residue program has
been conducted for etoxazole in all
major growing regions of the United
States for the following crops: Almond
and pecans (representing nut, tree, Crop
Group 14), and grapes. The results of
these studies can be summarized as
follows:
• For almonds, the maximum
etoxazole residues from two
applications at 0.135 pounds active
ingredient/acre/treatment, was 0.005
ppm for nutmeats and 1.79 ppm for
hulls harvested 28–days after
application. Almond hulls were also
analyzed for R–3, a metabolite of
etoxazole. The maximum residue of R–
3 was as 0.12 ppm.
• For pecans, no etoxazole residues
were observed in nutmeats (LOD =
0.005 ppm) treated twice at 0.135
pounds active ingredient/acre/treatment
and harvested 28–days after application.
• The maximum etoxazole residue
in grapes harvested 28–days following
the last of two treatments at 0.135
pounds active ingredient/acre/treatment
was 0.33 ppm.
• The results of a grape processing
study indicate that etoxazole residues
concentrate in both grape juice and
raisins. The concentration factor for
grape juice was determined in this study
to be 5.3X, which exceeds the
theoretical concentration factor of 1.2X.
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Using this theoretical concentration
factor to estimate the tolerance for juice,
a tolerance of 0.32 ppm was calculated.
Since this tolerance is less than the
tolerance proposed for grapes, grape
juice tolerances are not required. The
concentration factor for raisins was
determined in this study to be 3.5X. The
theoretical concentration factor for
raisins is, however, 4.7x. To be
consistent with the grape juice
calculations, this theoretical
concentration factor was used to
determine the proposed tolerance for
raisins.
These field trial data are adequate to
support proposed tolerances of 0.01
ppm for nut, tree (Crop Group 14);
pistachios at 0.01 ppm; 2.0 ppm for
almond, hull; 0.5 ppm for grapes; and
1.5 ppm for raisins.
Almond, hull is the only commodity
under consideration that is a significant
feed item for beef and dairy cattle.
Tolerances of 0.03 ppm in the fat of
animals and 0.04 ppm in milk fat,
previously proposed and pending at the
Agency, are adequate to support the use
on almonds.
None of the commodities under
consideration are used as poultry feed
items. Additionally, the results of a hen
metabolism study demonstrated very
low potential for residues in feed to
transfer to poultry tissues or eggs.
Therefore, no hen residue feeding study
was performed and tolerances are not
proposed for secondary residues in
poultry commodities.
B. Toxicological Profile
A full battery of toxicology testing,
including studies of acute, chronic,
oncogenicity, developmental,
mutagenicity, and reproductive effects
has been completed for etoxazole. The
acute toxicity of etoxazole is low by all
routes. Etoxazole is not a developmental
or reproductive toxicant, and is not
mutagenic or oncogenic. For the
purpose of dietary risk analysis, Valent
proposes 0.04 milligrams/kilogram body
weight/day (mg/kg bwt/day) as the
chronic Population Adjusted Dose
(cPAD) and 2 mg/kg bwt/day as the
acute Population Adjusted Dose (aPAD).
The cPAD is based on a chronic
endpoint of 4 mg/kg bwt/day no
observed adverse effect level (NOAEL)
for males from the rat chronic/
oncogenicity feeding study and an
uncertainty factor of 100. The aPAD is
based on the 200 mg/kg bwt/day
NOAEL from the rabbit developmental
toxicity study and an uncertainty factor
of 100. Valent is unable to identify
toxicity endpoints of concern for acute,
short-term or chronic human exposures
by any route other than oral.
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1. Acute toxicity. The acute toxicity of
technical grade etoxazole is low by all
routes. The battery of acute toxicity
studies place etoxazole in Toxicity
Category III. The oral LD50 in the rat was
greater than 5 grams/kilogram (g/kg), the
dermal LD50 was greater than 2.0 g/kg,
and the inhalation LC50 in the rat was
greater than 1.09 milligrams/liter (mg/
L). Etoxazole technical was not an
irritant to eyes or skin and was not a
skin sensitizer.
2. Genotoxicity. Etoxazole was
evaluated and found to be negative in an
Ames reverse mutation assay, a
chromosome aberration assay, a
micronucleus assay, and an
unscheduled DNA synthesis (UDS)
assay. Etoxazole produced a positive
result in the mouse lymphoma gene
mutation assay but only in the presence
of metabolic activation. Etoxazole does
not present a genetic hazard.
3. Reproductive and developmental
toxicity—i. Rat developmental study.
Etoxazole did not produce
developmental toxicity in rats.
Etoxazole technical was administered
by oral gavage to pregnant rats at dosage
levels of 40, 200, and 1,000 mg/kg/day
on days 6 through 15 of gestation. There
were no mortalities or treatment-related
adverse effects in any dose group. Food
consumption was slightly decreased in
dams during the dosing period for the
1,000 mg/kg/day group. On cesarean
section evaluation there was no
differences in number of corpora lutea,
number of live and dead fetuses, percent
resorption, placental weight, fetal
weight or sex ratio in the dams and no
treatment-related external, visceral or
skeletal malformations noted in any of
the fetuses. It was concluded that, the
maternal no observed adverse effect
Level (NOAEL) was 200 mg/kg/day,
based on decreased food consumption at
1,000 mg/kg/day. The developmental
NOAEL was 1,000 mg/kg/day, the
highest dose tested (HDT).
ii. Rabbit developmental study.
Etoxazole did not produce
developmental toxicity in rabbits.
Etoxazole technical was administered
by oral gavage to pregnant rabbits at
dosage levels of 40, 200, and 1,000 mg/
kg/day on days 6 through 18 of
gestation. No treatment-related adverse
effects were found on maternal rabbits
in the 40 and 200 mg/kg/day groups.
One high dose rabbit died but it is
unclear whether this death was
attributed to treatment. Decreased body
weight, body weight gain, food
consumption and enlarged liver were
noted at 1,000 mg/kg/day. Cesarean
section findings showed that there was
no differences in number of corpora
lutea, number of live and dead fetuses,
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percent resorptions, placental weight,
fetal weight and sex ratio in the dams
and showed no treatment-related
malformations (external, visceral,
skeletal) in any of the fetuses. A
statistically significant increased
incidence of 27 presacral vertebrae with
13th ribs was observed in fetuses at
1,000 mg/kg/day compared with
controls. This finding was within
historical control range for fetal
incidence but above the historical
control range for litter incidence. No
dose response was evident and the
variation is considered to be equivocally
treatment related. The NOAEL for
maternal and developmental toxicity
was 200 mg/kg/day based on decreased
body weight and body weight gain,
decreased food consumption, and liver
enlargement at 1,000 mg/kg/day. The
NOAEL for developmental toxicity was
200 mg/kg/day based on statistically
significant increased incidence of 27
presacral vertebrae with 13th ribs in
fetuses at 1,000 mg/kg/day.
iii. Rat reproduction study. Etoxazole
showed no effects on reproduction in a
two-generation rat study. Etoxazole
technical was fed to two generations of
male and female Sprague Dawley rats at
dietary concentrations of 80, 400, and
2,000 ppm. No treatment-related
adverse effects were observed in the 80
and 400 ppm groups for any parameter.
In the 2,000 ppm group, relative liver
weights were increased in the F0 and F1
parental males. No adverse reproductive
effects were noted at any dose level in
the incidence of normal estrous cycle,
mating index, fertility and gestation
indices, the number of implantation
sites, and duration of gestation in F0
and F1 parental animals. For the
offspring, it was noted that at 2,000
ppm, the viability index on lactation
Day 4 was significantly lower in the F1
pups and body weights were lowered in
pups during the latter half of the
lactation period. For the F0 and F1 pups
of the 80 and 400 ppm groups, there
were no treatment-related adverse
effects observed for any parameter, i.e.
mean number of pups delivered, sex
ratio, viability indices on lactation days
0, 4 and 21, clinical signs, body weights
and gross pathological findings. The
parental NOAEL was 400 ppm (17.0 mg/
kg/day) based on the effects on relative
liver weight in males at 2,000 ppm. The
pup NOAEL was 400 ppm (37.9 mg/kg/
day) based on decreased viability on
lactation Day 4 and decreased body
weight at 2,000 ppm in the F1 pups. The
reproductive NOAEL was 2,000 ppm
(86.4 mg/kg/day), the (HDT).
4. Subchronic toxicity. Subchronic
toxicity studies conducted with
etoxazole technical in the rat (oral and
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19449
dermal), mouse and dog indicate a low
level of toxicity. Effects observed at high
dose levels consisted primarily of
anemia and histological changes in the
adrenal gland, liver and kidneys.
i. Rat feeding study. A 90–day
subchronic toxicity study was
conducted in rats, with dietary intake
levels of 100, 300, 1,000 and 3,000 ppm
etoxazole technical. The NOAEL was
100 ppm for males and 300 ppm for
females based on increased incidence of
hepatocellular swelling at 1,000 ppm
and 3,000 ppm.
ii. Mouse feeding study. A 90–day
subchronic toxicity study was
conducted in mice, with dietary intake
levels of 100, 400, 1,600, and 6,400 ppm
etoxazole technical. The NOAEL was
400 ppm for males and 1,600 ppm for
females based on increased alkaline
phosphatase activity, increased liver
weights, and increased incidence of
hepatocellular swelling at 6,400 ppm
(both sexes) and at 1,600 ppm in males
and enlarged livers in females at 6,400
ppm.
iii. Dog feeding study. Etoxazole
technical was fed to male and female
Beagle dogs for 13 weeks at dietary
concentrations of 200, 2,000, and 10,000
ppm. The NOAEL was 200 ppm (5.3
mg/kg/day) based on clinical signs,
clinical pathology changes, liver weight
effects and histopathological changes at
2,000 and 10,000 ppm.
iv. Repeated dose dermal study. A
28–day dermal toxicity study was
conducted in rats at dose levels of 30,
100, and 1,000 mg/kg. There were no
treatment related changes in any of the
parameters monitored. The NOAEL was
1,000 mg/kg, the (HDT).
5. Chronic toxicity. Etoxazole
technical has been tested in chronic
studies with dogs, rats and mice. Valent
proposes a chronic oral endpoint of 4
mg/kg bwt/day, based on the NOAEL for
male rats in a 2–year chronic toxicity
oncogenicity feeding study.
i. Dog chronic feeding study.
Etoxazole technical was fed to male and
female beagle dogs for one year at
dietary concentrations of 200, 1,000,
and 5,000 ppm. The NOAEL was 200
ppm (4.6 mg/kg/day for males and 4.79
mg/kg/day for females) based on
increased absolute and relative liver
weights with corresponding
histopathological changes in the liver at
1,000 and 5,000 ppm.
ii. Rat chronic feeding/oncogenicity
study. Etoxazole was not oncogenic in
rats in either of two chronic feeding
studies conducted. In the first study,
etoxazole technical was fed to male and
female Sprague Dawley rats for 2–years
at dietary concentrations of 4, 16, and
64 mg/kg/day. A trend toward decreased
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body weight gain for males at 64 mg/kg/
day in the latter half of the study was
observed. Hemotology and clinical
chemistry changes, increased liver
weights and hepatic enlargement at 16
mg/kg/day or above were observed.
Testicular masses, centrilobular
hepatocellular swelling and testicular
interstitial (Leydig) cell tumors occurred
at or above 16 mg/kg/day. The
interstitial (Leydig) cell tumors were
believed to be incidental. The NOAEL
was 4 mg/kg/day for males and 16 mg/
kg/day for females. Because an MTD
level was not achieved in this study, a
second study was conducted in which
etoxazole technical was fed to male and
female Sprague Dawley rats for 2–years
at dietary concentrations of 50, 5,000,
and 10,000 ppm. In this study,
decreased mortality, body weight and
food consumption/ efficiency (females)
at 10,000 ppm was observed.
Hematological, clinical, and
histopathological changes of the
incisors, and increased liver weights
occurred in both sexes at 5,000 and
10,000 ppm. Centrilobular
hepatocellular hypertrophy was
observed in both sexes at 10,000 ppm.
The interstitial (Leydig) cell tumors
observed in the first study, were not
observed in the repeat study. The
NOAEL in the repeat study was 50 ppm
(1.8 mg/kg/day).
iii. Mouse oncogenicity study.
Etoxazole was not oncogenic in either of
2 mouse oncogenicity studies
conducted. In the first study, etoxazole
technical was fed to male and female
CD–1 mice for 18–months at dietary
concentrations of 15, 60, and 240 mg/
kg/day. Increased liver weights occurred
in females at the highest dose tested.
Histopathology parameters were altered
for males at 240 mg/kg/day. No
neoplastic lesions were observed at any
dose level. The NOAEL was 60 mg/kg/
day. Since the toxicity in this study was
minimal and did not meet the definition
of MTD, a second study was conducted
at dose levels of 2,250 and 4,500 ppm
etoxazole. There were no effects in any
group on clinical observations,
mortality, body weight, food
consumption or hematology. Females
showed a significant elevation in
relative liver weight after 52–weeks of
treatment at 4,500 ppm. In
histopathology, a significantly higher
incidence of centrilobular
hepatocellular fatty change was
observed in males in the 4,500 ppm
group necropsied after 78–weeks of
treatment. There were no treatmentrelated changes in either sex in the
2,250 ppm dose group. No increase in
neoplastic lesions were observed in any
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treated group of either sex. Therefore, it
was concluded that, the NOAEL is 2,250
ppm (242 mg/kg/day for the males and
243 mg/kg/day for the females).
6. Animal metabolism. The
absorption, tissue distribution,
metabolism and excretion of etoxazole
were studied in rats after single oral
doses of 5 or 500 mg/kg, and after 14
daily oral doses at 5 mg/kg. Etoxazole,
labeled in both the t-butylphenyl ring
and the oxazole ring were used in this
study. For both single dose groups, most
(94–97%) of the administered radiolabel
was excreted in the urine and feces
within 7–days after dosing. Most of this
excretion occurred in the first 48 hours
after dosing. Maximum plasma
concentrations occurred 2–4 hours after
dosing, with half-lives ranging from 53–
89 hours at the low dose and 7–44 hours
at the high dose. Plasma levels were
significantly lower in females.
Concentrations of radioactivity were
significantly higher in the tissues of
male rats compared to females. The
highest concentrations occurred at 3
hours after dosing and were greatest in
the gastrointestinal tract and tissues
such as liver and kidneys, which are
responsible for metabolism and
excretion. By 168 hours, the
concentration in most tissues was below
the concentration in the corresponding
plasma, with only the liver and fat
having significant levels of
radioactivity. After multiple doses, peak
concentrations of radioactivity in tissues
occurred 2 hours after dosing and then
declined. The distribution of
radioactivity showed a similar profile to
those found after single oral doses but
were significantly higher, indicating
some accumulation. Etoxazole was
extensively metabolized by rats. The
main metabolic reactions in rats were
postulated to be hydroxylation of the
4,5-hydrooxazole ring followed by
cleavage of the molecule and
hydroxylation of the t-butyl side chain.
7. Metabolite toxicology. In an oral
toxicity limit test in rats, the oral LD50
of metabolite R–3 was estimated to be
greater than 5 g/kg for both male and
female rats. No treatment related body
weight changes and no treatment related
macroscopic abnormalities were
observed in this study. In another test,
the oral toxicity of metabolite R–7 (as
the HCl salt) was assessed. The oral
LD50 of this metabolite was also
estimated to be greater than 5 g/kg for
both male and female rats. No treatment
related macroscopic abnormalities were
observed in this test, although, some
clinical signs were observed within 6–
minutes of dosing. Mutagenicity screens
were performed with metabolite R–3
and metabolite R–7 (as the HCl salt).
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Neither metabolite was mutagenic when
tested with multiple strains of two
bacterial cultures (salmonella
typhimurium and e coli).
8. Endocrine disruption. No special
studies to investigate the potential for
estrogenic or other endocrine effects of
etoxazole have been performed.
However, as summarized above, a large
and detailed toxicology data base exists
for the compound including studies in
all required categories. These studies
include acute, sub-chronic, chronic,
developmental, and reproductive
toxicology studies including detailed
histology and histopathology of
numerous tissues, including endocrine
organs, following repeated or long term
exposures. These studies are considered
capable of revealing endocrine effects.
The results of all of these studies show
no evidence of any endocrine-mediated
effects and no pathology of the
endocrine organs. Consequently, it is
concluded that etoxazole does not
possess estrogenic or endocrine
disrupting properties.
C. Aggregate Exposure
1. Dietary exposure. A full battery of
toxicology testing including studies of
acute, chronic, oncogenicity,
developmental, mutagenicity, and
reproductive effects is available for
etoxazole. In these risk assessments,
Valent proposes as the chronic oral
toxic endpoint the NOAEL for males
from the rat chronic/oncogenicity
feeding study, 4 mg/kg/day. To assess
the chronic risk to the U.S. population
from exposure to etoxazole, the daily
chronic exposures were compared
against an estimated chronic population
adjusted dose (cPAD) of 0.04 mg/kg
bwt/day. This endpoint is derived from
the NOAEL from the 2–year chronic rat
study by applying an uncertainty factor
of 100 to account for intraspecies and
interspecies variations. There is no
evidence that any additional safety
factors are needed to further protect
vulnerable subpopulations. The
proposed acute oral toxic endpoint is
the NOAEL from the rabbit oral
developmental toxicity study, 200 mg/
kg/day. To assess the acute risk to the
U.S. population from exposure to
etoxazole, acute exposures were
compared against an estimated acute
population adjusted dose (aPAD) of 2
mg/kg bwt/day. This endpoint is
derived from the NOAEL from the rabbit
oral developmental toxicity study by
applying an uncertainty factor of 100 to
account for intraspecies and
interspecies variations. Based on
dietary, drinking water, and nonoccupational exposure assessments,
there is reasonable certainty of no harm
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to the U.S. population, any population
subgroup, or infants and children from
short-term or chronic exposure to
etoxazole.
i. Food. Dietary exposure was
estimated using the Cumulative and
Aggregate Risk Evaluation System
(CARES). Acute dietary exposure was
estimated for the overall U.S.
population and 16 population
subgroups using proposed tolerances
and conservative estimates of the
percentages of crop treated. The results
demonstrate that estimated exposure is
less than 1% of the estimated aPAD (at
the 99.9th percentile) for all population
groups examined. Acute dietary
exposure for the overall U.S. population
was estimated to be 0.006 mg/kg bwt/
day at the 99.9th percentile of exposure
(0.29% of the aPAD). Chronic dietary
exposure was estimated for the overall
U.S. population and 16 population
subgroups. Annual exposure for the
overall U.S. population was estimated to
be 0.00014 mg/kg bwt/day, representing
0.36% of the estimated cPAD. Annual
exposure for the most highly exposed
population subgroup, children 1–2 years
of age, was estimated to be 0.00065 mg/
kg bwt/day, or 1.62% of the estimated
cPAD.
ii. Drinking water. Since etoxazole is
applied outdoors to growing agricultural
crops, the potential exists for the parent
or its metabolites to reach ground water
or surface water that may be used for
drinking water. But, because of the
physical properties of etoxazole, it is
unlikely that etoxazole or its metabolites
can leach to potable ground water.
Although, relatively stable to
hydrolysis, etoxazole undergoes fairly
rapid photolysis, degrades fairly readily
in soil and is immobile in all soil types
examined. To quantify potential
exposure from drinking water, FIRST
and SCI-GROW models were used to
estimate surface water and ground water
residues. Estimated surface water
residues were much higher than
estimated ground water residues and
therefore, the surface residues were
used as the Drinking Water
Environmental Concentration (DWEC).
The peak (acute) concentration
predicted in the simulated pond water
was estimated to be 2.47 ppb and the
annual average (chronic) concentration
predicted in the simulated pond water
was estimated to be 1.93 ppb. To assess
the contribution to the dietary risk from
exposure to drinking water containing
residues of etoxazole, these DWEC’s are
compared to drinking water levels of
comparison (DWLOC’s), the maximum
drinking water concentration allowed
before combined water, dietary, and
other exposures will exceed the
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population adjusted doses. If the
DWLOC is greater than the DWEC, then
overall exposure will not exceed the
population adjusted doses and
combined exposure from water and food
is considered to be acceptable. Acute
DWLOC’s for etoxazole range from
19,900 to 69,910 ppb and chronic
DWLOC’s range from 377 to 1,380 ppb
for all U.S. population subgroups
examined. Since these DWLOC’s exceed
the modeled acute and chronic DWEC
surface water residues by a wide
margin, it can be concluded that,
exposure to potential residues in
drinking water is negligible and that
aggregate (food and water) exposure to
etoxazole residues will be acceptable.
2. Non-dietary exposure. Etoxazole is
proposed only for agricultural uses and
no homeowner or turf uses. Thus, no
non-dietary risk assessment is needed.
D. Cumulative Effects
Section 408(b)(2)(D)(v) requires that
the Agency must consider ‘‘available
information’’ concerning the cumulative
effects of a particular pesticide’s
residues and ‘‘other substances’’ that
have a common mechanism of toxicity.
Available information in this context
include not only toxicity, chemistry,
and exposure data, but also scientific
policies and methodologies for
understanding common mechanisms of
toxicity and conducting cumulative risk
assessments. For most pesticides,
although, the Agency has some
information in its files that may turn out
to be helpful in eventually determining
whether a pesticide shares a common
mechanism of toxicity with any other
substances, EPA does not at this time
have the methodologies to resolve the
complex scientific issues concerning
common mechanism of toxicity in a
meaningful way.
In consideration of potential
cumulative effects of etoxazole and
other substances that may have a
common mechanism of toxicity, there
are currently no available data or other
reliable information indicating that any
toxic effects produced by etoxazole
would be cumulative with those of other
chemical compounds. Thus, only the
potential risks of etoxazole have been
considered in this assessment of
aggregate exposure and effects.
Valent will submit information for
EPA to consider concerning potential
cumulative effects of etoxazole
consistent with the schedule established
by EPA at (62 FR 42020) (Aug. 4, 1997)
and other subsequent EPA publications
pursuant to the Food Quality Protection
Act.
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19451
E. Safety Determination
1. U.S. population—i. Acute risk. The
potential acute exposure from food to
the U.S. population and various nonchild/infant population subgroups are
estimated to be 0.15 to 0.30% of the
proposed aPAD. Exposure to potential
acute residues in drinking water is
expected to be negligible, as acute
DWLOC’s are substantially higher than
modeled acute DWEC’s. Based on this
assessment, it can be concluded that,
there is a reasonable certainty that no
harm to the U.S. population or any
population subgroup will result from
acute exposure to etoxazole.
ii. Chronic risk. The potential chronic
exposure from food to the U.S.
population and various non-child/infant
population subgroups are estimated to
be 0.24 to 1.59% of the proposed cPAD.
Chronic exposure to potential residues
in drinking water is also expected to be
negligible, as chronic DWLOC’s are
substantially higher than modeled
chronic DWEC’s. Based on this
assessment, it can be concluded that
there is a reasonable certainty that no
harm to the U.S. population or any
population subgroup will result from
chronic exposure to etoxazole.
2. Infants and children—i. Safety
factor for infants and children. In
assessing the potential for additional
sensitivity of infants and children to
residues of etoxazole, FFDCA section
408 provides that EPA shall apply an
additional margin of safety, up to ten–
fold, for added protection for infants
and children in the case of threshold
effects unless EPA determines that a
different margin of safety will be safe for
infants and children. The toxicological
data base for evaluating prenatal and
postnatal toxicity for etoxazole is
complete with respect to current data
requirements. There are no special
prenatal or postnatal toxicity concerns
for infants and children, based on the
results of the rat and rabbit
developmental toxicity studies or the 2generation reproductive toxicity study
in rats. Valent has concluded, that
reliable data support use of the standard
100–fold uncertainty factor and that an
additional uncertainty factor is not
needed for etoxazole to be further
protective of infants and children.
ii. Acute risk. The potential acute
exposure from food to infants and
children are estimated to be 0.28 to
0.97% of the proposed aPAD. Exposure
to potential acute residues in drinking
water is expected to be negligible, as
acute DWLOC’s are substantially higher
than modeled acute DWEC’s. Based on
this assessment, it can be concluded
that, there is a reasonable certainty that
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no harm to infants and children will
result from acute exposure to etoxazole.
iii. Chronic risk. The potential chronic
exposure from food to infants and
children are estimated to be 0.64 to
1.62% of the proposed cPAD. Chronic
exposure to potential residues in
drinking water is expected to be
negligible, as chronic DWLOC’s are
substantially higher than modeled
DWEC’s. Based on this assessment, it
can be concluded that, there is a
reasonable certainty that no harm to
infants and children will result from
chronic exposure to etoxazole.
3. Safety determination summary.
Aggregate acute or chronic dietary
exposure to various subpopulations of
children and adults demonstrate
acceptable risk. Acute and chronic
dietary exposures to etoxazole occupy
considerably less than 100% of the
appropriate PAD. EPA generally has no
concern for exposures below 100% of
the acute and chronic PAD’s because
these represent levels at or below which
daily aggregate dietary exposure over a
lifetime will not pose appreciable risks
to human health. Chronic and acute
dietary risk to children from etoxazole
should not be of concern. Further,
etoxazole has only agricultural uses and
no other uses, such as indoor pest
control, homeowner or turf, that could
lead to unique, enhanced exposures to
vulnerable sub-groups of the
population. It can be concluded that,
there is a reasonable certainty that no
harm will result to the U.S. population
or to any sub-group of the U.S.
population, including infants and
children, from aggregate chronic or
aggregate acute exposures to etoxazole
residues resulting from the proposed
uses.
Clarence M. Mitchell, Jr.
Conference Room on the Ninth Floor of
the EEOC Office Building, 1801 ‘‘L’’
Street, NW., Washington, DC 20507.
STATUS: Part of the meeting will be open
to the public and part of the meeting
will be closed.
MATTERS TO BE CONSIDERED:
PLACE:
Open Session
1. Announcement of Notation Votes.
2. Renewal of LexisNexis
Subscription Services.
3. Renewal of Westlaw and West
Publishing Subscriptions.
4. Oracle License Maintenance
Agreement.
5. Competitive Lease Contract for New
Mail Machine Systems.
Closed Session
Litigation Authorization: General
Counsel Recommendations.
Note: In accordance with the Sunshine Act,
the open session of the meeting will be open
to public observation of the Commission’s
deliberations and voting. (In addition to
publishing notices on EEOC Commission
meetings in the Federal Register, the
Commission also provides a recorded
announcement a full week in advance on
future Commission sessions.)
Please telephone (202) 663–7100
(voice) and (202) 663–4074 (TTY) at any
time for information on these meetings.
CONTACT PERSON FOR MORE INFORMATION:
Stephen Llewellyn, Acting Executive
Officer on (202) 663–4070.
This notice issued April 11, 2005.
Stephen Llewellyn,
Acting Executive Officer, Executive
Secretariat.
[FR Doc. 05–7537 Filed 4–11–05; 8:45 am]
BILLING CODE 6750–06–M
F. International Tolerances
Etoxazole has not been evaluated by
the JMPR and there are no codex
maximum residue limits (MRL) for
etoxazole. MRL values have been
established for etoxazole in the
following countries: Turkey, Israel,
South Africa, Japan, France, Taiwan,
and Korea. The use pattern and MRL’s
are similar to those proposed for the
U.S.
[FR Doc. 05–7223 Filed 4–12–05; 8:45 am]
BILLING CODE 6560–50–S
EQUAL EMPLOYMENT OPPORTUNITY
COMMISSION
Meeting, Sunshine Act
Thursday, April 21,
2005, a.m. eastern time.
DATE AND TIME:
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FEDERAL COMMUNICATIONS
COMMISSION
Notice of Public Information
Collection(s) being Reviewed by the
Federal Communications Commission
for Extension Under Delegated
Authority
April 4, 2005.
SUMMARY: The Federal Communications
Commission, as part of its continuing
effort to reduce paperwork burden
invites the general public and other
Federal agencies to take this
opportunity to comment on the
following information collection(s), as
required by the Paperwork Reduction
Act (PRA) of 1995, Public Law 104–13.
An agency may not conduct or sponsor
a collection of information unless it
displays a currently valid control
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number. No person shall be subject to
any penalty for failing to comply with
a collection of information subject to the
Paperwork Reduction Act (PRA) that
does not display a valid control number.
Comments are requested concerning (a)
whether the proposed collection of
information is necessary for the proper
performance of the functions of the
Commission, including whether the
information shall have practical utility;
(b) the accuracy of the Commission’s
burden estimate; (c) ways to enhance
the quality, utility and clarity of the
information collected; and (d) ways to
minimize the burden of the collection of
information on the respondents,
including the use of automated
collection techniques or other forms of
information technology.
DATES: Written Paperwork Reduction
(PRA) comments should be submitted
on or before June 13, 2005. If you
anticipate that you will be submitting
comments, but find it difficult to do so
within the period of time allowed by
this notice, you should advise the
contact listed below as soon as possible.
ADDRESSES: Direct all Paperwork
Reduction Act (PRA) comments to
Cathy Williams, Federal
Communications Commission, Room 1–
C823, 445 12th Street, SW., Washington,
DC 20554 or via the Internet to
Cathy.Williams@fcc.gov.
For
additional information or copies of the
information collection(s), contact Cathy
Williams at 202–418–2918 or via the
Internet at Cathy.Williams@fcc.gov.
SUPPLEMENTARY INFORMATION: OMB
Control Number: 3060–0386.
Title: Section 73.1635, Special
Temporary Authorizations (STA).
Form Number: Not applicable.
Type of Review: Extension of a
currently approved collection.
Respondents: Business or other forprofit entities; not-for-profit institutions.
Number of Respondents: 1,550.
Estimated Time per Response: 1–4
hours.
Frequency of Response: On occasion
reporting requirement.
Total Annual Burden: 2,000 hours.
Total Annual Cost: $939,950.
Privacy Impact Assessment: No
impact(s).
Needs and Uses: 47 CFR 73.1635
allows licensees/permittees of broadcast
stations to file for special temporary
authority to operate broadcast stations at
specified variances from station
authorization not to exceed 180 days.
Data is used by FCC staff to ensure that
such operations will not cause
interference to other stations.
FOR FURTHER INFORMATION CONTACT:
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Agencies
[Federal Register Volume 70, Number 70 (Wednesday, April 13, 2005)]
[Notices]
[Pages 19446-19452]
From the Federal Register Online via the Government Printing Office [www.gpo.gov]
[FR Doc No: 05-7223]
-----------------------------------------------------------------------
ENVIRONMENTAL PROTECTION AGENCY
[OPP-2005-0047; FRL-7699-9]
Etoxazole; Notice of Filing a Pesticide Petition to Establish a
Tolerance for a Certain Pesticide Chemical in or on Food
AGENCY: Environmental Protection Agency (EPA).
ACTION: Notice.
-----------------------------------------------------------------------
SUMMARY: This notice announces the initial filing of a pesticide
petition proposing the establishment of regulations for residues of a
certain pesticide chemical in or on various food commodities.
DATES: Comments, identified by docket identification (ID) number OPP-
2005-0047, must be received on or before May 13, 2005.
ADDRESSES: Comments may be submitted electronically, by mail, or
through hand delivery/courier. Follow the detailed instructions as
provided in Unit I. of the SUPPLEMENTARY INFORMATION.
FOR FURTHER INFORMATION CONTACT: Kable Bo Davis, Registration Division
(7505C), Office of Pesticide Programs, Environmental Protection Agency,
1200 Pennsylvania Ave., NW., Washington, DC 20460-0001; telephone
number: (703) 306-0415; e-mail address: davis.kable@epa.gov.
SUPPLEMENTARY INFORMATION:
I. General Information
A. Does this Action Apply to Me?
You may be potentially affected by this action if you an
agricultural producer, food manufacturer, or pesticide manufacturer.
Potentially affected entities may include, but are not limited to:
Crop production (NAICS 111)
Animal production (NAICS 112)
Food manufacturing (NAICS 311)
Pesticide manufacturing (NAICS 32532)
This listing is not intended to be exhaustive, but rather provides
a guide for readers regarding entities likely to be affected by this
action. Other types of entities not listed in this unit could also be
affected. The North American Industrial Classification System (NAICS)
codes have been provided to assist you and others in determining
whether this action might apply to certain entities. If you have any
questions regarding the applicability of this action to a particular
entity, consult the person listed under FOR FURTHER INFORMATION
CONTACT.
B. How Can I Get Copies of this Document and Other Related Information?
1. Docket. EPA has established an official public docket for this
action under docket ID number OPP-2005-0047. The official public docket
consists of the documents specifically referenced in this action, any
public comments received, and other information related to this action.
Although, a part of the official docket, the public docket does not
include Confidential Business Information (CBI) or other information
whose disclosure is restricted by statute. The official public docket
is the collection of materials that is available for public viewing at
the Public Information and Records Integrity Branch (PIRIB), Rm. 119,
Crystal Mall 2, 1801 S. Bell St., Arlington, VA. This docket
facility is open from 8:30 a.m. to 4 p.m., Monday through Friday,
excluding legal holidays. The docket telephone number is (703) 305-
5805.
2. Electronic access. You may access this Federal Register document
electronically through the EPA Internet under the ``Federal Register''
listings at https://www.epa.gov/fedrgstr/.
An electronic version of the public docket is available through
EPA's electronic public docket and comment system, EPA Dockets. You may
use EPA Dockets at https://www.epa.gov/edocket/ to submit or view public
comments, access the index listing of the contents of the official
public docket, and to access those documents in the public docket that
are available electronically. Although, not all docket materials may be
available electronically, you may still access any of the publicly
available docket materials through the docket facility identified in
Unit I.B.1. Once in the system, select ``search,'' then key in the
appropriate docket ID number.
Certain types of information will not be placed in the EPA
Dockets. Information claimed as CBI and other information whose
disclosure is restricted by statute, which is not included in the
official public docket, will not be available for public viewing in
EPA's electronic public docket. EPA's policy is that copyrighted
material will not be placed in EPA's electronic public docket but will
be available only in printed, paper form in the official public docket.
To the extent feasible, publicly available docket materials will be
made available in EPA's electronic public docket. When a document is
selected from the index list in EPA Dockets, the system will identify
whether the document is available for viewing in EPA's electronic
public docket. Although, not all docket materials may
[[Page 19447]]
be available electronically, you may still access any of the publicly
available docket materials through the docket facility identified in
Unit I.B. EPA intends to work towards providing electronic access to
all of the publicly available docket materials through EPA's electronic
public docket.
For public commenters, it is important to note that EPA's policy
is that public comments, whether submitted electronically or on paper,
will be made available for public viewing in EPA's electronic public
docket as EPA receives them and without change, unless the comment
contains copyrighted material, CBI, or other information whose
disclosure is restricted by statute. When EPA identifies a comment
containing copyrighted material, EPA will provide a reference to that
material in the version of the comment that is placed in EPA's
electronic public docket. The entire printed comment, including the
copyrighted material, will be available in the public docket.
Public comments submitted on computer disks that are mailed or
delivered to the docket will be transferred to EPA's electronic public
docket. Public comments that are mailed or delivered to the docket will
be scanned and placed in EPA's electronic public docket. Where
practical, physical objects will be photographed, and the photograph
will be placed in EPA's electronic public docket along with a brief
description written by the docket staff.
C. How and to Whom Do I Submit Comments?
You may submit comments electronically, by mail, or through hand
delivery/courier. To ensure proper receipt by EPA, identify the
appropriate docket ID number in the subject line on the first page of
your comment. Please ensure that your comments are submitted within the
specified comment period. Comments received after the close of the
comment period will be marked ``late.'' EPA is not required to consider
these late comments. If you wish to submit CBI or information that is
otherwise protected by statute, please follow the instructions in Unit
I.D. Do not use EPA Dockets or e-mail to submit CBI or information
protected by statute.
1. Electronically. If you submit an electronic comment as
prescribed in this unit, EPA recommends that you include your name,
mailing address, and an e-mail address or other contact information in
the body of your comment. Also, include this contact information on the
outside of any disk or CD ROM you submit, and in any cover letter
accompanying the disk or CD ROM. This ensures that you can be
identified as the submitter of the comment and allows EPA to contact
you in case EPA cannot read your comment due to technical difficulties
or needs further information on the substance of your comment. EPA's
policy is that EPA will not edit your comment, and any identifying or
contact information provided in the body of a comment will be included
as part of the comment that is placed in the official public docket,
and made available in EPA's electronic public docket. If EPA cannot
read your comment due to technical difficulties and cannot contact you
for clarification, EPA may not be able to consider your comment.
i. EPA Dockets. Your use of EPA's electronic public docket to
submit comments to EPA electronically is EPA's preferred method for
receiving comments. Go directly to EPA Dockets at https://www.epa.gov/
edocket/, and follow the online instructions for submitting comments.
Once in the system, select ``search,'' and then key in docket ID number
OPP-2005-0047. The system is an ``anonymous access'' system, which
means EPA will not know your identity, e-mail address, or other contact
information unless you provide it in the body of your comment.
ii. E-mail. Comments may be sent by e-mail to opp-docket@epa.gov,
Attention: Docket ID number OPP-2005-0047. In contrast to EPA's
electronic public docket, EPA's e-mail system is not an ``anonymous
access'' system. If you send an e-mail comment directly to the docket
without going through EPA's electronic public docket, EPA's e-mail
system automatically captures your e-mail address. E-mail addresses
that are automatically captured by EPA's e-mail system are included as
part of the comment that is placed in the official public docket, and
made available in EPA's electronic public docket.
iii. Disk or CD ROM. You may submit comments on a disk or CD ROM
that you mail to the mailing address identified in Unit I.C.2. These
electronic submissions will be accepted in WordPerfect or ASCII file
format. Avoid the use of special characters and any form of encryption.
2. By mail. Send your comments to: Public Information and Records
Integrity Branch (PIRIB) (7502C), Office of Pesticide Programs (OPP),
Environmental Protection Agency, 1200 Pennsylvania Ave., NW.,
Washington, DC 20460-0001, Attention: Docket ID number OPP-2005-0047.
3. By hand delivery or courier. Deliver your comments to: Public
Information and Records Integrity Branch (PIRIB), Office of Pesticide
Programs (OPP), Environmental Protection Agency, Rm. 119, Crystal Mall
2, 1801 S. Bell St., Arlington, VA, Attention: Docket ID
number OPP-2005-0047. Such deliveries are only accepted during the
docket's normal hours of operation as identified in Unit I.B.1.
D. How Should I Submit CBI to the Agency?
Do not submit information that you consider to be CBI
electronically through EPA's electronic public docket or by e-mail. You
may claim information that you submit to EPA as CBI by marking any part
or all of that information as CBI (if you submit CBI on disk or CD ROM,
mark the outside of the disk or CD ROM as CBI and then identify
electronically within the disk or CD ROM the specific information that
is CBI). Information so marked will not be disclosed except in
accordance with procedures set forth in 40 CFR part 2.
In addition to one complete version of the comment that includes
any information claimed as CBI, a copy of the comment that does not
contain the information claimed as CBI must be submitted for inclusion
in the public docket and EPA's electronic public docket. If you submit
the copy that does not contain CBI on disk or CD ROM, mark the outside
of the disk or CD ROM clearly that it does not contain CBI. Information
not marked as CBI will be included in the public docket and EPA's
electronic public docket without prior notice. If you have any
questions about CBI or the procedures for claiming CBI, please consult
the person listed under FOR FURTHER INFORMATION CONTACT.
E. What Should I Consider as I Prepare My Comments for EPA?
You may find the following suggestions helpful for preparing your
comments:
1. Explain your views as clearly as possible.
2. Describe any assumptions that you used.
3. Provide copies of any technical information and/or data you used
that support your views.
4. If you estimate potential burden or costs, explain how you
arrived at the estimate that you provide.
5. Provide specific examples to illustrate your concerns.
6. Make sure to submit your comments by the deadline in this
notice.
7. To ensure proper receipt by EPA, be sure to identify the docket
ID number assigned to this action in the subject line on the first page
of your response.
[[Page 19448]]
You may also provide the name, date, and Federal Register citation.
II. What Action is the Agency Taking?
EPA has received a pesticide petition as follows proposing the
establishment and/or amendment of regulations for residues of a certain
pesticide chemical in or on various food commodities under section 408
of the Federal Food, Drug, and Cosmetic Act (FFDCA), 21 U.S.C. 346a.
EPA has determined that this petition contains data or information
regarding the elements set forth in FFDCA section 408(d)(2); however,
EPA has not fully evaluated the sufficiency of the submitted data at
this time or whether the data support granting of the petition.
Additional data may be needed before EPA rules on the petition.
List of Subjects
Environmental protection, Agricultural commodities, Feed
additives, Food additives, Pesticides and pests, Reporting and
recordkeeping requirements.
Dated: April 1, 2005.
Lois Rossi,
Director, Registration Division, Office of PesticidePrograms.
Summary of Petition
The petitioner's summary of the pesticide petition is printed
below as required by FFDCA section 408(d)(3). The summary of the
petition was prepared by Valent U.S.A. Corporation and represents the
view of the petitioner. The petition summary announces the availability
of a description of the analytical methods available to EPA for the
detection and measurement of the pesticide chemical residues or an
explanation of why no such method is needed.
Valent U.S.A. Corporation
PP 3F6739
EPA has received a pesticide petition PP 3F6739 from Valent U.S.A.
Corporation, 1333 North California Boulevard, Suite 600, Walnut Creek,
CA 94596-8025 proposing, pursuant to section 408(d) of the Federal
Food, Drug, and Cosmetic Act (FFDCA), 21 U.S.C. 346a(d), to amend 40
CFR part 180, by establishing a tolerance for residues of the chemical
etoxazole, 2-(2,6-difluorophenyl)-4-[4-(1,1-dimethylethyl)-2-
ethoxyphenyl]-4,5-dihydrooxazole, in or on the raw agricultural
commodities nut, tree (Crop Group 14), including pistachios at 0.01
parts per million (ppm), almond, hulls at 2.0 ppm, grapes at 0.5 ppm,
and raisins at 1.5 ppm. EPA has determined that the petition contains
data or information regarding the elements set forth in section
408(d)(2) of the FFDCA; however, EPA has not fully evaluated the
sufficiency of the submitted data at this time or whether the data
support granting of the petition. Additional data may be needed before
EPA rules on the petition.
A. Residue Chemistry
1. Plant metabolism. The metabolism of etoxazole is adequately
understood for the purpose of the proposed tolerances.
2. Analytical methods. Practical analytical methods for detecting
and measuring levels of etoxazole have been developed and validated in/
on all appropriate agricultural commodities and respective processing
fractions. The extraction methodology has been validated using aged
radiochemical residue samples from 14C-metabolism studies.
The enforcement methods have been validated in cottonseed, cotton gin
trash, and in fresh mandarin oranges at independent laboratories. The
LOQ of etoxazole in these methods is 0.01 ppm in grapes and nutmeats
and 0.05 ppm in almond, hulls, which will allow monitoring of food with
residues at the levels proposed for the tolerances.
3. Magnitude of residues. An extensive crop residue program has
been conducted for etoxazole in all major growing regions of the United
States for the following crops: Almond and pecans (representing nut,
tree, Crop Group 14), and grapes. The results of these studies can be
summarized as follows:
For almonds, the maximum etoxazole residues from two
applications at 0.135 pounds active ingredient/acre/treatment, was
0.005 ppm for nutmeats and 1.79 ppm for hulls harvested 28-days after
application. Almond hulls were also analyzed for R-3, a metabolite of
etoxazole. The maximum residue of R-3 was as 0.12 ppm.
For pecans, no etoxazole residues were observed in
nutmeats (LOD = 0.005 ppm) treated twice at 0.135 pounds active
ingredient/acre/treatment and harvested 28-days after application.
The maximum etoxazole residue in grapes harvested 28-days
following the last of two treatments at 0.135 pounds active ingredient/
acre/treatment was 0.33 ppm.
The results of a grape processing study indicate that
etoxazole residues concentrate in both grape juice and raisins. The
concentration factor for grape juice was determined in this study to be
5.3X, which exceeds the theoretical concentration factor of 1.2X. Using
this theoretical concentration factor to estimate the tolerance for
juice, a tolerance of 0.32 ppm was calculated. Since this tolerance is
less than the tolerance proposed for grapes, grape juice tolerances are
not required. The concentration factor for raisins was determined in
this study to be 3.5X. The theoretical concentration factor for raisins
is, however, 4.7x. To be consistent with the grape juice calculations,
this theoretical concentration factor was used to determine the
proposed tolerance for raisins.
These field trial data are adequate to support proposed tolerances
of 0.01 ppm for nut, tree (Crop Group 14); pistachios at 0.01 ppm; 2.0
ppm for almond, hull; 0.5 ppm for grapes; and 1.5 ppm for raisins.
Almond, hull is the only commodity under consideration that is a
significant feed item for beef and dairy cattle. Tolerances of 0.03 ppm
in the fat of animals and 0.04 ppm in milk fat, previously proposed and
pending at the Agency, are adequate to support the use on almonds.
None of the commodities under consideration are used as poultry
feed items. Additionally, the results of a hen metabolism study
demonstrated very low potential for residues in feed to transfer to
poultry tissues or eggs. Therefore, no hen residue feeding study was
performed and tolerances are not proposed for secondary residues in
poultry commodities.
B. Toxicological Profile
A full battery of toxicology testing, including studies of acute,
chronic, oncogenicity, developmental, mutagenicity, and reproductive
effects has been completed for etoxazole. The acute toxicity of
etoxazole is low by all routes. Etoxazole is not a developmental or
reproductive toxicant, and is not mutagenic or oncogenic. For the
purpose of dietary risk analysis, Valent proposes 0.04 milligrams/
kilogram body weight/day (mg/kg bwt/day) as the chronic Population
Adjusted Dose (cPAD) and 2 mg/kg bwt/day as the acute Population
Adjusted Dose (aPAD). The cPAD is based on a chronic endpoint of 4 mg/
kg bwt/day no observed adverse effect level (NOAEL) for males from the
rat chronic/oncogenicity feeding study and an uncertainty factor of
100. The aPAD is based on the 200 mg/kg bwt/day NOAEL from the rabbit
developmental toxicity study and an uncertainty factor of 100. Valent
is unable to identify toxicity endpoints of concern for acute, short-
term or chronic human exposures by any route other than oral.
[[Page 19449]]
1. Acute toxicity. The acute toxicity of technical grade etoxazole
is low by all routes. The battery of acute toxicity studies place
etoxazole in Toxicity Category III. The oral LD50 in the rat
was greater than 5 grams/kilogram (g/kg), the dermal LD50
was greater than 2.0 g/kg, and the inhalation LC50 in the
rat was greater than 1.09 milligrams/liter (mg/L). Etoxazole technical
was not an irritant to eyes or skin and was not a skin sensitizer.
2. Genotoxicity. Etoxazole was evaluated and found to be negative
in an Ames reverse mutation assay, a chromosome aberration assay, a
micronucleus assay, and an unscheduled DNA synthesis (UDS) assay.
Etoxazole produced a positive result in the mouse lymphoma gene
mutation assay but only in the presence of metabolic activation.
Etoxazole does not present a genetic hazard.
3. Reproductive and developmental toxicity--i. Rat developmental
study. Etoxazole did not produce developmental toxicity in rats.
Etoxazole technical was administered by oral gavage to pregnant rats at
dosage levels of 40, 200, and 1,000 mg/kg/day on days 6 through 15 of
gestation. There were no mortalities or treatment-related adverse
effects in any dose group. Food consumption was slightly decreased in
dams during the dosing period for the 1,000 mg/kg/day group. On
cesarean section evaluation there was no differences in number of
corpora lutea, number of live and dead fetuses, percent resorption,
placental weight, fetal weight or sex ratio in the dams and no
treatment-related external, visceral or skeletal malformations noted in
any of the fetuses. It was concluded that, the maternal no observed
adverse effect Level (NOAEL) was 200 mg/kg/day, based on decreased food
consumption at 1,000 mg/kg/day. The developmental NOAEL was 1,000 mg/
kg/day, the highest dose tested (HDT).
ii. Rabbit developmental study. Etoxazole did not produce
developmental toxicity in rabbits. Etoxazole technical was administered
by oral gavage to pregnant rabbits at dosage levels of 40, 200, and
1,000 mg/kg/day on days 6 through 18 of gestation. No treatment-related
adverse effects were found on maternal rabbits in the 40 and 200 mg/kg/
day groups. One high dose rabbit died but it is unclear whether this
death was attributed to treatment. Decreased body weight, body weight
gain, food consumption and enlarged liver were noted at 1,000 mg/kg/
day. Cesarean section findings showed that there was no differences in
number of corpora lutea, number of live and dead fetuses, percent
resorptions, placental weight, fetal weight and sex ratio in the dams
and showed no treatment-related malformations (external, visceral,
skeletal) in any of the fetuses. A statistically significant increased
incidence of 27 presacral vertebrae with 13th ribs was
observed in fetuses at 1,000 mg/kg/day compared with controls. This
finding was within historical control range for fetal incidence but
above the historical control range for litter incidence. No dose
response was evident and the variation is considered to be equivocally
treatment related. The NOAEL for maternal and developmental toxicity
was 200 mg/kg/day based on decreased body weight and body weight gain,
decreased food consumption, and liver enlargement at 1,000 mg/kg/day.
The NOAEL for developmental toxicity was 200 mg/kg/day based on
statistically significant increased incidence of 27 presacral vertebrae
with 13th ribs in fetuses at 1,000 mg/kg/day.
iii. Rat reproduction study. Etoxazole showed no effects on
reproduction in a two-generation rat study. Etoxazole technical was fed
to two generations of male and female Sprague Dawley rats at dietary
concentrations of 80, 400, and 2,000 ppm. No treatment-related adverse
effects were observed in the 80 and 400 ppm groups for any parameter.
In the 2,000 ppm group, relative liver weights were increased in the F0
and F1 parental males. No adverse reproductive effects were noted at
any dose level in the incidence of normal estrous cycle, mating index,
fertility and gestation indices, the number of implantation sites, and
duration of gestation in F0 and F1 parental animals. For the offspring,
it was noted that at 2,000 ppm, the viability index on lactation Day 4
was significantly lower in the F1 pups and body weights were lowered in
pups during the latter half of the lactation period. For the F0 and F1
pups of the 80 and 400 ppm groups, there were no treatment-related
adverse effects observed for any parameter, i.e. mean number of pups
delivered, sex ratio, viability indices on lactation days 0, 4 and 21,
clinical signs, body weights and gross pathological findings. The
parental NOAEL was 400 ppm (17.0 mg/kg/day) based on the effects on
relative liver weight in males at 2,000 ppm. The pup NOAEL was 400 ppm
(37.9 mg/kg/day) based on decreased viability on lactation Day 4 and
decreased body weight at 2,000 ppm in the F1 pups. The reproductive
NOAEL was 2,000 ppm (86.4 mg/kg/day), the (HDT).
4. Subchronic toxicity. Subchronic toxicity studies conducted with
etoxazole technical in the rat (oral and dermal), mouse and dog
indicate a low level of toxicity. Effects observed at high dose levels
consisted primarily of anemia and histological changes in the adrenal
gland, liver and kidneys.
i. Rat feeding study. A 90-day subchronic toxicity study was
conducted in rats, with dietary intake levels of 100, 300, 1,000 and
3,000 ppm etoxazole technical. The NOAEL was 100 ppm for males and 300
ppm for females based on increased incidence of hepatocellular swelling
at 1,000 ppm and 3,000 ppm.
ii. Mouse feeding study. A 90-day subchronic toxicity study was
conducted in mice, with dietary intake levels of 100, 400, 1,600, and
6,400 ppm etoxazole technical. The NOAEL was 400 ppm for males and
1,600 ppm for females based on increased alkaline phosphatase activity,
increased liver weights, and increased incidence of hepatocellular
swelling at 6,400 ppm (both sexes) and at 1,600 ppm in males and
enlarged livers in females at 6,400 ppm.
iii. Dog feeding study. Etoxazole technical was fed to male and
female Beagle dogs for 13 weeks at dietary concentrations of 200,
2,000, and 10,000 ppm. The NOAEL was 200 ppm (5.3 mg/kg/day) based on
clinical signs, clinical pathology changes, liver weight effects and
histopathological changes at 2,000 and 10,000 ppm.
iv. Repeated dose dermal study. A 28-day dermal toxicity study was
conducted in rats at dose levels of 30, 100, and 1,000 mg/kg. There
were no treatment related changes in any of the parameters monitored.
The NOAEL was 1,000 mg/kg, the (HDT).
5. Chronic toxicity. Etoxazole technical has been tested in chronic
studies with dogs, rats and mice. Valent proposes a chronic oral
endpoint of 4 mg/kg bwt/day, based on the NOAEL for male rats in a 2-
year chronic toxicity oncogenicity feeding study.
i. Dog chronic feeding study. Etoxazole technical was fed to male
and female beagle dogs for one year at dietary concentrations of 200,
1,000, and 5,000 ppm. The NOAEL was 200 ppm (4.6 mg/kg/day for males
and 4.79 mg/kg/day for females) based on increased absolute and
relative liver weights with corresponding histopathological changes in
the liver at 1,000 and 5,000 ppm.
ii. Rat chronic feeding/oncogenicity study. Etoxazole was not
oncogenic in rats in either of two chronic feeding studies conducted.
In the first study, etoxazole technical was fed to male and female
Sprague Dawley rats for 2-years at dietary concentrations of 4, 16, and
64 mg/kg/day. A trend toward decreased
[[Page 19450]]
body weight gain for males at 64 mg/kg/day in the latter half of the
study was observed. Hemotology and clinical chemistry changes,
increased liver weights and hepatic enlargement at 16 mg/kg/day or
above were observed. Testicular masses, centrilobular hepatocellular
swelling and testicular interstitial (Leydig) cell tumors occurred at
or above 16 mg/kg/day. The interstitial (Leydig) cell tumors were
believed to be incidental. The NOAEL was 4 mg/kg/day for males and 16
mg/kg/day for females. Because an MTD level was not achieved in this
study, a second study was conducted in which etoxazole technical was
fed to male and female Sprague Dawley rats for 2-years at dietary
concentrations of 50, 5,000, and 10,000 ppm. In this study, decreased
mortality, body weight and food consumption/ efficiency (females) at
10,000 ppm was observed. Hematological, clinical, and histopathological
changes of the incisors, and increased liver weights occurred in both
sexes at 5,000 and 10,000 ppm. Centrilobular hepatocellular hypertrophy
was observed in both sexes at 10,000 ppm. The interstitial (Leydig)
cell tumors observed in the first study, were not observed in the
repeat study. The NOAEL in the repeat study was 50 ppm (1.8 mg/kg/day).
iii. Mouse oncogenicity study. Etoxazole was not oncogenic in
either of 2 mouse oncogenicity studies conducted. In the first study,
etoxazole technical was fed to male and female CD-1 mice for 18-months
at dietary concentrations of 15, 60, and 240 mg/kg/day. Increased liver
weights occurred in females at the highest dose tested. Histopathology
parameters were altered for males at 240 mg/kg/day. No neoplastic
lesions were observed at any dose level. The NOAEL was 60 mg/kg/day.
Since the toxicity in this study was minimal and did not meet the
definition of MTD, a second study was conducted at dose levels of 2,250
and 4,500 ppm etoxazole. There were no effects in any group on clinical
observations, mortality, body weight, food consumption or hematology.
Females showed a significant elevation in relative liver weight after
52-weeks of treatment at 4,500 ppm. In histopathology, a significantly
higher incidence of centrilobular hepatocellular fatty change was
observed in males in the 4,500 ppm group necropsied after 78-weeks of
treatment. There were no treatment-related changes in either sex in the
2,250 ppm dose group. No increase in neoplastic lesions were observed
in any treated group of either sex. Therefore, it was concluded that,
the NOAEL is 2,250 ppm (242 mg/kg/day for the males and 243 mg/kg/day
for the females).
6. Animal metabolism. The absorption, tissue distribution,
metabolism and excretion of etoxazole were studied in rats after single
oral doses of 5 or 500 mg/kg, and after 14 daily oral doses at 5 mg/kg.
Etoxazole, labeled in both the t-butylphenyl ring and the oxazole ring
were used in this study. For both single dose groups, most (94-97%) of
the administered radiolabel was excreted in the urine and feces within
7-days after dosing. Most of this excretion occurred in the first 48
hours after dosing. Maximum plasma concentrations occurred 2-4 hours
after dosing, with half-lives ranging from 53-89 hours at the low dose
and 7-44 hours at the high dose. Plasma levels were significantly lower
in females. Concentrations of radioactivity were significantly higher
in the tissues of male rats compared to females. The highest
concentrations occurred at 3 hours after dosing and were greatest in
the gastrointestinal tract and tissues such as liver and kidneys, which
are responsible for metabolism and excretion. By 168 hours, the
concentration in most tissues was below the concentration in the
corresponding plasma, with only the liver and fat having significant
levels of radioactivity. After multiple doses, peak concentrations of
radioactivity in tissues occurred 2 hours after dosing and then
declined. The distribution of radioactivity showed a similar profile to
those found after single oral doses but were significantly higher,
indicating some accumulation. Etoxazole was extensively metabolized by
rats. The main metabolic reactions in rats were postulated to be
hydroxylation of the 4,5-hydrooxazole ring followed by cleavage of the
molecule and hydroxylation of the t-butyl side chain.
7. Metabolite toxicology. In an oral toxicity limit test in rats,
the oral LD50 of metabolite R-3 was estimated to be greater
than 5 g/kg for both male and female rats. No treatment related body
weight changes and no treatment related macroscopic abnormalities were
observed in this study. In another test, the oral toxicity of
metabolite R-7 (as the HCl salt) was assessed. The oral LD50
of this metabolite was also estimated to be greater than 5 g/kg for
both male and female rats. No treatment related macroscopic
abnormalities were observed in this test, although, some clinical signs
were observed within 6-minutes of dosing. Mutagenicity screens were
performed with metabolite R-3 and metabolite R-7 (as the HCl salt).
Neither metabolite was mutagenic when tested with multiple strains of
two bacterial cultures (salmonella typhimurium and e coli).
8. Endocrine disruption. No special studies to investigate the
potential for estrogenic or other endocrine effects of etoxazole have
been performed. However, as summarized above, a large and detailed
toxicology data base exists for the compound including studies in all
required categories. These studies include acute, sub-chronic, chronic,
developmental, and reproductive toxicology studies including detailed
histology and histopathology of numerous tissues, including endocrine
organs, following repeated or long term exposures. These studies are
considered capable of revealing endocrine effects. The results of all
of these studies show no evidence of any endocrine-mediated effects and
no pathology of the endocrine organs. Consequently, it is concluded
that etoxazole does not possess estrogenic or endocrine disrupting
properties.
C. Aggregate Exposure
1. Dietary exposure. A full battery of toxicology testing including
studies of acute, chronic, oncogenicity, developmental, mutagenicity,
and reproductive effects is available for etoxazole. In these risk
assessments, Valent proposes as the chronic oral toxic endpoint the
NOAEL for males from the rat chronic/oncogenicity feeding study, 4 mg/
kg/day. To assess the chronic risk to the U.S. population from exposure
to etoxazole, the daily chronic exposures were compared against an
estimated chronic population adjusted dose (cPAD) of 0.04 mg/kg bwt/
day. This endpoint is derived from the NOAEL from the 2-year chronic
rat study by applying an uncertainty factor of 100 to account for
intraspecies and interspecies variations. There is no evidence that any
additional safety factors are needed to further protect vulnerable
subpopulations. The proposed acute oral toxic endpoint is the NOAEL
from the rabbit oral developmental toxicity study, 200 mg/kg/day. To
assess the acute risk to the U.S. population from exposure to
etoxazole, acute exposures were compared against an estimated acute
population adjusted dose (aPAD) of 2 mg/kg bwt/day. This endpoint is
derived from the NOAEL from the rabbit oral developmental toxicity
study by applying an uncertainty factor of 100 to account for
intraspecies and interspecies variations. Based on dietary, drinking
water, and non-occupational exposure assessments, there is reasonable
certainty of no harm
[[Page 19451]]
to the U.S. population, any population subgroup, or infants and
children from short-term or chronic exposure to etoxazole.
i. Food. Dietary exposure was estimated using the Cumulative and
Aggregate Risk Evaluation System (CARES). Acute dietary exposure was
estimated for the overall U.S. population and 16 population subgroups
using proposed tolerances and conservative estimates of the percentages
of crop treated. The results demonstrate that estimated exposure is
less than 1% of the estimated aPAD (at the 99.9th
percentile) for all population groups examined. Acute dietary exposure
for the overall U.S. population was estimated to be 0.006 mg/kg bwt/day
at the 99.9th percentile of exposure (0.29% of the aPAD).
Chronic dietary exposure was estimated for the overall U.S. population
and 16 population subgroups. Annual exposure for the overall U.S.
population was estimated to be 0.00014 mg/kg bwt/day, representing
0.36% of the estimated cPAD. Annual exposure for the most highly
exposed population subgroup, children 1-2 years of age, was estimated
to be 0.00065 mg/kg bwt/day, or 1.62% of the estimated cPAD.
ii. Drinking water. Since etoxazole is applied outdoors to growing
agricultural crops, the potential exists for the parent or its
metabolites to reach ground water or surface water that may be used for
drinking water. But, because of the physical properties of etoxazole,
it is unlikely that etoxazole or its metabolites can leach to potable
ground water. Although, relatively stable to hydrolysis, etoxazole
undergoes fairly rapid photolysis, degrades fairly readily in soil and
is immobile in all soil types examined. To quantify potential exposure
from drinking water, FIRST and SCI-GROW models were used to estimate
surface water and ground water residues. Estimated surface water
residues were much higher than estimated ground water residues and
therefore, the surface residues were used as the Drinking Water
Environmental Concentration (DWEC). The peak (acute) concentration
predicted in the simulated pond water was estimated to be 2.47 ppb and
the annual average (chronic) concentration predicted in the simulated
pond water was estimated to be 1.93 ppb. To assess the contribution to
the dietary risk from exposure to drinking water containing residues of
etoxazole, these DWEC's are compared to drinking water levels of
comparison (DWLOC's), the maximum drinking water concentration allowed
before combined water, dietary, and other exposures will exceed the
population adjusted doses. If the DWLOC is greater than the DWEC, then
overall exposure will not exceed the population adjusted doses and
combined exposure from water and food is considered to be acceptable.
Acute DWLOC's for etoxazole range from 19,900 to 69,910 ppb and chronic
DWLOC's range from 377 to 1,380 ppb for all U.S. population subgroups
examined. Since these DWLOC's exceed the modeled acute and chronic DWEC
surface water residues by a wide margin, it can be concluded that,
exposure to potential residues in drinking water is negligible and that
aggregate (food and water) exposure to etoxazole residues will be
acceptable.
2. Non-dietary exposure. Etoxazole is proposed only for
agricultural uses and no homeowner or turf uses. Thus, no non-dietary
risk assessment is needed.
D. Cumulative Effects
Section 408(b)(2)(D)(v) requires that the Agency must consider
``available information'' concerning the cumulative effects of a
particular pesticide's residues and ``other substances'' that have a
common mechanism of toxicity. Available information in this context
include not only toxicity, chemistry, and exposure data, but also
scientific policies and methodologies for understanding common
mechanisms of toxicity and conducting cumulative risk assessments. For
most pesticides, although, the Agency has some information in its files
that may turn out to be helpful in eventually determining whether a
pesticide shares a common mechanism of toxicity with any other
substances, EPA does not at this time have the methodologies to resolve
the complex scientific issues concerning common mechanism of toxicity
in a meaningful way.
In consideration of potential cumulative effects of etoxazole and
other substances that may have a common mechanism of toxicity, there
are currently no available data or other reliable information
indicating that any toxic effects produced by etoxazole would be
cumulative with those of other chemical compounds. Thus, only the
potential risks of etoxazole have been considered in this assessment of
aggregate exposure and effects.
Valent will submit information for EPA to consider concerning
potential cumulative effects of etoxazole consistent with the schedule
established by EPA at (62 FR 42020) (Aug. 4, 1997) and other subsequent
EPA publications pursuant to the Food Quality Protection Act.
E. Safety Determination
1. U.S. population--i. Acute risk. The potential acute exposure
from food to the U.S. population and various non-child/infant
population subgroups are estimated to be 0.15 to 0.30% of the proposed
aPAD. Exposure to potential acute residues in drinking water is
expected to be negligible, as acute DWLOC's are substantially higher
than modeled acute DWEC's. Based on this assessment, it can be
concluded that, there is a reasonable certainty that no harm to the
U.S. population or any population subgroup will result from acute
exposure to etoxazole.
ii. Chronic risk. The potential chronic exposure from food to the
U.S. population and various non-child/infant population subgroups are
estimated to be 0.24 to 1.59% of the proposed cPAD. Chronic exposure to
potential residues in drinking water is also expected to be negligible,
as chronic DWLOC's are substantially higher than modeled chronic
DWEC's. Based on this assessment, it can be concluded that there is a
reasonable certainty that no harm to the U.S. population or any
population subgroup will result from chronic exposure to etoxazole.
2. Infants and children--i. Safety factor for infants and children.
In assessing the potential for additional sensitivity of infants and
children to residues of etoxazole, FFDCA section 408 provides that EPA
shall apply an additional margin of safety, up to ten-fold, for added
protection for infants and children in the case of threshold effects
unless EPA determines that a different margin of safety will be safe
for infants and children. The toxicological data base for evaluating
prenatal and postnatal toxicity for etoxazole is complete with respect
to current data requirements. There are no special prenatal or
postnatal toxicity concerns for infants and children, based on the
results of the rat and rabbit developmental toxicity studies or the 2-
generation reproductive toxicity study in rats. Valent has concluded,
that reliable data support use of the standard 100-fold uncertainty
factor and that an additional uncertainty factor is not needed for
etoxazole to be further protective of infants and children.
ii. Acute risk. The potential acute exposure from food to infants
and children are estimated to be 0.28 to 0.97% of the proposed aPAD.
Exposure to potential acute residues in drinking water is expected to
be negligible, as acute DWLOC's are substantially higher than modeled
acute DWEC's. Based on this assessment, it can be concluded that, there
is a reasonable certainty that
[[Page 19452]]
no harm to infants and children will result from acute exposure to
etoxazole.
iii. Chronic risk. The potential chronic exposure from food to
infants and children are estimated to be 0.64 to 1.62% of the proposed
cPAD. Chronic exposure to potential residues in drinking water is
expected to be negligible, as chronic DWLOC's are substantially higher
than modeled DWEC's. Based on this assessment, it can be concluded
that, there is a reasonable certainty that no harm to infants and
children will result from chronic exposure to etoxazole.
3. Safety determination summary. Aggregate acute or chronic dietary
exposure to various subpopulations of children and adults demonstrate
acceptable risk. Acute and chronic dietary exposures to etoxazole
occupy considerably less than 100% of the appropriate PAD. EPA
generally has no concern for exposures below 100% of the acute and
chronic PAD's because these represent levels at or below which daily
aggregate dietary exposure over a lifetime will not pose appreciable
risks to human health. Chronic and acute dietary risk to children from
etoxazole should not be of concern. Further, etoxazole has only
agricultural uses and no other uses, such as indoor pest control,
homeowner or turf, that could lead to unique, enhanced exposures to
vulnerable sub-groups of the population. It can be concluded that,
there is a reasonable certainty that no harm will result to the U.S.
population or to any sub-group of the U.S. population, including
infants and children, from aggregate chronic or aggregate acute
exposures to etoxazole residues resulting from the proposed uses.
F. International Tolerances
Etoxazole has not been evaluated by the JMPR and there are no
codex maximum residue limits (MRL) for etoxazole. MRL values have been
established for etoxazole in the following countries: Turkey, Israel,
South Africa, Japan, France, Taiwan, and Korea. The use pattern and
MRL's are similar to those proposed for the U.S.
[FR Doc. 05-7223 Filed 4-12-05; 8:45 am]
BILLING CODE 6560-50-S